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Organisationseinheit der BAM
Eingeladener Vortrag
- nein (1)
Functionalised surfaces are of interest in many fields, e.g. in biomedicine, materials science and molecular electronics. In this study a series of self-assembled aliphatic and aromatic monolayers on gold substrates with terminal amino groups was investigated. Four different thiol molecules were used: aliphatic 11-aminoundecane-1-thiol (AUDT), aromatic 4-aminobenzenethiol (ABT) and aromatic ω-amino thiols with an alkyl spacer as 4-aminophenylbutane-1-thiol (APBT) and 3-(4''-amino-1,1':4',1''-terphenyl-4-yl)propane-1-thiol (ATPT). Evaluation of N 1s XPS data revealed that on the aromatic self-assembled monolayers (SAMs) amino groups exist preferentially as primary amines, whereas on the aliphatic SAM protonated and/or hydrogen-bonded amines are the major species. This result is crosschecked by N K edge near edge X-ray absorption fine structure (NEXAFS) spectroscopy and can be rationalised by the different basicity of aliphatic and aromatic amines.
Build-up strategies for generating components of cylindrical shape with laser metal deposition
(2015)
Laser Metal Deposition LMD) as additive manufacturing process offers the potential to produce near net shape components. This reduces the amount of material and post-processing. The components are composed of individual layers. Already mall irregularities within a layer can add up over multiple layers and lead to error propagation. This paper deals with the issue of build-up strategies to minimize irregularities and prevent error propagation. Different travel paths and the influence of a changing starting point regarding to error propagation are discussed. Different deposition rates between core and peripheral area are detected and successfully compensated by adjusting the build-up sequence. Stainless steel and titanium alloy Ti-6Al-4V are used in the experiments. The results are intended to illustrate the potential of an adjusted build-up strategy and provide basic information on the way to an automated deposition process. This paper is of interest for engineers in industry or science using LMD as additive manufacturing process.
Maintenance, repair and overhaul of components are of increasing interest for parts of high complexity and expensive manufacturing costs. In this paper a production process for laser metal deposition is presented, and used to repair a gas turbine burner of Inconel 718. Different parameters for defined track geometries were determined to attain a near net shape deposition with consistent build-up rate for changing wall thicknesses over the manufacturing process. Spot diameter, powder feed rate, welding velocity and laser power were changed as main parameters for a different track size. An optimal overlap rate for a constant layer height was used to calculate the best track size for a fitting layer width similar to the part dimension. Deviations in width and height over the whole build-up process were detected and customized build-up strategies for the 3D sequences were designed. The results show the possibility of a near net shape repair by using different track geometries with laser metal deposition.
The industrial demand for flexible and innovative manufacturing technologies is continuously increasing. These technologies have to be sustainable and resource-efficient, and have to allow the production of long-life capital goods. Consequently, the additive processes gain in importance as they offer an enormous potential of application, especially for the turbomachinery industry.
In order to use additive manufacturing technologies in industrial applications, it is necessary to consider the complete process chain, including all necessary pre- and postprocessing. Although additive manufacturing is increasingly covered in scientific research, the linking between this technology and conventional industrial processes is rarely described.
Das Laser-Pulver-Auftragschweißen als additives Fertigungsverfahren ermöglicht einen endformnahen Aufbau von Bauteilen. Ein Zielkonflikt besteht zwischen der Forderung nach hoher Aufbaurate und hoher Endformnähe, welcher von der Schweißraupengröße wesentlich beeinflusst wird. In dieser Veröffentlichung wird das Laser-Pulver-Auftragschweißen eingesetzt, um komplexe Formen additiv aufzubauen. Am Beispiel eines Tannenbaumprofiles werden unterschiedliche Einflussfaktoren dargestellt. Dazu gehören die Raupengeometrie, die Überlappung einzelner Raupen, die Verwendung unterschiedlicher Aufbaustrategien und die Teilung des Gesamtkörpers in Teilkörper. Der Zielkonflikt wird durch die Herstellung von Probekörpern mit unterschiedlichen Steigungswinkeln an den Seitenflächen verdeutlicht. Die Ergebnisse zeigen eine verbesserte Endformnähe in Bereichen flacher Steigung beim Einsatz kleiner Schweißraupen. Im Vergleich dazu erlauben die Schweißparameter der großen Raupen eine 5-fach höhere Aufbaurate. Bei einer Raupenüberlappung kleiner und großer Raupengeometrien innerhalb einer Lage treten Anbindungsfehler auf. Strategien zur Behebung dieses Fehlers durch Anpassung der Schweißreihenfolge werden in dieser Veröffentlichung aufgezeigt. Diese Erfahrungen werden genutzt, um einen Gesamtkörper aus Teilkörpern unterschiedlicher Raupengeometrien zu fertigen.
