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Co-Cr alloys are frequently used for highly stressed components, especially in turbine and plant construction, due to their high resistance to thermal and mechanical stress, as well as to corrosive and abrasive loads. Furthermore, they are classified as difficult-to-cut materials because of their high strength and toughness as well as their low thermal conductivity. However, for Co, an increased cost and supply risk can be observed in recent years. Therefore, additive manufacturing (AM) offers significant economic advantages due to higher material efficiency regarding repair, modification, and manufacturing of such components. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. In addition, subsequent machining, particularly contour milling, is essential to generate the required complex contours and surfaces. Hence, additive and machining manufacturing processes need to be coordinated in a complementary way, especially due to additional challenges arising in milling of heterogeneous hard-to-cut microstructures. Recently, it has been shown that modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), can improve the cutting situation. In this investigation, the Co-Cr initial alloy is additionally modified with Ti and Zr up to 1 wt% with the aim to enhance the homogeneity of the microstructure and, thus, the machinability. Hence the investigation includes finish milling tests of the AM components and the comparison of US and conventional machining. Both the modifications and the ultrasonic assistance exhibit a significant effect on the machining situation; for example US causes a higher surface integrity of the finish milled surfaces compared to conventional milling.
High- and medium-entropy alloys (HEAs) are a quite new class of materials. They have a high potential for applications from low to high temperatures due to the excellent combination of their structural properties.
Concerning their application as components; processing properties, such as machinability, have hardly been investigated so far. Hence, machinability analyses with a focus on the influence of the milling process and its basic parameters (cutting speed, feed per cutting edge) on the resulting surface integrity of specimens from an equiatomic high- (CoCrFeMnNi) and a medium- (CoCrNi) entropy alloy have been carried out. A highly innovative milling process with ultrasonic assistance (USAM) was compared to conventional milling processes.
Recent studies have shown that USAM has a high potential to significantly reduce the mechanical load on the tool and workpiece surface during milling. In this study, the basic machining and ultrasonic parameters were systematically varied. After machining, the surface integrity of the alloys was analyzed in terms of topography, defects, subsurface damage, and residual stresses. It was observed that USAM reduces the cutting forces and increases the surface integrity in terms of lower tensile residual stresses and defect density near the surfaces for the CoCrFeMnNi alloy. It was shown that the cutting forces and the metallurgical influence in the sub surface region are reduced by increasing the cutting speed and reducing the feed rate per cutting edge. With the CoCrNi alloy, the tool revealed severe wear. As a result, for this alloy no influence of the parameters on the machinability could be determined.
Multi-element systems with defined entropy (HEA - High Entropy Alloy or MEA - Medium Entropy Alloy) are rather new material concepts that are becoming increasingly important in materials research and development. Some HEA systems show significantly improved properties or combinations of properties, e.g., the overcome of the trade-off between high strength and ductility. Thus, the synthesis, the resulting microstructures, and properties of HEA have been primarily investigated so far. In addition, processing is crucial to achieve a transfer of potential HEA/MEA materials to real applications, e.g. highly stressed components. Since fusion welding is the most important joining process for metals, it is of vital importance to investigate the weldability of these materials. However, this has rarely been the subject of research up to date. For that reason, in this work the weldability depending on the surface preparation of a CoCrFeMnNi-HEA and a CoCrNi-MEA for TIG welding is investigated. The fusion welding of longer plates is described here for the first time for the CoCrNi alloy. The welds of both materials showed distinct formation of cracks in the heat affected zone (HAZ). Optical and scanning electron microscopy analysis clearly confirmed an intergranular fracture topography. But based on the results, the crack mechanism cannot be conclusively clarified as either a liquid metal embrittlement (LME) or hot cracking like liquid film separation occurred.
