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Organisationseinheit der BAM
Eingeladener Vortrag
- nein (48)
COMPOSITE MATERIALS OF A 99.7 % ALPHA-ALUMINA MATRIX WITH PLATELETS OF SILICON CARBIDE (SICP) HAVE BEEN PREPARED BY GELCASTING. DENSIFICATION WAS CARRIED OUT BY GAS-PRESSURE SINTERING WITHOUT FURTHER SINTERING AIDS. FIVE DIFFERENT COMPOSITIONS WITH 0, 5, 10, 15, AND 20 VOL.% SICP RESP. HAVE BEEN INVESTIGATED AND TRIBOLOGICAL PROPERTIES WERE CHARACTERIZED. INCREASING AMOUNT OF SICP AS RIGID PARTICLES IN THE FINE GRAINED MATRIX COMPLICATE THE DENSIFICATION PROCESS. WITH THE APPLICATION OF 50 BAR AR PRESSURE DURING THE FINAL SINTERING STEP AT A TEMPERATURE OF 1700 DEGREE C THE DENSITY OF THE SAMPLES COULD BE INCREASED BY 3-5%. INVESTIGATION OF THE TRIBOLOGICAL PROPERTIES AGAINST STEEL AS A COUNTERBODY UNDER UNLUBRICATED OSCILLATING SLIDING CONDITIONS SHOWED A HIGH COEFFICIENT OF FRICTION AND AN INCREASING WEAR RATE UP TO A SICP CONTENT OF 10 VOL. % . AT 15 AND 20 VOL. % SICP RESP. BOTH THE COEFFICIENT OF FRICTION AND THE COEFFICIENT OF WEAR DROP DOWN.
Influence of Slip Viscosity on the Mechanical Properties of High Purity Alumina made by Gelcasting
(1997)
The tribological behavior of different low infrared (IR) emission ceramic materials from the titanate group has been investigated at room temperature under gross slip fretting conditions against 100Cr6 ball bearing steel and α-alumina as the counterface materials. For all material pairs, friction and wear depended largely on the relative humidity of the environment. When paired with steel the low IR-emission ceramic disks showed higher wear resistance. Under dry conditions, almost no wear was found on the low IR-emission ceramic specimen. The high wear on the steel counter body is caused not only by tribo-oxidation, which is the main wear mechanism, but also by abrasion. In dry conditions a COF of 0.6 and in humid conditions a COF of 0.2 have been measured. When paired with α-alumina the results on wear are just opposite to those with steel counterbody and the low IR-emission ceramic materials show much lower wear resistance under all conditions. This is explained by the predominance of abrasion and the relatively large difference in hardness between the low IR-emission ceramic and α-alumina. In high humidity environments the results point to the formation of stable reaction layers causing lower friction and wear.
Self-mated magnesia stabilized zirconia (Mg-PSZ) ceramic sliding couples have been investigated at 100 N load (P0max= 1324 MPa) in oscillating sliding conditions in different humidity conditions in air and in hot steam. Temperatures have been varied up to 400 °C and pressures up to 6 bars. The results show that the wear behavior of MgO-ZrO2 under high Hertzian contact pressures is strongly dependent on temperature and is similar for both dry oscillating and oscillating in hot steam. However, although the evolution in wear rates on temperature is similar and the wear rates of MgO-ZrO2 plunged above 300 °C in hot steam and air by nearly three orders of magnitude, SEM micrographs revealed in hot steam at 400 °C smooth wear tracks. In contrast, hot steam enhanced the tribochemistry of self-mated alumina couples and reduced wear rates. Hot steam decreased the coefficients of friction of MgO-ZrO2 with increasing temperature, but not the wear rates.
It has been successfully demonstrated that ceramic materials can be joined in the green
state without a second phase by using low pressure injection molded parts. The investigation of the
joining interface revealed that a high quality interface can be achieved by carefully adjusting the
different manufacturing steps. The use of monomodal particle size distribution in the used powder
CT3000SG is inferior to a broader particle size distribution obtained by replacing 33% of the finer
alumina powder by coarser CT1200SG. In this way the dewaxing process is significantly improved
when the wall thickness of the part exceeds 3 mm. The investigation of the mechanical properties of
the joined and sintered parts revealed, that the bending strength of the joined specimens achieved
about 80 % of the unjoined, monolithic specimens.
Zeta potential as measured with the electrokinetic sonic amplitude (ESA) method has been compared to streaming potential as measured with the particle charge detection (PCD) method. The measurements have been carried out on identical suspensions of a-Al2O3, SiC and Si3N4 with a solids volume fraction of 1% and 10%. Zeta potential and streaming potential are related by a linear function. The correlation coefficients for this relationship are better than 0.99 for the suspensions with 1% solids loading. For the suspensions with 10% solids loading, correlation coefficients are slightly lower due to the influence of increasing viscosity. Regardless of lower correlation at the higher solids loading, the isoelectric pH is constant within the limits of accuracy of the pH measurements.