Metal additive manufacturing is often based on laser beam processes like Laser Metal Fusion (LMF) or Laser Metal Deposition (LMD). The LMF process is in particular suitable for very complex geometries. However build rate, part volume and material flexibility are limited in LMF. In contrast, LMD achieves higher deposition rates, less restricted part sizes and the possibility to change the material composition during the build-up process. On the other hand, due to the lower spatial precision of the material deposition process, the complexity of geometries is limited. Therefore, combined manufacturing with both LMF and LMD has the potential to utilize the respective advantages of both technologies.
In this paper, combined additive manufacturing with LMF and LMD is described for Ti-6Al-4V and Inconel 718. First, lattice structures with different wall thickness and void sizes are built with LMF. The influence of LMD material deposition on these LMF-structures is examined regarding metallurgical impact and distortion. Cross-sections, x-ray computer tomography and 3D-scanning results are shown.
For the titanium alloy specimen, oxygen and Nitrogen content in the deposited material are analysed to evaluate the LMD shielding gas atmosphere. The results are used to develop guidelines for a LMD build-up strategy on LMF substrates. With these findings, a gas turbine burner is manufactured as reality test for the combined approach.
Laser beam processes are increasingly used in the field of additive manufacturing.
Prominent methods are either powderbed-based like Laser Metal Fusion (LMF), or utilizing a powder nozzle like Laser Metal Deposition (LMD). While LMF allows the manufacturing of complex structures, build rate, part volumes and material flexibility are limited. In contrast, LMD is able to operate with high deposition rates on existing parts, and materials can be changed easily during the process. However LMD shape complexity is limited. Utilizing their respective strengths, a combination of these two additive technologies has the potential to produce complex parts with high deposition rates and increased material flexibility. In this paper, combined manufacturing with additive technologies LMF and LMD is described. Its benefit for industry with emphasis on turbomachinery is shown. As reality test for the innovation, an industrial turbine blade is manufactured.
Der Einsatz von Hochleistungswerkstoffen verlangt nach einer hohen Endformnähe der zu fertigenden Bauteile, um den Aufwand und somit die Kosten für Materialeinsatz und Nachbearbeitung möglichst gering zu halten. Der additive Einsatz in Form des Laser-Pulver-Auftragschweißens bietet hierfür durch den gezielten Materialauftrag ein hohes Potential. Herausforderungen bestehen in Bereichen der Vorhersagbarkeit und der Reproduzierbarkeit des Materialauftrages, sowie der Fertigungszeit. Unterschiedliche Einflüsse bei der Schichterzeugung führen dabei zu Abweichungen von der Soll-Geometrie. Die vorliegenden Untersuchungen behandeln den Einfluss von Spurgeometrie, Spurüberlappung, Verfahrweg und Aufbaureihenfolge auf die entstehende Bauteilform. Die Teilung einer Lage in Rand- und Kernbereich ermöglicht einen konturangepassten Verfahrweg und eine Erhöhung der Endformnähe innerhalb einer Ebene. Die Verwendung unterschiedlicher Spurgrößen bei der Bauteilerzeugung verdeutlicht die Möglichkeiten einer hohen Auftragsrate bei gleichzeitig hoher Formgenauigkeit. Bereits kleine Unterschiede beim Materialauftrag zwischen Kern- und Randbereichen, Start- und Endpunkten sowie in Bereichen des Richtungswechsels führen aufgrund von Fehlerfortpflanzung nachmehreren Lagen zu Abweichungen in der Aufbaurichtung. Kompensierungen mittels angepasster Baustrategien werden aufgezeigt und diskutiert. Die Nickelbasislegierung Inconel 718, die Titanlegierung Ti-6Al-4V sowie der austenitische Stahl 316L sind Bestandteil der vorliegenden Untersuchungen. Die gewonnenen Erkenntnisse verdeutlichen das Potenzial einer angepassten Aufbaustrategie zur reproduzierbaren Erzeugung von Bauteilen am Beispiel unterschiedlicher Körpergeometrien.
The process of laser metal deposition can be applied in many ways. Mostly, it is relevant to coating, for repair welding and for additive manufacturing. To increase the effectiveness and the productiveness, a good process understanding is necessary. Statistical test planning is effectual and often used for this purpose. For financial and temporal reasons, a restriction of the test space is reasonable. In this case, it is recommended to use a D-optimal experimental design which is practically applied to extend existing test plans or if process Limits are known. This paper investigates the applicability of a D-optimum experimental design for the laser metal deposition. The results are compared to the current results of a full factorial test plan.
Known restrictions are used for the limitation of the test space. Ti6Al4 is utilized as Substrate material and powder. Comparable results of the D-optimal experimental design and of the full factorial test plan can be demonstrated. However, 80 % of time can be saved by the experimental procedure. For this reason, the application of D-optimal experimental design for laser metal deposition is recommend.
Laser metal deposition is described with its applications for additive manufacturing. The necessary process chain is discussed, with regard to weld bead dimensions and 3D build-up strategy. Metallurgical cross sections, x-ray and tensile tests are conducted. As demonstrative components, a gas turbine burner and a turbine blade are shown