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Eingeladener Vortrag
- nein (13)
MoSi alloys containing up to 1 wt.% Si were fabricated by powder-metallurgical processing and their lattice parameters, elastic constants, densities, grain sizes, strengths, ductilities, and fracture toughness values were measured. The yield strength was insensitive to the grain size, i.e., a HallPetch relationship was not observed. Generally, Si additions caused pronounced solid solution strengthening. However, for small Si concentrations (≤0.1 wt.%) solid solution softening was observed at room temperature and below. With increasing Si concentration, the room temperature ductility and fracture toughness dropped precipitously. This is attributed to the increase in strength and a transition from transgranular to intergranular fracture.
A miniature specimen geometry is presented that allows to extract small samples for tensile creep tests directly from critical components of steam generators in power plants like e.g. superheater tubes. In this way, material can be tested which has been subjected to the full processing chain of the component. The specimens then exhibit all microstructural modifications that are present in the component after the shaping process and heat treatment, and representative mechanical properties are determined. Similarly, specimens can be extracted from pre-corroded test pieces or used components after service to determine the impact of complex aging/loading/oxidation conditions during service on the mechanical properties of the material. The applicability of the miniature specimen test method is demonstrated in a comparative creep study involving standard and miniature specimens of P91 tempered martensite ferritic steel. Test results indicate satisfactory accuracy/repeatability of the method. Comparison with large scale specimen data reveals an influence of specimen size on the obtained creep behavior. These size effects need to be considered for a correct interpretation of results from miniature specimen creep tests.
The uniaxial, torsional and axial-torsional thermomechanical fatigue (TMF) behavior of the near-γ TiAl-alloy TNB-V5 was investigated. TMF tests were performed at 400-800 °C with mechanical strain amplitudes ranging from 0.15% to 0.7%. The tests were conducted thermomechanically in-phase (IP) and out-of-phase (OP).
For the same lifetimes, uniaxial IP tests required the highest strain amplitudes, while OP test conditions were most damaging and needed the lowest strain amplitudes. The Mises equivalent mechanical strain amplitudes of pure torsional tests were found in between uniaxial in-phase and out-of-phase tests for the same lifetimes. The non-proportional multiaxial out-of-phase test showed a lower lifetime at the same equivalent mechanical strain amplitude compared to the other types of tests.
The microstructure has been characterized applying electron microscopy and microstructural parameters such as fraction of twinned grains, grain size, lamellar distance and dislocation density have been quantified.