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Anwendung des instrumentierten Kerbschlagbiegeversuchs zur Abschätzung der Rissauffangzähigkeit
(2001)
Die moderne Bauteilsicherheitsbewertung basiert auf Methoden der Bruchmechanik unter Anwendung von bruchmechanischen Kennwerten, die den Werkstoffwiderstand gegen Rissinitiierung und Rissfortschritt sowie das Rissauffangverhalten charakterisieren. Die experimentelle Ermittlung der Rissarrestzähigkeit ist im Allgemeinen jedoch schwierig und aufwendig. In diesem Beitrag werden Korrelationen für die Abschätzung der Sprödbruch-Übergangstemperatur (TNDT) und der Rissarrestzähigkeit (KIa) mit Hilfe einer Übergangstemperatur, die der Rissauffangkraft im instrumentierten Kerbschlagbiegeversuch entspricht, vorgestellt. Als Kriterien für den Zähigkeitsübergang gelten die an Charpy-V-Proben gemessene Rissauffangkraft 4 kN und die nach Master-Curve-Ansatz berechnete mittlere Rissarrestzähigkeit 100 MPam. Die für verschiedene Baustähle vorgeschlagenen Korrelationen zwischen den Übergangstemperaturen T(Fa = 4 kN), T(KIa) und TNDT werden am Beispiel des Stahles 18Ch2MFA bestätigt.
Federal Institute for Materials Research and Testing (BAM) is the competent authority for mechanical and thermal safety assessment of transport packages for spent fuel and high level waste in Germany. In context with package design approval of the new German high level waste cask CASTOR® HAW28M, BAM performed several drop tests with a half scale model of the CASTOR® HAW/TB2. The cask is manufactured by Gesellschaft für Nuklear Service mbH and was tested under accident transport conditions on the 200 tons BAM drop test facility at the BAM Test Site Technical Safety. For this comprehensive test program, the test specimen CASTOR® HAW/TB2 was instrumented at 21 measurement planes with altogether 23 piezo resistive accelerometers, five temperature sensors and 131 triaxial strain gauges in the container interior and exterior respectively. The strains of four representative lid bolts were recorded by four uniaxial strain gauges per each bolt. Helium leakage rate measurements were performed before and after each test in the above noted testing sequence. The paper presents some experimental results of the half scale CASTOR® HAW/TB2 prototype (14 500 kg) and measurement data logging. It illustrates the extensive instrumentation and analyses that are used by BAM for evaluating the cask performance to the mechanical tests required by regulations. Although some of the quantitative deceleration, velocity and strain values cannot be shown because of confidentially issues, they are provided qualitatively to illustrate the types of measurements and methodologies used at BAM.
The performance of shock absorbers has been tested in specific regulatory drop tests onto an unyielding target at the BAM drop test facility. Optical surface digitisation methods have been used to measure, analyse and evaluate permanent deformations of shock absorbers more systematically. The measurement principle of the used fringe projection technique and its technical application to shock absorber investigations is explained in detail. Furthermore, examples of shock absorber testing results as well as final data visualisation are given in the present paper.
Drop and fire testing of spent fuel and HLW transport casks at 'BAM test site technical safety'
(2011)
BAM, as a competent German government institute for the mechanical and thermal testing of radioactive material transport and storage containers, operates unique drop and fire test facilities for experimental investigations on the open air BAM Test Site Technical Safety. To be able to perform even drop tests with full scale spent fuel or HAW casks (i.e. the German CASTOR cask designs), BAM constructed in 2004 a large drop test facility capable to handle 200 ton test objects, and to drop them onto a steel plate covered unyielding target with a mass of nearly 2600 ton. Drop test campaigns of the 181 ton GNS CONSTOR V/TC, the 129 ton MHI MSF-69BG and a 1:2 scale model of the GNS CASTOR HAW28M (CASTOR HAW/TB2) have been performed since then. The experimental BAM drop testing activities can be supported also by drop testing of smaller packages (up to 2 ton) in an in-house test facility and by dynamic, guided impact testing of package components and material specimen inside a new drop test machine. In May 2008, a new modern fire test facility was put into operation. The facility provides two test stands fired with liquid propane. Testing in every case has to be completed by computational investigations, where BAM operates appropriate finite element modelling on appropriate computer codes, e.g. ABAQUS, LS-DYNA, ANSYS and other analytical tools.
