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Referierte Publikation
- nein (122) (entfernen)
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Organisationseinheit der BAM
Eingeladener Vortrag
- nein (48)
The friction and wear properties of polyetherimide composites under dry oscillating sliding condition at room temperature (RT) as well as at elevated temperature (120 °C) was investigated. The polymer specimens were made to oscillate against steel cylinder as a counterpart. The friction and wear properties of PEI and composites were strongly influenced by the temperature. In case of carbon fiber composite abrasive action of carbon fibers has severely damaged the counterpart and resulted in accelerated wear of the composite at RT. Solid lubricants filled (PTFE, MoS2, graphite) along with glass fiber is beneficial in improving the friction and wear performance of the PEI composite at RT, whereas at elevated temperature wear performance was deteriorated.
Performance and efficiency of piezo-electric stick-slip actuators are dependent on the waveform of the electrical actuation of the piezo-stack. This paper compares between a conventional saw-tooth actuation with two waveforms that feature softer acceleration in order to minimize the duration of the slip-phase. It is shown that the proposed waveforms increase both maximum mechanical output power (by 43%) and overall efficiency (by 25%) of the examined actuator.
Untersucht wurden Verschleißpartikel als elektronentransparente Proben auf dünnen Trägerfolien mit einem hochauflösendem Rasterelektronenmikroskop und energiedispersiver Röntgenspektrometrie im Transmissionsmodus.
Die hohe laterale Auflösung dieser modernen Methoden ermöglicht eine morphologische Charakterisierung der Verschleißpartikel bis in den nm-Bereich. Die hochauflösende Elementanalyse erlaubt eine Interpretation der Zusammensetzung und damit Rückschlüsse auf die Verschleißpartikelbildung. Die tribologischen Untersuchungen sind an einem Modell-Verschleißtribometer nach DIN 51834-2 geschmiert, aber ohne Ölkreislauf, durchgeführt worden. Die Präparation der Verschleißpartikel über eine Entnahme und Übertragung einer geringen Schmierstoffmenge mit einer Mikropipette auf eine TEM-Trägerfolie ist mit einem geringen Aufwand möglich. Der präparative Aufwand ist relativ gering. Das benötigte Schmierstoffvolumen beträgt wenige Mikroliter (0,001 ml).
Die Untersuchung zeigt die geringe geometrische Größe der Verschleißpartikel und bestätigt indirekt die These der Reaktionsschichtbildung mit einer geringen Schichtdicke, die ständig verschleißt und sich stetig neu bildet. Die beschriebenen Verschleißprozesse sind in der Modell-Verschleiß-Prüfung mit sehr hohen Pressungen am Versuchsbeginn nachweisbar.
The wear rates of self-mated alumina couples show that friction as well as wear is largely determined by the above-mentioned hydro-thermal conditions. The presence of water and its amount available in the surrounding system either in liquid or in gaseous form plays a key role for friction and wear behavior and can be beneficial for the tribological profile of steam degradation resistant materials. Hot steam enhances the tribo-chemical formations of oxides and hydroxides on MgO-ZrO2 alumina and antimony impregnated carbon.
The accurate EDS microanalysis of light elements such as boron and carbon by spectrum imaging will be demonstrated using a sintered hard ceramic material composed of the three major phases titanium boride (TiB2), titanium carbide (TiC), silicon carbide (SiC) and minor phases, sub-μm in size.
The combination of these three materials leads to improved mechanical and tribological properties. Silicon carbide is a material used for mechanical seals. It has the disadvantage of reduced failsafe running functions, causing increased wear when running dry. The added titanium components (TiC and TiB2) improve the failsafe running functions. This technology has already been transferred to industrial applications.
The sintering behaviour of one microcrystalline and several nanocrystalline TiN powders was investigated by means of a gas pressure furnace with an integrated dilatometer. The investigated nanocrystalline powders strongly differ in the sintering activity. It can be concluded from the experiments, that small grain size, narrow grain size distribution and a low oxygen content are the most important prerequisites for high sintering activity of the nanocrystalline TiN powders.
The extraordinary sintering activity of the best TiN powder makes it possible to produce a dense (< 2 % porosity), pure (no sintering aids) and nanostructured (mean diameter of crystals about 100 nm) TiN bodies.
The tribological behaviour of different monolithic and composite ceramics was evaluated in the temperature range between room temperature and 750°C. The test method was oscillating sliding with a ball-on-disk arrangement in an SRV machine. Alumina balls were used as counter body. The friction behaviour was determined on-line, and the wear behaviour was determined from calculations on the basis of wear scar dimensions and profilometric measurements. The friction depends on temperature and shows an increase for most materials for increasing temperature; the smallest friction at all temperatures is found for monolithic TiC. The wear behaviour shows different trends for the different materials. In tests against SiC a maximum of wear is found at 500°C, for TiC at 200°C and for TiB2 at 750°C. The composite ceramics suffer the smallest wear of all materials in the range from 200°C to 500°C.
Stepping piezoelectric actuators based on the stick-slip effect inherently make use of a friction contact between strator and rotor. This contact defines not only the actuator's performance but also is prone to wear and tear. For broad use, the actuator has to be able to perform around 1 million strokes. To assess the actuator's performance in terms of force, speed, mechanical output, electrical input, and long-term stability under different load- and environmental conditions, as well as different friction partners, a dedicated test-bed for a LSPA30µXS motor by Cedrat Technologies has been set up.
The manufacturing of NbC with Ni binder with addition of titanium carbide by using a colloidal process for blending the different powders without a milling step were investigated. The the sintering process and formation of the resulting microstructures, the phase relations and the hardness of the produced cermet materials are characterized.
Niobium carbide is a ceramic material which can be used with excellent results to replace tungsten carbide with cobalt binder. Furthermore, it might be manufactured by classic ceramic technologies and even colloidal processing. To achieve high toughness and strength, it is necessary to have a perfect mix of hard phase and binder, which is mainly achieved by ball milling. Mechanical and physical properties as well as results on different tribological and application-oriented machining tests are presented. The results have been compared with results obtained with NbC grades with Co and Fe3Al binders as well as with pure binderless hot-pressed NbC and SPS sintered Nb2O5.
Niobium-titanium carbide cermets with nickel binder have been prepared by colloidal processing in water without a milling step by using Poly-diallyl-dimethyl-ammonium chloride (Poly-DADMAC) as a dispersant. Homogeneous microstructures with relative densities larger than 99% of the theoretical density have been achieved by gas pressure sintering in argon atmosphere. However, mechanical properties like hardness and strength were slightly decreased due to precipitation of free carbon.
The tribological behaviour under dry sliding conditions of Magneli phase Ti4O7 and e-phase Ti2Cr2O7 with α-alumina as a sliding partner has been characterised at room temperature by oscillating sliding. The mechanical properties as well as Vickers hardness measurements do not reveal big differences between the materials, and 4-point bending strengths are around 200 MPa for both materials. Although the friction coefficients are in the medium range of 0.6 and do not differ much between the materials, the wear behaviour is very different. At room temperature, the wear coefficient of Ti2O7 is strongly dependent on relative humidity, and wear is highest under dry conditions when relative humidity is low as it is typically found for many ceramic materials. Ti2Cr2O7 shows remarkably different wear behaviour with the lowest wear in dry conditions. The measured coefficients of wear at low relative humidity of 4% are more than 2 orders of magnitude lower than those for Ti2O7.