Nickel-Iron-Alloy Modification to Enhance Additively Welded Microstructure for Subsequent Milling
(2022)
The aerospace industry uses nickel–iron alloys, e.g., FeNi36, to create moulding tools for composite materials, since these alloys have a low coefficient of thermal expansion. Nickel–iron alloys are hard-to-cut materials. The moulding tools are large in size and involve complex structures, making them cost-intensive and difficult to manufacture. Thus, the focus is set on additive manufacturing, which can additionally enable the repair of components in order to eliminate local defects. However, the process usually results in a heterogeneous microstructure and anisotropic mechanical properties. As there is a high demand for a precise and exact fit of the precision moulds and the surface quality, the welded components must be subsequently machined. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. Consequently, a modification of the microstructure morphology is achieved through specific alloy modifications in order to stabilise and improve the subsequent machining process. Therefore, titanium and zirconium are chosen as modification elements with a maximum 1% weight percent and are added to nickel–iron alloy powder. The elements are alloyed, and build-up welded by plasma-transferred-arcwelding. The resulting microstructure morphology of the welded wall structure and the machining properties are then determined. It can be shown that titanium has a significant effect on the structural morphology of the welded layers, as well as on the machining.
This work explores the feasibility of producing bead-on-plate welds of a CrCoNi medium entropy alloy and a CrMnFeCoNi high entropy alloy using electron beam welding. The alloys were welded in two states: one in an as-cold-rolled condition and the other in an annealed condition. In addition, the materials are welded with two different parameters. The FCC microstructure of the welds is investigated using scanning electron microscopy assisted by energy-dispersive X-ray spectroscopy and electron-backscattered diffraction. The impact of the weld on the microstructure is discussed. The heat-affected zone is negligible for the annealed condition of both medium and high entropy alloys since there is no driving force for recrystallisation and the exposure time to high temperature is insufficient for grain coarsening. The texture formed in the fusion zone is also discussed and compared to the texture in the base metal and the heat-affected zone. Although the grain growth along the (100) crystallographic direction is preferential in all cases, the crystallographic texture type differs from each weld. Higher hardness values are measured in the medium entropy alloy’s base metal and fusion zone than in the high entropy alloy.
When welding super duplex stainless steels a non-admissible pore formation can occur even if recommended processing guidelines are followed strictly. To investigate this phenomenon and to determine the influencing factors different claddings were produced using gas metal arc welding and submerged arc welding. The welding consumables, the shielding gas and the welding flux were varied. As shielding gases several mixtures, based on argon and 30 % helium, with various amounts of nitrogen, nitric oxide, carbondioxid and oxygen were applied. As welding flux agglomerated fluoride basic fluxes and aluminate fluoride basic fluxes were used. Different batches of the similar solid filler wire G 25 9 4 N L were used to produce the claddings on the base material UNS32750. To determine the pore formation X-ray examinations and microsections were used, to analyze the chemical composition of the claddings melt extractions and spectrometric examinations were applied. Additionally, the microhardness and the ferrite number were detected. The studies have shown the shielding gas, the welding flux and the filler metal possess a great influence on the pore formation. Even small variations in the chemical composition of the welding consumables lead to totally different results. In addition, the ferrite number and the chemical composition of the claddings depend strongly on the used gases and filler metals.
Current efforts for lightweight design result in a growing application of high-strength fine-grained structural steel in modern steel constructions, e.g. mobile cranes, with yield strength from 960 MPa. The design of welded structures and the welding process become more challenging with increasing material strength due to higher elastic ratios. The formation of high residual stresses, which are able to diminish lifetime, load capacity and component safety, has to be avoided. Recent numerical and experimental analyses have shown a strong influence of the heat control and the rigidity of the weld on the welding stresses. Global reaction stresses due to an external shrinkage restraint superimpose with local residual stresses in the weld seam. Modern inverter technologies allowed the development of numerous modified spray arc processes driven by the power source manufactures with almost equal characteristics. They provide several well-known technical and economic benefits, like the possibility of welding narrower seam configurations. As a result a smaller weld volume, total heat input and, therefore, reduced welding stresses are achievable. This research focuses on the welding loads due to modified weld seams. The global reaction forces in welded components due to an external shrinkage restraint were investigated in a special in-house developed testing facility. Additionally, the superposition of the local residual stresses, global stresses and bending moments were analysed with the help of X-ray diffraction. The intensity of the restraint, the weld seam configuration and the weld process (transitional arc and modified spray arc) were varied for a statistical evaluation of the resulting welding loads. It was observed that under restraint a smaller weld seam volume affects reduced reaction stresses.
