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Composite pressure vessels are commonly manufactured using the wet filament winding process, where various process parameters can influence the performance of the finished component. In this study two designs of wet filament wound 6.8-liter type 4 composite pressure vessels were manufactured. Both differ only by the internal pressure used during the filament winding, which primarily influences the residual stress state in the composite structure. An extensive experimental study was carried out, including 10 slow burst tests and strain measurements with fiber optic sensors. Significant differences can be observed in the performance of the two designs even though the used stacking sequence, materials and other manufacturing parameters are the same for both designs. A discussion of the differences in the behavior of both cylinder types is provided, including the strain distribution in slow burst tests and failure mechanism.
The publication is an extended abstract on the modelling of the manufacturing process related residual stresses in type 4 pressure vessels for hydrogen storage. A 2D analytical model based on the classical laminate theory and a 3D finite element model are introduced. The calculated residual stress state after the filament winding process as well as the stress state in service are presented and discussed.
The number of in-operation composite pressure vessels is increasing, partly due to their attractiveness for on-board compressed gas storage and transport applications. A possible way to maintain the highest safety levels is through the structural health monitoring of the composite cylinders. Here, the use of fiber optic sensors appears to be a promising approach. However, the integration of the optical fibers into the composite structure of a pressure vessel has been shown to be challenging. In this study, insights on the embedding of optical fibers in the composite structure under industrial conditions are provided. A protection concept for the ingress and egress of the optical fibers is presented. Finally, the results from destructive slow burst tests are evaluated, showing no clear trend in the impact of the embedded optical fibers on the performance of composite pressure vessels.
Hydrogen storage is a crucial part of the hydrogen value chain, particularly in terms of safety and social acceptance of hydrogen technologies. For on-board and transportation applications, hydrogen is commonly stored as a compressed gas in pressure vessels. Full composite wrapped Type 4 pressure vessels are especially beneficial due to their high weight-saving potential and their capability to withstand high working pressures. To maintain an appropriate safety level, the mechanical behavior of the composite structure has been the subject of investigation in numerous studies. In this study, the failure mechanisms of two designs of Type 4 cylinders are investigated. The two designs differ solely in the manufacturing process parameters, particularly the internal pressure applied during the filament winding process. Variations in internal pressure result in different residual stress states and changes in the quality of the composite structure. The stacking sequence, materials used, and other manufacturing parameters remain unchanged. The cylinders show different failure mechanisms in slow burst tests: one design fails in hoop windings, while the other one fails in helical windings, despite no stress exaggeration in the fiber direction being observed with embedded optical fibers or in numerical simulations. To explain the failure mechanisms, the quality of the cylinders is investigated. The results of X-ray computed tomography and pulse-echo investigation, highlight the complexity of the interactions between manufacturing process parameters, residual stresses, manufacturing quality, and the mechanical behavior of composite pressure vessels. Resin-rich areas in the composite material are identified as a possible cause of the differing failure mechanisms.
Hole-drilling method is a standardized technique for obtaining residual stresses in isotropic structures. Previous studies provide a foundation that enables the use of this method to investigate orthotropic structures, such as fiber-reinforced composites. In this study, the incremental hole-drilling method was applied to investigate residual stresses in filament wound type 4 composite pressure vessels. The investigated composite cylinders were manufactured with different internal pressure functions during the winding process, to achieve distinct residual stress states. Additionally, the influence of the initial loading under sustained internal pressure and increased temperature on the stress distribution was investigated. It was shown that the residual stress state can be influenced by varying the internal pressure in the winding process. After testing at sustained load and increased temperature, a stress redistribution was observed, which took place due to creep phenomena. Finally, a discussion of the challenges for the application of the hole-drilling method to composite pressure vessels is provided.
The number of applications that demand zero-emission energy carriers, such as liquified hydrogen (LH2), is increasing worldwide. LH2 is typically transported or stored under cryogenic conditions. Storage in such conditions requires super thermal insulations which maintain very low boil-off for a prolonged time. Multi-Layer insulation (MLI) finds widespread use in cryogenic applications, designed to effectively restrict heat inleak towards cryogenic fluids. However, recent studies evidenced that exposure to high heat fluxes, such as in the event of a fire accident, can cause the thermal degradation of the insulation material, resulting in the severe collapse of its heat resistance performance. Therefore, the risk of rapid tank pressurization and its connection to the risk of BLEVE may be possible. This study proposes a numerical model to assess the performances of aluminum-based MLI materials under fire conditions. The model offers insights into the total heat transfer rate through the insulation, serving as a
Hydrogen is recognized as a keystone of the global energy transition, offering a clean, high-energy-density energy carrier ideal for storage and transportation. Among various storage options, liquid hydrogen (LH2) is especially advantageous for both mobile and stationary applications. However, ensuring the safety and performance of LH2 storage systems under extreme thermal conditions, such as fire exposure, remains an engineering challenge.
