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Eingeladener Vortrag
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Evaluating porosity in cordierite diesel particulate filter materials, part 1 X-ray refraction
(2013)
Bi-continuous porous ceramics for filtration applications possess a particularly complicated microstructure, with porosity and solid matter being intermingled. Mechanical, thermal, and filtration properties can only be precisely estimated if the morphology of both solid matter and porosity can be quantitatively determined. Using x-ray absorption and refraction, we quantitatively evaluate porosity and pore orientation in cordierite diesel particulate filter ceramics. Porosity values turn out to agree with mercury intrusion measurements, while pore orientation factors agree with published crystallographic texture data.
For validation of structural integrity under normal and hypothetical accident conditions during transport and storage of radioactive material the Federal Institute for Materials Research and Testing (BAM) focuses its safety related scientific research on advanced mechanical safety assessment methods including simulation of high rate impact of model components and structures. A drop and crash test facility with an unyielding target and a load capacity of 1.200 kg was designed for materials testing of component size specimen under impact conditions at elevated and higher loading rates. The maximum drop height is 12 meters which enables impact velocities up to 15 m/s. An exactly falling test object or drop weight allows impact, bending, compression as well as crash and crush tests with maximum input energy of 118 kJ. An arresting unit has been developed to avoid multiple impacts during instrumented drop tests. The paper presents experimental techniques and examples of various measurement methods and advancements in order to assess assumption of materials and components behavior by definite displacement and stresses within mechanical testing. Instrumented drop weight tests are performed to complete materials data base and energy absorption of shock-absorbing materials and structures as well as to implement materials and structural parameters into FEA of reference structures. Furthermore, fracture mechanics parameters of thick walled DCI containers by means of dynamic bending tests are characterized by crack initiation and crack resistance behavior at the lowest operational temperature depending on the strain rate.
Complementary to Part 1 of this work, the bi-continuous microstructure of porous synthetic cordierite ceramics for filtration applications was investigated using 3D x-ray computed tomography at different resolutions. Applying both Fast Fourier Transform and a newly developed image analysis algorithm, we quantitatively evaluated porosity and pore orientation. The statistical approach allows extraction of spatially resolved or average values. Porosity values based on x-ray absorption agree with mercury intrusion measurements, while pore orientation factors agree with x-ray refraction data (Part 1 of this work), and with published crystallographic texture data.
Internal cask content collisions during drop test of transport casks for radioactive materials
(2013)
In transport casks for radioactive materials, significantly large axial and radial gaps between cask and internal content are often present because of certain specific geometrical dimensions of the content (e.g. spent fuel elements) or thermal reasons. The possibility of inner relative movement between content and cask will increase if the content is not fixed. During drop testing, these movements can lead to internal cask content collisions, causing significantly high loads on the cask components and the content itself. Especially in vertical drop test orientations onto a lid side of the cask, an internal collision induced by a delayed impact of the content onto the inner side of the lid can cause high stress peaks in the lid and the lid bolts with the risk of component failure as well as impairment of the leak tightness of the closure system. This paper reflects causes and effects of the phenomenon of internal impact on the basis of experimental results obtained from instrumented drop tests with transport casks and on the basis of analytical approaches. Furthermore, the paper concludes the importance of consideration of possible cask content collisions in the safety analysis of transport casks for radioactive materials under accident conditions of transport.
Leakage testing during lateral displacement of metallic seals under mechanical accident impact
(2013)
A management system based on international, national or other standards acceptable to the competent authority shall be established and implemented for all activities including design, manufacture, testing, documentation, use, maintenance, inspection in accordance with IAEA SSR-6. Hereby, quality assured testing and documentation can substantially contribute to the demonstration of package design compliance with the regulations. Nowadays, a drop test campaign within the approval process of packages for radioactive materials can be a very complex and extensive project including various test and measurement techniques. On this basis of procedures and documents the experimental tests of packages and containers are performed with quality proofed results and a high reliability. A complete traceability and direct transferability of package design test results can give particular importance to the type approval procedure.
In context with new cask designs and their approval procedure, the experimental testing of impact limiters under drop test conditions becomes more and more important in order to assess the damage mechanics behaviour and safety margins for validation reasons. In recent years, various designs of impact limiters have been tested by the Federal Institute for Materials Research and Testing within specific component testing and particularly with regard to type B package design approval procedures. The paper focuses on the experimental realisation of impact limiter tests and presents implemented measurement techniques to determine the amount of deformation and to explain the impact behaviour by means of photogrammetric metrology and three-dimensional fringe projection method, high speed motion analysis and adjusted deceleration measurements.
Mechanical loading conditions of transport and storage casks for radioactive materials in accidental scenarios are highly affected by the behavior of both: the impact limiters and the footing materials. To minimize potential damages during the handling of casks, a so called damping concrete is frequently used for the footings in interim nuclear facilities. It obtains its shock absorbing properties through admixing of polymer cells. For a comprehensive mechanical evaluation of casks, advanced material models are also needed for damping concrete. In order to characterize the mechanical properties and to develop numerical material models, penetration tests were carried out at different test facilities of BAM. The tests contain static and dynamic penetration tests on cubic specimen with an edge length of 100 mm as well as mortared specimen with a size of 240 x 240 x 50 cm³. Indenters with different geometries and diameters were used for these model-sized penetration tests. Subsequently a full-scale cylindrical cast-iron indenter with a diameter of 110 cm was dropped of 5 m height on a realistic damping concrete footing.