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Overview of ongoing research and future prospects on polyethylene neutron shielding materials at bam
(2023)
The extension of the interim storage period of radioactive waste before disposal will cause additional challenges for the nuclear waste management in Germany, so that an extensive knowledge of the long-term performance of casks, including their components and inventories, will be required for future extended storage licenses.
Ultra-high and high molecular weight polyethylenes ((U)HMW-PE) are used for neutron shielding purposes in casks for storage and transport of spent fuel and high-level waste due to their extremely high hydrogen content. During their service life of several decades as cask components, the PE materials are exposed to neutron and gamma radiation from the radioactive inventory of the casks, mechanical assembling stresses and temperature. All these combined effects affect the material properties of such components which in turn may be crucial for some possible accident scenarios.
At the Bundesanstalt für Materialforschung und -prüfung (BAM), the effects of high temperature exposure in combination with subsequent or previous irradiation were investigated with a comprehensive aging program including thermal aging at 125 °C for different aging periods up to 5 years and irradiation with doses ranging from 50 to 600 kGy.
This contribution provides an overview of the ongoing research related to the structural changes of (U)HMW-PE induced by gamma irradiation and high temperature exposure and focuses on current research perspectives at BAM with regard to the prediction of the dynamic behavior of the material during extended interim storage in case of an accident scenario. First results of the coupled effect of temperature, radiation and mechanical loading will be presented. The effect of microstructural changes induced by gamma irradiation and high temperature on the mechanical behavior of (U)HMW-PE will be assessed.
In line with the industrial trend of additive manufacturing, cold spray as a non-laser-based process is becoming increasingly important for many fields of application. For the evaluation of additive manufacturing of winding components made of copper for large electrical high-voltage machines, material and component properties such as electrical conductivity, mechanical load capacity and the component size that can be produced are of particular importance. In this context, the cold spray process offers advantages over laser-based additive manufacturing processes such as laser powder bed fusion (LPBF) or laser cladding by using the kinetic energy of the copper powder particles to generate particle cohesion. To investigate the electrical conductivity as well as the mechanical load capacity of cold spray parts, specimens were machined out of cold sprayed bulk copper deposits. The characteristic values were obtained with regard to the direction of deposition, which is defined by the direction of the robot’s movement. Thus, for the investigation of the component properties, specimens were provided that had been produced both longitudinally and transversely as well as orthogonally to the direction of deposition. The results of the investigations show that both the electrical conductivity and the mechanical load capacity of the specimen have a strong preferential direction of the specimen orientation with respect to the direction of deposition. Furthermore, it could be shown that by increasing the deposition height, there is an increasing oxygen content in the sample material, combined with increasingly significant defect networks. These effects have a negative impact on the electrical conductivity as well as on the mechanical load capacity. As a conclusion, further need for investigation is identified in the optimization of the process parameters as well as in the deposition strategy for the additive manufacturing of large-volume components with cold spray.
Cast iron arch bridges were built in the late 18th and early 19th century across Europe. After the famous Iron Bridge in the Ironbridge Gorge in Coalbrookdale in England, being now part of the UNESCO world heritage, many cast iron bridges followed and substituted timber bridges. A series of cast iron bridges has been built in central Europe, in Laasan, Breslau, (now Wrocław), in Berlin, Potsdam, Bad Muskau and Schwerin. The paper gives an overview about the current state of some remaining cast iron arch bridges, typical damage cases, material properties and rehabilitation. Most of the old cast iron arch bridges serve as pedestrian bridges. Some of these bridges have been strengthened to increase the traffic load. Different rehabilitation measures as substitution of parts of the bridges and strengthening using Carbon Reinforced Polymers (CFRP) are discussed.
In 1976, a pressure vessel of a tank wagon burst during gravity shunting. The pressure vessel was filled with cold fluid carbon dioxide and failed by cleavage fracture explosively. Big parts of the vessel were flung up to 300 m, a building was destroyed, and rails as well as the superstructure of the gravity shunting yard were damaged.
The initiation sites of the fracture and the orientations of crack propagation were determined by means of the patterns on the fracture surfaces of the broken parts. The initiation sites were located in the heat-affected zone (HAZ) of welds, close to transitions of cross-sections and the starting and end points, respectively, of the welds. The primary initiation of crack propagation was almost certainly on the left side, close to the weld of the fixed bearing connecting the vessel with the carriage.
The results of metallographic investigations indicated the development of cold weld cracks during welding. Mechanical behavior assessments on specimens extracted from the failed vessel indicated sufficient strength and ductility in tensile loading. The values of the notched-bar impact energy or toughness were within the limits according to industry rules and standards, except for one metal sheet of the vessel that was welded to the left fixed bearing.
During shunting, two tank wagons were inappropriately braked, and began to roll too quickly. One rail brake used for deceleration of the wagons caused impulsive noises and vibrations, resulting in high impulsive loading of the first wagon. The cold weld cracks in the heat-affected zones near the fixed bearing of the pressure vessel were initiation points for unstable crack growth. As the result of very low notched-bar impact toughness, crack propagation was not arrested and unstable cleavage fracture occurred.
