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Eingeladener Vortrag
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The multiple-sample approach by means of centrifugal adhesion testing (CAT-technology) allows the determination of bonding strength of adhesive-bonded joints on a statistical basis of up to eight samples. Therefore, it is obvious to ensure the continuous handling and identical processing of an octet of samples within the entire process chain of wet-chemical cleaning, plasma-chemical pre-treatment, bonding of samples, and testing of bonding strength. Within the multiple-sample bonding set-up (MPKV-technology) a defined bonding pressure can be adjusted regardless the actual number of samples. A comparison of single- and multiple-sample approach is made for bonding strength of selected adhesives, double-sided adhesive tapes and different material combinations [stainless steel (V2A) vs. stainless steel, polyamide (PA), or polypropylene (PP)]. It is shown that both technologies improve reliability of results
The future commercial prospects for adhesive tapes are very good and its application range is very broad. From every-day-use in office, packaging, maintenance, and quick repair in workshops, it ranges from handicraft work, medical purposes and cosmetics up to workmanship. The study describes a new multi-sample approach in adhesive tape testing from theoretical background, preparation of test specimen for tensile as well as shear testing, detailed measurement procedures up to analysis and result interpretation. Various types of single and double-sided pressure sensitive adhesive tapes supplied by different manufacturers were investigated and compared
Adhesion is a key functionality for any kind of coating/substrate system. For optical applications, metallic and dielectric coatings are of major interest, in particular for crucial materials such as silver and gold on glass or metals and dielectrics on polymers. Adhesive strength is defined as the tensile force per area upon delamination. There are only two tensile testing procedures available, the single-sample pull-off test in a tensile testing machine and the multiple-sample test within a centrifuge. Both tests require bonded test stamps on top of the coating. After testing, a microscopic inspection is required in order to determine the failure pattern according to ISO 10365 such as adhesive failure (AF), delamination failure (DF), and cohesive failure (CF). There are remarkable effects of the substrate thickness and the plasto-elastic properties of the substrate on the measured adhesive strength. This fact is in general unavoidable as adhesion is a system property and testing of adhesion is a destructive stress test of the entire coating/substrate system. Various material combinations such as Al on polypropylene (PP), SiO₂ on CR39 polymer, protected layers of Au and Ag on glass have been investigated. Delamination failure (DF) could be divided into DF-R (delamination of metallic reflector) and DF-D (delamination of dielectric protection). Plasto-elastic properties and different thicknesses of the substrate yield to an uneven bending of these substrates during the test. As a result, unavoidable material-induced shear forces are produced, e.g. in dependence on substrate thickness, which is simulated by means of “inverse” the filmdoctor software usually applied to compressive stress conditions. From the first results this might give access to the adhesive strength as calculated independent of the substrate thickness.