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Eingeladener Vortrag
- nein (22)
Im Rahmen des europäischen Forschungsprojekts Microcon wurden wirtschaftliche und ökologische Ansätze zur Verwendung von Feinstfüllstoffen so genannten Microfillern in Bauprodukten, die auf zementgebundenen Systemen basieren, untersucht. Hauptzielsetzung war die Entwicklung von modifizierten Bindemitteln und Zusätzen für die Transportbeton- und Fertigteilindustrie bis hin zur Marktreife. Eine der Neuentwicklungen war eine leicht handhabbare Werktrockenmischung für selbstverdichtenden Beton (SVB), die alle Schlüsselkomponenten bis auf das Bindemittel und die grobe Gesteinskörnung enthält und eine hohe Robustheit in der Anwendung gewährleistet.
Varying ambient temperatures in plants or on construction sites during casting of SCC can cause serious problems affecting the fresh concrete performances, such as rheological properties and setting time, with consequences for the hardened properties in the structure. By sensible choices of the components, the robustness of SCC mixtures against temperature variations can be improved. However, this aspect has not been the focus of intensive research yet. In this study the effects of varied ambient temperatures on the early performance of differently composed SCC mixtures are investigated, with emphasis on changes in rheology, early deformations, heat evolution and setting. Focus is placed on the study of the influence of the polycarboxylate ether molecule type as well as different viscositymodifying agents on the temperature robustness. Effects on the relevance for practical concrete applications are evaluated, which will provide a reliable framework of possible actions on the appropriate use of admixtures for SCC.
Stabilising admixtures are commonly used additives in repair mortars and grouts. Beyond this, such type of admixture is increasingly used in concrete and other cementitious materials. In particular when fresh mortar or concrete properties have to be adjusted reliably, stabilising agents can be beneficially used to improve workability and robustness of the mixture. The mode of operation of these admixtures varies, rather affecting either the liquid phase or the solid particles in the dispersion, both causing strong interactions with the mortar or concrete system, and significant changes in their rheological behaviour. Furthermore, these are strongly affected by the environmental temperature during the casting process. In the paper the effect of temperature on the performance of stabilising agents in cementitious systems is presented and how performance changes affect fresh and hardening mortar or concrete properties. Particular attention is placed on interactions between stabilising agents and superplasticizers. Results are discussed with special focus on self-compacting concrete.
Today polycarboxylate ether based superplasticizer (PCE) is commonly used in concrete technology when high flow properties and water reduction are specified. The ionic strength of the polymers’ backbones determines the adsorption behaviour of polymers on clinker and early hydration products. The amount of required polymers for specified flow properties and the performance over the time of casting is thus determined by the molecular structure of the superplasticizer. The time depending consumption of polycarboxylate ether polymers strongly affects the reaction of aluminates and sulphate ions as well as the hydration process in general. Hence, the choice of polymers for particular flow properties greatly affects the very early properties of cementitious materials such as setting, heat evolution and autogenous deformations.
In order to better understand how PCEs influence the early properties, mixes from cement, limestone filler, viscosity modifying agent and water were varied with a high and a low charge density superplasticizer in differing amounts. Results are presented from measurements with an automatic Vicat device, an isothermal heat flow calorimeter, and shrinkage cones. Tests were conducted at 5, 20, and 30 °C.
It is shown that in presence of PCE the final set correlates well with the inflexion point of the heat flow curve, which emphasises the interrelation between C-S-H formation and setting. No such clear correlation can be found for the initial set, which is attributed to the fact that the initial set is rather a rheological than a structural phenomenon, so that other effects overlap with C-S-H formation. The results demonstrate that for a given polymer concentration low charge density polymers yield earlier setting than high charge polymers. However, this influence is overridden by the influence of the total amount of polymers in a cementitious system. Since PCE is typically added according to rheological specifications, and low charge PCE typically requires higher amounts of polymers than high charge PCE for comparable flow performance, low charge PCE retards setting more than high charge PCE.
The paper furthermore points out that there is no significant influence of the polymer type or amount on the early deformations. Since type and amount strongly affect the hydration, it is demonstrated that early setting causes higher strain after the final set. It is hence concluded that higher PCE solid contents reduce the risk of early cracks that occur at time of setting, when a solid structure has already been formed but without resistance against cracks yet.