Due to a second similar accident, happened one year before, a program was started to assess characteristic values of pressure vessel materials and the influence of weld parameters by the manufacturer, the inspecting authority, and BAM. The scientific findings led to modifications of industry rules and standards with regard to using ISO-V specimens and to higher required values for notched-bar impact energy for fine grain structural steels.
Surface modification of mild steel was undertaken using two covered electrodes and two tubular electrodes. The two covered electrodes are DIN 8555: E6-UM-60 and E10-UM-60GR; however, the two tubular electrodes are E10-GF-60GR1 and E10-GF-60GR2. Chemical analysis for the weld metal and XRD of the flux covering for covered electrodes and flux core for tubular electrodes were conducted. The most important factor in determining the wear resistance is the microstructure of the deposit layers. In similar carbon equivalent electrodes E10-UM-60GR and E10-GF-60GR1, electrode E10-GF-60GR1 (tubular) shows larger carbides area fraction and better wear resistance than electrode E10-UM-60GR (covered). This could be attributed to a lower dilution associated with tubular electrode compared with covered electrode. The two tubular electrodes showed higher wear resistance than the covered electrodes which is mainly due to the larger Fe-Cr carbide precipitation area fraction.
Grain refinement is an important possibility to enhance the mechanical properties such as strength, ductility and toughness of aluminium weld metal. In this study, grain refinement was achieved through the addition of commercial grain refiner Al Ti5B1 to gas tungsten arc weld metal of the aluminium alloys 1050A (Al 99.5) and 5083 (Al Mg4.5Mn0.7). The grain refiner additions led to a significant reduction of the weld metal mean grain size (Alloy 1050A, 86 %; Alloy 5083, 44 %) with a change in grain shape from columnar to equiaxed. Tensile tests showed for Alloy 5083 that the weld metal's ductility can be increased through grain refinement. No improvement in weld metal strength (i.e. yield strength and ultimate tensile strength) was observed. Furthermore, tear tests with notched specimens revealed that the resistance against initiation and propagation of cracks in the weld metal can be enhanced through grain refinement. The toughness was observed to increase clearly by grain refinement in weld metal of commercial pure Al (Alloy 1050A). In Alloy 5083 weld metal, the toughness was not improved through grain refinement, likely because of a semi-continuous network of brittle intermetallic phases that facilitate crack propagation.
End of November 2005 strong south-west wind and heavy snowfall were predominant in the region Münsterland, north-western part of Germany. This led to accretion of a considerable quantity of wet snow to overhead electrical lines in form of snow rolls on the conductors. Eighty-two transmission towers failed catastrophically, most of them by buckling, however some by brittle fracture. As a consequence nearly 250,000 people have been cut off from electrical power supply for several days with major media attention.
This paper describes the forensic analysis in order to investigate the failure cause. Therefore extensive materials investigations, mechanical testing of original components and specimens thereof, estimations for the real wind and snow loads and their combinations, structural analyses as well as detailed evaluations on the basis of previous investigations, literature and regulations were conducted. It was revealed that some of the examined components were manufactured from Thomas steel which was partially in embrittled condition. The investigated towers fulfilled the design codes valid at the time of erection. However the present line loads of the wet snow rolls on the conductors exceeded by far the ones given in the design codes valid at that time.
The load case leading to failure was reconstructed by the derived positions of loads mainly caused by unequal and asymmetric distribution of snow rolls on left and right electrical system. The loads and corresponding stresses acting on the structure before failure were estimated. By comparison with the fracture forces from mechanical testing of original members of the collapsed tower the component that primarily failed was localised. The primary fracture occurred on a diagonal member under tension made of Thomas steel which was weakened by embrittlement. The failure cause was a combination of heavy weather conditions (storm, approx. 0 °C and wet snowfall leading to heavy snow rolls on conductors), asymmetric loading conditions and the usage of Thomas steel which was partially embrittled. Finally, recommendations for avoiding future failures are given.
Zur Abschätzung der Lebensdauer eines bei höherer Temperatur langzeitbelasteten Bauteils wurden Zeitstandversuche, Relaxationsversuche und weitere Versuche mit unterschiedlichen Umgebungssteifigkeiten durchgeführt.
Die Zeitstandversuche, deren Versuchsführung eine unendlich niedrige Umgebungssteifigkeit simuliert, liefern geringere Lebensdauern (Bruchzeiten) im Vergleich zu Versuchen mit endlich hohen, technisch relevanten Steifigkeiten bei vergleichbarer Probensteifigkeit (Geometrie), wobei die Lebensdauern mit steigender Umgebungssteifigkeit zunehmen. Die längsten Lebensdauern zeigen Relaxationsversuche mit einer unendlich hohen Umgebungssteifigkeit aufgrund ihrer Versuchsregelung.
Für die Übertragung der an Proben gewonnenen Ergebnisse auf das Bauteil wurde das Steifigkeitsverhältnis Z zwischen der Steifigkeit der 'Probe' und der der 'Umgebung' definiert und angewandt. Das Steifigkeitsverhältnis des kritischen Bereichs im Bauteil und das der Werkstoffprobe in der Prüfmaschine sollten möglichst ähnlich sein. Dann lassen sich bei der Übertragung auf das Bauteil realistisch höhere Lebensdauern abschätzen als nur mit Kenntnis der Ergebnisse der Zeitstandversuche.