Evaluating porosity in cordierite diesel particulate filter materials, part 1 X-ray refraction
(2013)
Bi-continuous porous ceramics for filtration applications possess a particularly complicated microstructure, with porosity and solid matter being intermingled. Mechanical, thermal, and filtration properties can only be precisely estimated if the morphology of both solid matter and porosity can be quantitatively determined. Using x-ray absorption and refraction, we quantitatively evaluate porosity and pore orientation in cordierite diesel particulate filter ceramics. Porosity values turn out to agree with mercury intrusion measurements, while pore orientation factors agree with published crystallographic texture data.
The mechanical and geometrical properties of impact targets greatly influence the outcome of a drop test. The International Agreement concerning the International Carriage of Dangerous Goods by Road (ADR) as well as ISO 2248 describe the characteristics of impact targets for drop tests of dangerous goods packagings.
According to these regulations, the impact target’s surface needs to be unyielding, under testing conditions non-deformable, flat, and integral with a mass at least 50 times that of the heaviest packaging to be tested. The problem is that many production facilities, especially manufacturers of corrugated fibreboard boxes, do not have their own testing device with the required 50 times mass ratio of the impact target for a regulation compliant drop test during series production. Furthermore, at UN level it is considered necessary to revise these requirements.
In the present paper, the impact target requirements are examined in detail and compared with those in other technical areas (e.g., impact target for container for the transport of radioactive materials). A research method is being developed to investigate the dependency between the mass ratio of the packaging and the target as well as the damage resistance of a drop tested package in relation to specific design characteristics. The results are of high relevance for industry purposes and intended to ensure a uniform level of safety assessment for the mechanical testing of dangerous goods packagings.
Complementary to Part 1 of this work, the bi-continuous microstructure of porous synthetic cordierite ceramics for filtration applications was investigated using 3D x-ray computed tomography at different resolutions. Applying both Fast Fourier Transform and a newly developed image analysis algorithm, we quantitatively evaluated porosity and pore orientation. The statistical approach allows extraction of spatially resolved or average values. Porosity values based on x-ray absorption agree with mercury intrusion measurements, while pore orientation factors agree with x-ray refraction data (Part 1 of this work), and with published crystallographic texture data.
Internal cask content collisions during drop test of transport casks for radioactive materials
(2013)
In transport casks for radioactive materials, significantly large axial and radial gaps between cask and internal content are often present because of certain specific geometrical dimensions of the content (e.g. spent fuel elements) or thermal reasons. The possibility of inner relative movement between content and cask will increase if the content is not fixed. During drop testing, these movements can lead to internal cask content collisions, causing significantly high loads on the cask components and the content itself. Especially in vertical drop test orientations onto a lid side of the cask, an internal collision induced by a delayed impact of the content onto the inner side of the lid can cause high stress peaks in the lid and the lid bolts with the risk of component failure as well as impairment of the leak tightness of the closure system. This paper reflects causes and effects of the phenomenon of internal impact on the basis of experimental results obtained from instrumented drop tests with transport casks and on the basis of analytical approaches. Furthermore, the paper concludes the importance of consideration of possible cask content collisions in the safety analysis of transport casks for radioactive materials under accident conditions of transport.
Bi-continuous porous ceramics for filtration applications possess a particularly complicated microstructure, whereby porosity and solid matter are intermingled. Mechanical, thermal, and filtration properties can only be precisely estimated if the morphology of both solid matter and porosity can be quantitatively determined. Using 3D computed tomography (CT) at different resolutions, and several X-ray refraction-based techniques, we quantitatively evaluated porosity and pore orientation in cordierite diesel particulate filter ceramics.Moreover, applying both Fast Fourier Transform (FFT) and a newly developed image analysis algorithm (directional interface variance analysis, DIVA), we quantitatively evaluated porosity and pore orientation. Both the experimental techniques and the statistical approach allow extraction of spatially resolved or average values.Porosity values from synchrotron computed tomography used turn out to agree with mercury intrusion measurements, while pore orientation factors agree with published crystallographic texture data. This latter point also implies that the study of the pore/matter interface is sufficient to describe the morphological properties of these materials.
BAM safety related research of containers for radioactive material focuses on advanced mechanical safety assessment methods for verification of the structural integrity and leak tightness under normal conditions of transport and hypothetical accident conditions during transport and storage. An essentially unyielding target with a rigid surface is required for impact tests performed for package approval according to IAEA regulations. In addition to specification of a target, e.g. with a combined mass more than 10 times that of the specimen for drop tests, unyielding target characteristics have been investigated with various package designs and different impact tests. The unyielding target of the BAM drop test facility, a reinforced concrete block together with an embedded and anchored mild steel plate, provides relatively large mass and stiffness with respect to the packages being tested. For monitoring reasons accelerometers and strain gauges are embedded in the concrete block of the foundation at several positions. Additionally, dynamic impact responses like vibrations and rigid body motion can be measured by seismic accelerometers. The mechanical characterisation of the target's rigidity is based on experimental results from various drop tests. Test containers with weights of 181 000 kg, 127 000 kg and 8010 kg hit the target with velocities up to 13·5 m s-1 in the horizontal and vertical drop positions. The rigidity of the impact target can be demonstrated with experimental results confirmed by analytical approaches. Some conclusions can be drawn about experimental testing as well as analytical calculations in order to compare impact effects.
