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Aufbereitungsuntersuchungen an schwermetallbelastetem Baggergut aus dem ältesten Kanal Deutschlands
(2000)
Das Basisanliegen - Einleitung
Mit der zunehmenden Zahl akkreditierter ZfP-Firmen und zunehmender Anwendung risikobasierender Konzepte ergibt sich die Notwendigkeit, internationale Standards wie die DIN EN ISO 17025 und darüber hinausgehende Richtlinien bei der Verfahrensauswahl in der ZfP zu berücksichtigen. Dieser Aufsatz soll aufzeigen, welche internationalen Aktivitäten gegenwärtig für die Zuverlässigkeitsbetrachtungen von Bedeutung sind (siehe auch [1]). In Übereinstimmung mit den Vereinbarungen und Definitionen der European-American Workshops zur Zuverlässigkeit [2, 3] gilt: Das Basisanliegen der Zuverlässigkeitsuntersuchungen beliebiger diagnostischer Systeme besteht darin, den Grad festzustellen mit dem das Prüfsystem in der Lage ist, seinen vorgesehenen Zweck zu erfüllen. Im Falle der ZfP besteht dieser Zweck zumeist in der Aufgabe, Bauteildefekte aufzufinden und zu beschreiben bzw. die Defektfreiheit von Bauteilen zu bestätigen, sowie Wanddicken zu messen oder Material zu charakterisieren.
Das Basisanliegen der Zuverlässigkeitsuntersuchungen findet seinen Niederschlag bei folgenden international relevanten Aktivitäten:
neue ISO 17025 als Notwendigkeit mit variablen Möglichkeiten der Verfahrensvalidierung
als Kettenglied in RBLM (Risk Based Life Time Management) (r) EPERC-Initiative
CEN/TC138/WG9 "Qualifizierung von ZfP-Verfahren"
Six-Sigma Strategie: als notwendiger Bestandteil
ASNT-Initiative: Standing Committee on NDE Reliability: als Arbeitspaket
Produkthaftung: als notwendige Voraussetzung für die Handhabung
Turbine components from conventionally cast nickel-base alloy René 80 show different hot cracking susceptibilities depending on their heat treatment conditions leading to slightly different microstructures. Electron probe micro-analysis, focused ion beam technique and analytical transmission electron microscopy were applied to reveal and identify grain boundary precipitates and the γγ'-microstructure. The distribution of borides along grain boundaries was evaluated statistically by quantitative metallography. The following features could be correlated with an increase of cracking susceptibility: i) Increasing grain size, ii) increasing fraction of grain boundaries with densely spaced borides, iii) lack of secondary γ'-particles in matrix channels between the coarse cuboidal γ'-precipitates. The latter feature seems to be responsible for linking-up of cracked grain boundary precipitates which occurred as an additional cracking mechanism after one heat treatment, whereas decohesion at the boride-matrix-interface in the heat affected zone of laser-drilled holes was observed for both heat treatments.
In a joint project of partners from industry and research, the automated recycling of construction and demolition waste (CDW) is investigated and tested by combing laser-induced breakdown spectroscopy (LIBS) and near-infrared (NIR) spectroscopy. Joint processing of information (data fusion) is expected to significantly improve the sorting quality of various materials like concrete, main masonry building materials, organic components, etc., and may enable the detection and separation of impurities such as SO3-cotaining building materials (gypsum, aerated concrete, etc.). The project focuses primarily on the Berlin site to analyze the entire value chain, minimize economic/technological barriers and obstacles at the cluster level, and sustainably increase recovery and recycling rates. First measurements with LIBS and NIR spectroscopy show promising results in distinguishing various material types and indicate the potential for a successful combination. In addition, X-ray fluorescence (XRF) spectroscopy is being performed to obtain more information about the quantitative elemental composition of the different building materials. Future work will apply the developed sorting methodology in a fully automated measurement setup with CDW on a conveyor belt.
The OECD test guidelines (TGs) for testing chemicals have been widely used for regulatory purposes all over the world since the establishment of the Mutual Acceptance of Data (MAD) principle in 1984. This MAD principle ensures that, if a chemical is tested under the Good Laboratory Practice (GLP) conditions accordingly to an OECD TG, the data should be accepted in all OECD countries. The TGs have been developed, harmonized, internationally validated (round robin tests) and adopted by OECD countries to be used for the physical-chemical characterisation, fate estimation, and hazard identification for risk assessment of various chemicals. In addition to the TGs, OECD Guidance Documents (GDs) usually provide guidance on how to use TGs and how to interpret the results. These GDs do not have to be fully experimentally validated, and hence they are not under MAD, but they are based on relevant published scientific research.
But are the existing TGs and the related GDs applicable and adequate for the regulatory testing of nanomaterials? In general, for nanomaterials it is accepted that most of the "endpoints" or more precisely measurement variables are applicable. However, for some endpoints new or amended TGs are needed. In addition, several GDs are needed to give more precise advice on the test performance in order to gain regulatory relevant data on nanomaterials.
The site of Schöningen (Germany), dated to ca. 300,000 years ago, yielded the earliest large-scale record of humanly-made wooden tools. These include wooden spears and shorter double-pointed sticks, discovered in association with herbivores that were hunted and butchered along a lakeshore. Wooden tools have not been systematically analysed to the same standard as other Palaeolithic technologies, such as lithic or bone tools. Our multianalytical study includes micro-CT scanning, 3-dimensional microscopy, and Fourier transform infrared spectroscopy, supporting a systematic technological and taphonomic analysis, thus setting a new standard for wooden tool analysis. In illustrating the biography of one of Schöningen’s double-pointed sticks, we demonstrate new human behaviours for this time period, including sophisticated woodworking techniques. The hominins selected a spruce branch which they then debarked and shaped into an aerodynamic and ergonomic tool. They likely seasoned the wood to avoid cracking and warping. After a long period of use, it was probably lost while hunting, and was then rapidly buried in mud. Taphonomic alterations include damage from trampling, fungal attack, root damage and compression. Through our detailed analysis we show that Middle Pleistocene humans had a rich awareness of raw material properties, and possessed sophisticated woodworking skills. Alongside new detailed morphometrics of the object, an ethnographic review supports a primary function as a throwing stick for hunting, indicating potential hunting strategies and social contexts including for communal hunts involving children. The Schöningen throwing sticks may have been used to strategically disadvantage larger ungulates, potentially from distances of up to 30 metres. They also demonstrate that the hominins were technologically capable of capturing smaller fast prey and avian fauna, a behaviour evidenced at contemporaneous Middle Pleistocene archaeological sites.