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Eingeladener Vortrag
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Quantitative online NMR spectroscopy of technical mixtures: on the fly quantification of fluids
(2014)
In this paper quantitative NMR spectroscopy is demonstrated as a tool for process analytical technology (PAT) in order to obtain real time information from dynamic processes. Different methods for quantification are presented and as a result the limit of detection for NMR measurement could be determined to 3.3 mg kg-1 (ethanol in water). As model processes esterification reactions and dissolution of pharmaceutical formulations are presented and important process parameters are extracted. Furthermore it is demonstrated that not only 1H-NMR spectroscopy can be used for process monitoring but also 13C-NMR for technical mixtures.
On the Fly Quantification of Fluids - Quantitative Online NMR Spectroscopy of Technical Mixtures
(2012)
On the Fly Quantification of Fluids - Quantitative Online NMR Spectroscopy of Technical Mixtures
(2012)
NMR-Alles im Fluss
(2012)
Immer im Bild mittels Prozess-Spektroskopie - Spektroskopische Methoden für die Prozessanalytik
(2012)