This paper presents a comparison between full scale prototype and reduced scale model drop test data in regard to similarity mechanics. Together with a current BAM research project, the paper contributes to the further development of mechanical evaluation methods for safety assessment of RAM transport and storage packages including the transferability of package impact response from reduced scale models to full scale packages.
This paper presents technical details of the drop test performance as well as some experimental results of tests carried out with the Japanese 'Yoyushindo-Disposal' waste container for intermediate depth disposal. The drop test program comprised three single 8 m drop tests at the specimen's corner edge orientation onto a concrete slab. The slab was connected to the unyielding IAEA target of the BAM's 200 t drop test facility. The three tested specimens had masses between 20 000 and 28 000 kg depending on their content mass. The tests were accompanied by various metrology, such as strain and deceleration measurements, optical three-dimensional deformation methods, leak tightness testing and test installation for potential particle release measurements to collect a set of data for establishing a basis for safety assessment.
Mechanical design assessment approaches of actual spent fuel and HLW transport package designs
(2010)
In context with new cask designs and their approval procedure, the experimental testing of impact limiters under drop test conditions becomes more and more important in order to assess the damage mechanics behaviour and safety margins for validation reasons. In recent years, various designs of impact limiters have been tested by the Federal Institute for Materials Research and Testing within specific component testing and particularly with regard to type B package design approval procedures. The paper focuses on the experimental realisation of impact limiter tests and presents implemented measurement techniques to determine the amount of deformation and to explain the impact behaviour by means of photogrammetric metrology and three-dimensional fringe projection method, high speed motion analysis and adjusted deceleration measurements.
Auswirkungen von Ermüdungsbeanspruchungen auf Struktur und Eigenschaften von Fahrbahndeckenbeton
(2015)
Ausgehend von der Zielsetzung der DFG-Forschergruppe 1498, die Einflüsse auf den AKR-Schädigungsprozess in Fahrbahndecken aus Beton grundlegend zu klären, sind zwei aufeinander aufbauende Untersuchungsschwerpunkte Gegenstand dieses Beitrags. Im ersten Schwerpunkt wurden die prüftechnischen Voraussetzungen für die Charakterisierung der Degradation und damit der Rissbildung im Fahrbahndeckenbeton durch die Vorschädigung infolge von Ermüdungsbeanspruchungen geschaffen. Realisiert wurde dies durch die Implementierung und Optimierung eines Monitoringsystems im zyklischen 4-Punkt-Biegeversuch zur simultanen Erfassung der Rissbildung im großformatigen Schwingbalken. Zusätzlich wurde die Röntgen-3D-Computertomografie für die hochauflösende räumliche quantitative Rissanalyse in den Bohrkernen aus den Schwingbalken ohne und mit Vorschädigung weiterentwickelt. Im zweiten Untersuchungsschwerpunkt wurde mittels vielfältiger Experimente an kleinformatigen Probekörpern aus dem Schwingbalken gezeigt, dass durch die Ermüdungsbeanspruchung die bruchmechanischen Materialkennwerte des Betons zum Teil eine signifikante Veränderung erfahren. Based on the objective of the DFG (German research foundation) funded research group 1498 to clarify the influences on the ASR damage process, this paper deals with two focuses of investigation. In the first focus the technical requirements for the characterisation concerning the degradation and the formation of cracks in concrete pavements by the pre-damage as a result of fatigue loading were created. This was realized by the implementation and the optimisation of a monitoring system in the cyclic four point bending test to capture simultaneously the formation of cracks in the beam under sinusoidal bending load. In addition, the X-ray 3D-computed tomography was enhanced for the high-resolution quantitative spatial crack analysis in the drilling cores extracted of the beam under sinusoidal bending load without and with a pre-damage. Building on the first focus, in the second focus of investigation a significant change of the fracture-mechanical properties of the concrete as a result of fatigue loading has been demonstrated in numerous experiments using small specimens extracted from the beam under sinusoidal bending load.
