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Concrete is the most applied building material in modern times. It is present in all kinds of structures and no other material secms to rcplace concrete as the most selected building material in the near future. The prime advantages are the high performance, the easy production and a facile processability. The sustainability and durability are important requirements to concrete. Even if concrete is significantly less susceptible against factors promoting a damage, compared to other materials, there are still mechanisms affecting it. In particular, high-ways and hydraulic structures made of concrete worldwide show cases of alkali-silica reaction (ASR) damages. This article refers to experience at BAM Federal InstituteforMaterials Research and Testing for several decades to ASR research and darnage assessment. ASR is a severe darnage mechanism that can occur in concrete, when certain conditions related to composition and cxposition arise in a critical combination. The chemical reaction is based on the alkalis and the silica in the concrete and was first identified by Stanton in highway structures in California (Stanton, 1940). Actually three components are needed to initiate ASR: alkali-sensitive siliceous aggregates, alkalis coming from internal (cement or other components) or external sources (de-icing salt or sea water) and water. If all of these components are sufficiently present an alkali-silica gel could be formed (Hobbs, 1988). This gel itself needs additional space when it is formed. Furthermore it is able to swell in the presence of humidity, both processes generating an expansion pressure inside the concrete. As a consequence of intensive expansion, cracks can occur, which significantly lowers thc strength of the material. Parameters like amount and chemical composition of the gel as weil as the pattern and width of cracks can help to classify the ASR darnage (Swamy, 1992). The objective of this article is to demoostrate the microscopic work on ASR affected concrete samples, carried out to assess the damaging process or to evaluate various alkali-sensitive aggregates. It will explain the approach of ASR investigation from the macroscale to microscale, starting briefly with the condition assessment, over treatment and investigations of samples in the laboratory, to the use of different microscopical and analytical techniques. In the main part the characteristic features for identifying ASR in concrete are presented by using microscopic images. Especially the emphasis lies on the role of the aggregate.
This study examines the relationship between the magnetic mesostructure with the microstructure of low carbon steel tungsten inert gas welds. Optical microscopy revealed variation in the microstructure of the parent material, in the heat affected and fusion zones, correlating with distinctive changes in the local magnetic stray fields measured with high spatial resolution giant magneto resistance sensors. In the vicinity of the heat affected zone high residual stresses were found using neutron diffraction.
Notably, the gradients of von Mises stress and triaxial magnetic stray field modulus follow the same tendency transverse to the weld. In contrast, micro-X-ray fluorescence characterization indicated that local changes in element composition had no independent effect on magnetic stray fields.
The susceptibility of different aggregate types used in concrete to ASR is strongly associated with their petrography. The aim of this study is to assess the influence of the aggregate size on the ASR potential, in particular applied to the sand fractions in the size range of 0.125-4 mm. The investigation concept is based on the hypothesis that at a specific particle size reactive aggregates could change their characteristic influence in mitigating ASR instead of promoting it. For the study of the size dependent behaviour mortars are prepared, considering aggregates of different reactivity, including very reactive, slow-late and quasi non-reactive types. The analysis is based on a stepwise substitution concept, in which mortars with a constant overall grain size distribution are compared, while only one size fraction of the non-reactive base aggregate is substituted by a reactive aggregate type of this specific size fraction. For the expansion experiments an accelerated mortar bar test (80°C, immersed in NaOH solution) was applied. The results show that the slow-late reactive greywacke yielded a strong reduction of the expansion below an aggregate size in the range of 0.5-1 mm. On the other side with the very reactive borosilicate glass, the expansions increased steadily with decreasing size. To validate if the acquired expansions were caused by ASR, thin sections were analysed. Mainly, higher expansion values were consistent with extensively more amounts of ASR indicators.
We present a comparative study of the spectroscopic properties of the donor–acceptor–donor substituted dyes triphenylamine-allylidenemalononitrile-julolidine (TMJ) and triphenylamine-allylidenemalononitriletriphenylamine (TMT), bearing one and two propeller-like triphenylamine donor moieties, in solvents of varying polarity and viscosity and in the aggregated and solid state. Our results reveal control of the aggregation-induced spectroscopic changes and the packing motifs of the dye molecules in the solid state by the chemical nature and structure of the second nitrogen-containing donor, i.e., a planar and a rigid julolidine or a twisted triphenyl group. Assuming that the TMT and TMJ aggregates show a comparable arrangement of the molecules to the respective crystals, these different molecular interactions in the solid state are responsible for aggregation induced emission (AIE) in the case of TMT and its absence for TMJ. Moreover, a versatile strategy for the fluorescence enhancement of only weakly emissive AIE dyes is shown, turning these dyes into bright nanoscale fluorescent reporters by using them as stains for preformed polymer particles.
This is a corrigendum to the original article "Determining the thickness and completeness of the shell of polymer core-shell nanoparticles by X-ray photoelectron spectroscopy, secondary ion mass spectrometry, and transmission scanning electron microscopy" that was published in "The journal of physical chemistry C", vol. 123 (2019), no. 49 pp. 29765-29775.
High quality tubular products are essential to the oil and gas industry. Quality control during their production focuses on the non-destructive detection of surface defects. The structured light technique is a candidate for the challenge to detect, monitor and evaluate such defects in real-time.
In the present study the automatic processing of structured light measurements is performed and validated. The algorithm for the automatic Analysis of inspection data has an advantage over current data evaluation methods based on individual assessments of operators.