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The paper deals with the integration of a light emitting diode (LED) into an additive manufactured metal component. Selective laser melting (SLM) and laser metal deposition (LMD) are used. The material used is the chrome-nickel steel 316L. The basic component is manufactured by means of SLM and consists of a solid body and an area with grid structure. The solid body includes a duct in the shape of a groove with a recess for the positioning of the power cable. The LED is embedded in the grid structure via an inlet from the solid body. In further processing, the groove is filled with LMD. Two strategies with different parameter combinations were investigated. It shows that a high energy input near the power cable leads to its destruction. By using multiple parameter combinations during the manufacturing process, this destruction can be prevented. There was a comparison of both strategies with regard to the necessary number of tracks and duration of welding time.
Pores in additive manufactured metal parts occur due to different reasons and affect the part Quality negatively. Few investigations on the origins of porosity are available, especially for Ni-based super alloys. This paper presents a new study to examine the influence of common processing Parameters on the Formation of pores in parts built by laser metal Deposition using Inconel 718 powder. Further, a comparison between the computed tomography (CT) and the Archimedes method was made. The Investigation Shows that CT is able to identify different kinds of pores and to give further Information about their distribution. The identification of some pores as well as their shape can be dependent on the Parameter Setting of the Analysis tool. Due to limited measurement Resolution, CT is not able to identify correctly pores with Diameters smaller than 0.1 mm, which leads to a false decrease on Overall porosity. The applied Archimedes method is unable to differentiate between gas porosity and other Kinds of holes like internal cracks or lack of Fusion, but it delivered a proper value for Overall porosity. The method was able to provide suitable data for the statistical Evaluation with design of Experiments, which revealed significant Parameters ont he Formation of pores in LMD.
Laser-Metal-Deposition (LMD) and Plasma-Transferred-Arc (PTA) are well known Technologies which can be used for cladding purposes. The prime objective in combining LMD and PTA as a Hybrid Metal Deposition-Technology (HMD) is to achieve high Deposition rates at low thermal Impact. Possible applications are coatings for wear protection or repair welding for components made of steel. The two energy sources (laser and Plasma arc) build a Joint process Zone and are configurated to constitute a stable process at laser powers between 0.4-1 kW (defocused) and Plasma currents between 75-200 A. Stainless steel 316L serves as filler material. For this HMD process, a Plasma Cu-nozzle is designed and produced by powder bed based Selective Laser Melting. The potential of the HMD Technology is investigated and discussed considering existing process. This paper demonstrates how the interaction of the two energy sources effects the following application-relevant properties: Deposition rate, powder Efficiency and energy Input.
Additive manufacturing is no longer just used for the production of prototypes but already found its way into the industrial production. However, the fabrication of massive metallic parts with high geometrical complexity is still too time-consuming to be economically viable. The combination of the powder bed-based selective laser melting process (SLM), known for its geometrical freedom and accuracy, and the nozzle-based laser metal deposition process (LMD), known for its high build-up rates, has great potential to reduce the process duration. For the industrial application of the SLM-LMD hybrid process chain it is necessary to investigate the interaction of the processes and its effect on the material properties to guarantee part quality and prevent component failure. Therefore, hybrid components are manufactured and examined before and after the heat treatment regarding the microstructure and the hardness in the SLM-LMD transition zone. The experiments are conducted using the nickel-based alloy Inconel 718.
Plasma-Transferred-Arc (PTA) welding is a process that enables high deposition rates, but also causes increased thermal load on the component. Laser metal deposition (LMD) welding, on the other hand, reaches a high level of precision and thus achieves comparatively low deposition rates, which can lead to high processing costs. Combining laser and arc energy aims to exploit the respective advantages of both technologies. In this study, a novel approach of this process combination is presented using a PTA system and a 2 kW disk laser. The energy sources are combined in a common process zone as a high-speed plasma laser cladding technology (HPLC), which achieves process speeds of 10 m/min at deposition rates of 6.6 kg/h and an energy per unit length of 39 J/mm.
Resistance spot welding (RSW) is widely used in the automotive industry
as the main joining method. Generally, an automotive body contains
around 2000 to 5000 spot welds. Therefore, it is of decisive importance to characterize the mechanical properties of these areas for the further optimization and improvement of an automotive body structure. The present paper aims to introduce a novel method to investigate the mechanical properties and microstructure of the resistance spot weldment of DP1000 sheet steel. In this method, the microstructure of RSW of two sheets was reproduced on one sheet and on a bigger area by changing of the welding parameters, e. g. welding current, welding time, electrode force and type. Then, tensile tests in combination with digital Image correlation (DIC) measurement were performed on the notched tensile specimens to determine the mechanical properties of the weld metal.
The notch must be made on the welded tensile specimen to force the fracture and elongation on the weld metal, enabling the characterization of its properties. Additionally, the parameters of a nonlinear isotropic material model can be obtained and verified by the simulation of the tensile specimens. The parameters obtained show that the strength of DP1000 steel and the velocity of dislocations for reaching the Maximum value of strain hardening, are significantly increased after RSW. The effect of sample geometry and microstructural inhomogeneity of the welded joint on the constitutive property of the weld metal are presented and discussed.
Self-assembled monolayers of aromatic omega-aminothiols on gold: surface chemistry and reactivity
(2010)
Amino-terminated self-assembled monolayers on gold substrates were studied by X-ray photoelectron spectroscopy (XPS), near-edge X-ray absorption fine structure (NEXAFS) measurements, and atomic force microscopy (AFM). Two different ω-amino-4,4'-terphenyl substituted alkanethiols of the general structure H2N-(C6H4)3-(CH2)n-SH (ATPn) were used: 2-(4''-amino-1,1':4',1''-terphenyl-4-yl)ethane-1-thiol (n = 2, ATP2) and 3-(4''-amino-1,1':4',1''-terphenyl-4-yl)propane-1-thiol (n = 3, ATP3). Moreover, the addressability of amino groups within the films was investigated by chemical derivatization of ATPn SAMs with 3,5-bis(trifluoromethyl)phenyl isothiocyanate (ITC) forming fluorinated thiourea ATPn-F films. Evaluation of high-resolution C 1s and N 1s XPS data revealed successful derivatization of at least 50% of surface amino species. Furthermore, it could be demonstrated by angle-resolved NEXAFS spectroscopy that chemical derivatization with ITC has no noticeable influence on the preferential upright orientation of the molecules in the SAMs.