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Towards the standardization of biochar analysis: the COST action TD1107 interlaboratory comparison
(2016)
Biochar produced by pyrolysis of organic residues is increasingly used for soil amendment and many other applications. However, analytical methods for its physical and chemical characterization are yet far from being specifically adapted, optimized, and standardized. Therefore, COST Action TD1107 conducted an interlaboratory comparison in which 22 laboratories from 12 countries analyzed three different types of biochar for 38 physical–chemical parameters (macro- and microelements, heavy metals, polycyclic aromatic hydrocarbons, pH, electrical conductivity, and specific surface area) with their preferential methods. The data were evaluated in detail using professional interlaboratory testing software. Whereas intralaboratory repeatability was generally good or at least acceptable, interlaboratory reproducibility was mostly not (20% < mean reproducibility standard deviation < 460%). This paper contributes to better comparability of biochar data published already and provides recommendations to improve and harmonize specific methods for biochar analysis in the future.
The principle of a low-cost but nevertheless powerful POF elongation sensor has already been described in the recent years [1, 2, 3]. The measurement of the phase shift of a signal of a modulated light source which is coupled into two different POF, one being stretched, yields information of the elongation with a resolution of up to 10-5. Analyzing the temporal or frequency behaviour of the signal gives additional information. Since the phase measurement can allow for frequencies up to 2 GHz, the vibrational analysis of macroscopic structures can be extended to several kHz very easily, limited mainly by the signal processing electronics. Thus we processed data of a sensing system applied to a 39 m rotor blade of a wind power generator and could resolve the various frequencies related to different exciting conditions, e.g. the appearance of a beat signal when the blade was externally excited by a mechanical system with a frequency close but not identical to the Eigen frequency of the blade.