This study introduces an experimental framework, called the Cryogenic High-Temperature Thermal Vacuum Chamber (CHTTVC), designed to investigate the thermal-hydraulic response of vacuum-insulated cryogenic tanks under fire-like conditions. The apparatus enables evaluation of insulation performance, such as perlite and multilayer insulation (MLI), with a focus on thermal degradation, heat ingress, and vacuum stability.
Results indicate that combustible MLIs undergo substantial thermal degradation, leading to heat ingress rates of up to 6.5 kW and the formation of hazardous combustion by-products. In contrast, non-combustible MLIs and bulk insulation materials restrict heat ingress to approximately 3 kW while more effectively preserving vacuum integrity. Combustible MLIs also exhibit pronounced pressure increases in the evacuated section, reaching ∼6 × 104 Pa, nearly six times higher than those observed for non-combustible counterparts. Analysis of effective emissivity further reveals an enhancement in radiative heat transfer, approximately five times, for combustible MLIs following degradation. Additionally, marked thermal stratification develops under both nominal and extreme heat loads, with temperature gradients approaching 10 °C per 100 mm during sustained thermal exposure.
Study the impact of spacer at thermal degradation process of MLI-based insulation in fire condition
(2024)
To reduce CO2 emissions, energy carriers such as hydrogen are considered to be a solution. Consumption of hydrogen as a fuel meets several limitations such as its low volumetric energy density in gas phase. To tackle this problem, storage as well as transportation in liquified phase is recommended. To be able to handle this component in liquid phase, an efficient thermal insulation e.g., MLI insulation is required. Different studies have been addressed the vulnerability of such insulation against high thermal loads e.g., in an accident engaging fire. Some of research works have highlighted the importance of considering the MLI thermal degradation focusing on its reflective layer. However, limited number of studies addressed the thermal degradation of spacer material and its effect on the overall heat flux.
In this study, through systematic experimental measurements, the effect of thermal loads on glass fleece, glass paper as well as polyester spacers are investigated. The results are reported in various temperature and heat flux profiles. Interpreting the temperature profiles revealed that, as the number of spacers in the medium increases, the peak temperature detectable by the temperature sensor on the measurement plate decreases. Each individual spacer contributes to mitigating the radiative energy received by the measurement plate. Stacks of 20–50 spacers (this is the number of layers in commercial MLI systems applied for liquid hydrogen applications) can potentially reduce the thermal radiation by 1–2 orders of magnitude.
An empirical correlation to predict a heat flux attenuation factor is proposed, which is useful for further numerical and analytical studies in the temperature range from ambient to 300 ◦C.
A Comprehensive Numerical Study of the Behaviour of an LH2 Storage Tank in the Event of a Fire
(2025)
As the world moves towards green energy production, effective storage and transportation solutions become essential. To support this transition, energy carriers with minimal or zero environmental impact are required. Liquified hydrogen represents a promising candidate due to its emissions-neutral properties. However, its highly flammable nature necessitates adherence to strict safety codes and standards. Storing hydrogen often requires advanced super-insulation materials. To enhance the safety of cryogenic hydrogen storage tanks under extreme conditions, such as those encountered during fire accidents, it is crucial to understand the thermal behaviour of the tank. Predicting pressurization and potential failure in advance demands a robust and comprehensive model. However, still such models suffer lack of detailed heat transfer models which account for various sub-processes during an accident scenario. Hence, this study introduces a comprehensive model for the pressurization of cryogenic tanks equipped with multi-layer insulation (MLI) systemsin the event of fire, which comprises several sub-models. These sub-models account for heat transfer phenomena through the thermal insulation at nominal conditions and its thermal degradation during fire exposure, the fluid, the internal pressurization, and the performance of the pressure relief valve. This study provides valuable insights into the safety and the behaviour of hydrogen storage tanks under thermal loads.
For decarbonizing the energy industry and transport, cryogenic energy carriers have great potential. The storage takes place in tanks with thermal super-insulations, which are in application for decades, but there is only limited knowledge about its behaviour in a fire scenario. This represents a major incident that may generate extraordinary loads on the tank and its insulation system, and that eventually lead to a sudden tank failure. This paper presents a test rig called the Cryogenic High Temperature Thermal Vacuum Chamber (CHTTVC), which can be used to test typical thermal superinsulation’s under cryogenic and fire-like conditions in parallel. The test method makes it possible to measure the heat flow through the thermal superinsulation over time and to investigate the degradation behaviour of the insulation within a test. In the paper results from the first tests are presented.
