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- Consequences (2)
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Organisationseinheit der BAM
- 3 Gefahrgutumschließungen; Energiespeicher (3)
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- 2.2 Prozesssimulation (2)
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- 7 Bauwerkssicherheit (2)
- 7.5 Technische Eigenschaften von Polymerwerkstoffen (2)
- 8.1 Sensorik, mess- und prüftechnische Verfahren (2)
- 3.5 Sicherheit von Gasspeichern (1)
Slow burst testing of samples as a method for quantification of composite cylinder degradation
(2014)
The current practise to focus periodic retesting of composite cylinders primarily on the hydraulic pressure test has to be evaluated as critical. The test itself always causes a certain amount of micro damage to the cylinders but does not necessarily deliver sufficient and evaluable information. Thus BAM Federal Institute of Materials Research and Testing (Germany) moves the focal point to a new approach for validation of composite cylinders, based on destructive sample tests parallel to operation. Statistical assessment of results of these destructive tests is employed for the estimation of remaining safe service life, based on reliability demands. The estimated service life is also used for the determination of re-test periods of the examined population of composite cylinders.
An essential aspect of this approach is the validation of current residual strength and its prediction at any point of service life. In cases of gas cylinders with very high cycle strength, residual strength cannot be quantified statistically by means of hydraulic load cycles. As a replacement, creep tests or burst tests may be employed. BAM suggests the 'slow burst test SBT' as a combination of these two test procedures. This is a compromise between the practicability of the (conventional) burst test and the practical relevance of sustained loads during service, to be tested in creep rupture tests. In this paper, a variety of 99 burst results of a cylinder design type used for breathing apparatus (CFRP with PE-liner) is evaluated. The influence of test procedure parameters and nature and intensity of artificial ageing on the test sample strength are analysed statistically. This leads to an evaluation of different procedures of artificial ageing and the recommendation to substitute conventional burst tests by slow burst tests for the assessment of composite pressure receptacles.
Commercial, off-the shelf propane cylinders are subjected to high safety regulations. Furthermore, those cylinders are equipped with safety devices like pressure relief valves (PRV). Despite these regulations and safety measures, a failure of the container is possible if exposed to an intense fire. The result of this is severe hazard for users, rescue forces and infrastructure. Within the framework of a destructive test series, 15 identical propane cylinders, without pressure relief devices, were exposed to an intensive fire in horizontal position until failure. Each cylinder was filled with a mass of m =11 kg of liquid propane. Three different fire sources were used (wood, petrol, propane). The experiments revealed the failure of all cylinders in a time period t < 155 s. The failure lead to a fragmentation into several major parts with throwing distances of up to l =262 m. In all trials, the temperature of the cylinder wall (top, side, bottom), of the liquid phase inside and of the surrounding fire (top, side, bottom) was recorded. In addition, the inner cylinder pressure and the induced overpressure of the blast wave after the failure were recorded. Overpressures of up to p=0.27 bar were recorded close to the cylinder (l =5 m). All tests were documented by video from several positions (general view, close-up, high-speed 5000 fps). This test series creates the basis for further experimental studies in the field of alternative fuels for vehicles. The aim of this test series is to assess and analyse the consequences of the failure of gas vessels (for LPG, CNG, CGH2) in the aftermath of severe incidents.
Compressed natural gas (CNG) is a widely used automotive fuel in a variety of countries. In case of a vehicle fire where the safety device also malfunctions, a failure of the CNG automotive cylinder could occur. Such a cylinder failure is associated with severe hazards for the surrounding environment. Firstly, a comprehensive analysis is given below, summarizing various accidents involving CNG automotive cylinders and their consequences. In an extensive experimental program, 21 CNG automotive cylinders with no safety device were tested. Of the 21, burst tests were carried out on 5 Type III and 5 Type IV cylinders. Furthermore, fire tests with 8 Type III and 3 Type IV cylinders were conducted. Apart from cylinder pressure, inner temperature and cylinder mantle temperature, the periphery consequences, such as nearfield blast pressure and fragmentation are documented. The maximum measured overpressure due to a Type III cylinder failure was p = 0.41 bar. Each traceable fragment was georeferenced. All-in-all, fragment throw distances of d > 300 m could be observed. As one key result, it can be stated that the tested Type IV CNG cylinders showed less critical failure behavior then the Type III cylinders under fire impingement.
In case of a vehicle fire, an installed LPG (liquefied petroleum gas) tank with a malfunctioning safety device poses severe hazards. To investigate the consequences in case of tank failure, we conducted 16 tests with toroidal shaped LPG vehicle tanks. Three tanks were used for a Hydraulic Burst Test under standard conditions. Another three tanks were equipped with a statutory safety device and were subjected to a gasoline pool fire. The safety device prevented tank failure, as intended. To generate a statistically valid dataset on tank failure, ten tanks without safety devices were exposed to a gasoline pool fire. Five tanks were filled to a level of 20 %; the re-maining five were filled to a level of 100 %. In order to gain information on the heating process, three tem-perature readings at the tank surface, and three nearby flame temperatures were recorded. At distances of l = (7; 9; 11) m to the tank, the overpressure of the shock wave induced by the tank failure and the unsteady tem-peratures were measured. All ten tanks failed within a time of t < 5 min in a BLEVE (boiling liquid expanding vapor explosion). Seven of these resulted directly in a catastrophic failure. The other three resulted in partial failure followed by catastrophic failure. A near field overpressure at a distance of l = 7 m of up to p = 0.27 bar was measured. All ten tests showed massive fragmentation of the tank mantle. In total, 50 fragments were found. These 50 fragments make-up 88.6 % of the original tank mass. Each fragment was georeferenced and weighed. Fragment throwing distances of l > 250 m occurred. For the tanks with a fill level of 20 %, the average number of fragments was twice as high as it was for the tanks that were filled completely.
Composite materials show a degradation of properties depending on Service life. This creates the necessity to find tailored methods to determine strength and residual strength of composite cylinders. The determination can be done e.g. by load cycles tests. The result needs a Statistical assessment for the precise description of strength. Especially the Statistical assessment of load cycle strength properties has a high uncertainty. It is unclear if a Log-Normal distribution, a WEIBULL distribution or others, describe the scatter behaviour of residual strength properties correctly. Distribution functions aim at approximating the frequency of occurrence of residual load cycle strength for high survival rates. An assumption has to be found and confirmed to prevent overestimation of reliability.
We present the results of distributed fiber optic strain sensing for condition monitoring of a hybrid type IV composite fully wrapped pressure vessel using multilayer integrated optical fibers. Distributed strain sensing was performed for a total number of 252,000 load cycles until burst of the vessel. During this ageing test material fatigue could be monitored and spatially localized. Critical material changes were detected 17,000 cycles before material failure. Results have been validated by acoustic emission analysis.
Gas cylinders made of composite materials receive growing popularity in light-weight applications. Current standards are mostly based on safety determination relying on minimum amounts of endured load cycles and a minimum burst pressure of a small number of specimens. This paper investigates the possibilities of a probabilistic strength assessment for safety improvements as well as cost and weight savings. The probabilistic assessment is based on destructive testing of small sized samples. The influence of sample size on uncertainty of the assessment is analysed. Furthermore, methods for the assessment of in-service ageing (degradation) are discussed and displayed in performance charts.