High-strength steels are increasingly applied in modern steel constructions to meet today’s lightweight requirements. Welding of these steels demands a profound knowledge of the interactions between the welding process, cooling conditions, heat input and the resulting metallurgical occurrences in the weld and its vicinity. Additionally, welding stresses may be detrimental for the safety and performance of high-strength steel component welds during fabrication and service, especially due to the high yield ratio. For a development of strategies to adjust welding heat control, all these effects should be considered, to reach a complete exploitation of the high-strength steel potential. In recent researches at BAM, multilayer GMAW experiments were performed with high-strength steels, in which cooling conditions and resulting microstructure were analysed for varied heat control parameters. The application of a unique 3d-operating testing facility and X-ray diffraction measurements allowed the analysis of local stresses in the weld while welding and cooling under component relevant shrinkage restraints. As a result, correlations between material behaviour, welding and cooling condition and the arising multi-axial stresses and forces were found. Based on this study, statements for the development of adapted heat control concepts were derived, which are presented by means of specific analysis examples.
Residual stresses are crucial when assessing the performance of welded components. The present work deals with the possibilities of transferring the real-life boundary conditions of welding, which influence the residual stress, into the laboratory. The possibilities of a test system with a load capacity of 2 MN specifically developed for online monitoring of stress formation and cracking are shown. Due to the structural design, global process, geometry and material-dependent stresses are induced, which can be quantified in-situ during welding and post weld heat treatment. Examples are presented how the conditions to be found during production are simulated in the laboratory. It is shown how welding residual stresses in high-strength steels are affected by the heat control. Elevated working temperatures significantly increase the tensile residual stresses in the heat affected zone (HAZ). The effect of mechanical stresses resulting from welding on stress relief cracking is demonstrated by the example of a creep resistant steel. Reheat cracks were monitored online during post weld heat treatment.
Submerged arc welded (SAW) components of creep-resistant low-alloyed Cr-Mo-V steels are used for thick-walled heavy petrochemical reactors (wall-thickness up to 475 mm) as well as employed in construction of modern high-efficient fossil fired power plants. These large components are accompanied by significant restraints during welding fabrication, especially at positions of different thicknesses like welding of nozzles. As a result, residual stresses occur, playing a domi-nant role concerning so-called stress relief cracking (SRC) typically during post weld heat treat-ment (PWHT). Besides specific metallurgical factors (like secondary hardening due to re-precipitation), high tensile residual stresses are a considerable influence factor on SRC. For the assessment of SRC susceptibility of certain materials mostly mechanical tests are applied which are isolated from the welding process. Conclusions regarding the influence of mechanical factors are rare so far. The present research follows an approach to reproduce loads, which occur during welding of real thick-walled components scaled to laboratory conditions by using tests designed on different measures. A large-scale slit specimen giving a high restraint in 3 dimensions by high stiffness was compared to a medium-scale multi-pass welding U-profile specimen showing a high degree of restraint in longitudinal direction and a small-scale TIG-re-melted specimen. The small-scale specimens were additionally subjected to mechanical bending to induce loads that are found during fabrication on the real-scale in heavy components. Results show for all three cases compa-rable high tensile residual stresses up to yield strength with high gradients in the weld metal and the heat affected zone. Those high tensile stresses can be significant for cracking during further PWHT.