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Modified Yoldas sols can be used to prepare crack-free well adherent layers on different substrate materials such as sodalime glass, corundum and metal (IN-718). These layers having thicknesses of 0.6 µm are strain tolerant and withstand thermal cycling between 810 °C and room temperature. Introducing alpha-Al2O3 filler particles into modified Yoldas sols allows the preparation of thicker layers of 1.6 µm, which as well can be thermally cycled without noticeable delaminations. Chemical bonding seems to be the predominant layer bonding mechanism.
Alumina coatings with differing phase compositions were deposited on Inconel-718 (IN-718) Ni-base
superalloy substrates using solgel processing. Mass gain measurements served for studying the oxidation
behavior of coated metal surfaces if exposed to 800°C and 900°C for up to 4000 h in static air. Itwas found, that
alumina coatings significantly reduce the oxidation related mass gain of IN-718 even after heating to 900°C
for 4000 h. Transmission electron microscopy (TEM) studies revealed diffusion of elements from the metal
substrate (IN-718) into the alumina coatings and to a much lower degree from the coating into the
substrate. These diffusion processes are greatly influenced by the phase composition of the coatings, especially
by the presence of alpha-alumina.
Alumosols in combination with well dispersed corundum were successfully used to form up to 2.5 ìm thick coatings on the Ni-base alloy SC16. These coatings withstood heat treatments at 700 °C in a water vapour containing atmosphere. The heat treatment caused formation of delta-alumina in the coating and diffusion of chromium and titanium into the coating.
Dynamic and quasi-static FE calculation of impact from 9 metre drop of spent fuel transport cask
(2009)
The drop from 9 m height onto a rigid target is one of the required proofs of safety for packages of radioactive materials. Direct dynamic finite element method (FEM) calculations and combined two step analytical quasi-static finite element (FE) calculations are both applied for the simulation of a 9 m drop test. This paper gives a comparative example of both approaches for the 9 m side drop simulation of the spent fuel transport cask with wood filled impact limiter. The model for dynamic FEM consists of cask body and impact limiter. Detailed material properties and geometry descriptions from each component of the impact limiter are required. The results (stress fields in the cask body) are obtained directly from the calculation. The combined method provides as intermediate results the force-deformation characteristic of impact limiter. The maximum impact limiter force determined by the law of energy conservation during the drop is then - in a second step - applied on the cask body in a quasi-static FE model in order to calculate the stresses. In this paper, the rigid body deceleration and the maximum stress in the middle of the cask body are used for the comparison between the dynamic FEM and the combined method. Similar maximum rigid body deceleration-time curves were obtained by both methods for the horizontal 9 m free fall. Concerning the stress in the cask body the dynamic FEM results oscillate about values calculated by the combined quasi-static approach. If the combined quasi-static approach is used in the safety assessment of a cask, a suitable factor has to be applied on its results to take into account the additional dynamic effects.
Porous ceramics prepared by the foam replication technique have a high porosity and low mechanical stability. It has been reported that coating such porous ceramics with gelatin allows for an improved compressive strength. Little details regarding the influence of important gelatin parameters such as concentration, temperature and drying conditions as well as bloom number which is a measure of the gel rigidity, on this toughening effect are available. This paper investigates the influence of these parameters on compressive strength of gelatin coated porous hydroxyapatite ceramics. It was found that concentration in the gelatin sols has a marked impact whereas sol temperature, bloom number and differing conditions during subsequent drying have only little influence on the compressive strength of the coated ceramics.