Due to the high damping mechanical properties of fiberboard materials, corrugated fiberboard boxes are widely used as transport packagings of dangerous goods. Since there is risk of vertical impact within the distribution system, drop tests are performed as design type tests to assess a package’s ability to withstand damage. In this context, however, little is known regarding the transient mechanical response of a filled fiberboard box. The reason is that the nature of the packaging material presents challenges in identifying the deformation mechanisms experimentally. The aim of this work is to provide a framework for predicting the damage resistance of complete, filled corrugated fiberboard boxes which are ready for transportation. Therein, drop test finite-element simulations are used and validated by experimental results. These numerical calculation models are a valuable tool for virtual product development and contribute to the optimization of the design cycle.
For dangerous goods packagings, drop testing onto an essential unyielding target can be used to assess the mechanical resistance to impact loads. Adopted regulations like ADR/RID require that the impact surface provided shall be integral with a mass at least 50 times than that of the heaviest package to be tested. The problem is that many manufacturers do not possess impact targets that satisfy the required 50 times mass ratio for regulative drop tests during series production. The objective of this work is to verify existing and define improved criteria for impact target structures based on systematic investigations. Previous evidence highlights the relevance of other parameters in addition to the mass ratio. Therefore, in this research, a variation of drop test parameters was carried out experimentally. Furthermore, numerical vibration analysis was applied to investigate the deformability of the impact surface. The results conclude that the mass ratio of 1:50 cannot be defined as a decisive criterion. In order to determine the influence of further drop test parameters, the research findings were used to validate a parametric model which assesses impact target deflection. An approximation quality of over 90 % was achieved. As a result, new evaluation criteria are proposed. Firstly, a method for identifying critical impact target designs is provided. Secondly, a new comprehensive formula compares the approximated maximum deflection of a real impact target to the respective theoretical threshold derived from a worst-case assumption. In practice, this leads to great advantages in the evaluation of already installed impact targets for dangerous goods packagings.
Titanium and its alloys are known to allow the straightforward laser-based manufacturing of ordered surface nanostructures, so-called high spatial frequency laser-induced periodic surface structures (HSFL). These structures exhibit sub-100 nm spatial periods – far below the optical diffraction limit. The resulting surface functionalities are usually enabled by both, topographic and chemical alterations of the nanostructured surfaces. For exploring these effects, multi-method characterizations were performed here for HSFL processed on Ti–6Al–4V alloy upon irradiation with near-infrared ps-laser pulses (1030 nm, ≈1 ps pulse duration, 1–400 kHz) under different laser scan processing conditions, i.e., by systematically varying the pulse repetition frequency and the number of laser irradiation passes. The sample characterization involved morphological and topographical investigations by scanning electron microscopy (SEM), atomic force microscopy (AFM), tactile stylus profilometry, as well as near-surface chemical analyses hard X-ray photoelectron spectroscopy (HAXPES) and depth-profiling time-of-flight secondary ion mass spectrometry (ToF-SIMS). This provides a quantification of the laser ablation depth, the geometrical HSFL characteristics and enables new insights into the depth extent and the nature of the non-ablative laser-induced near-surface oxidation accompanying these nanostructures. This allows to answer the questions how the processing of HSFL can be industrially scaled up, and whether the latter is limited by heat-accumulation effects.
Proper predictions of the behaviour of shock absorber materials are of utmost importance in safety assessments for licensing casks for transport and storage of highly active waste. After having identified significant discrepancies between numerical results and the actual response of polyurethane foam limiters subjected to accidental scenarios, a new research project ENREA was established by BAM. A major objective is to enhance and to develop advanced material models intended to simulate limiters under impact loading. They should account for all major factors influencing the load–deformation relationship like temperature, strain rate and specific stress state. The corresponding test program, applicable plasticity models, the overall parameter identification strategy based on local and global optimization techniques as well as experimental and numerical results are presented here in particular for closed cell foams.
BAM is the responsible authority in Germany for the assessment of the mechanical and thermal design safety of packages for the transport of radioactive materials. The assessment has to cover the proof of brittle fracture safety for package components made of potentially brittle materials. This paper gives a survey of the regulatory and technical requirements for such an assessment according to BAM's new 'Guidelines for the application of ductile cast iron for transport and storage casks for radioactive materials'. Based on these guidelines, higher stresses than before will be permissible, but it is necessary to put more effort into the safety assessment procedure. The fundamentals of such a proof using the methods of fracture mechanics are presented. The recommended procedure takes into account the guidelines of the IAEA's advisory material which are based on the prevention of crack initiation. Examples of BAM's research and safety assessment practices are given. Recommendations for further developments towards package designs with higher acceptable stress levels will conclude the paper.