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The relation between microstructure and corrosion behavior of GTA welded AZ31B magnesium sheet
(2007)
Welding of AZ31B magnesium alloy was carried out using gas-tungsten arc (GTA) welding. The microstructure and the corrosion behavior of welded magnesium AZ31B alloy were investigated. ac and dc polarization tests were carried out on the welded Mg sheet. The microstructure was examined using optical and electron microscopy (TEM and SEM), X-ray analysis and EDS. Scanning Kelvin probe force microscopy (SKPFM) was used in order to measure the Volta potential of different phases relative to the matrix. The results showed that the GTA process effected both the microstructure and the corrosion behavior. These results can be explained by the effects of the process on microstructure of AZ31B Mg alloy sheet such as grain size and precipitates caused by the change in precipitation and recrystallization behavior.
Analysis of Residual Stress Distribution in Welded Joints Depending on the Restraint Intensity
(2003)
Hydrogen assisted steel corrosion and cold cracking is still a major topic regarding the reliability of welded steel components, such as offshore platforms and pipelines. Measurement of local and crack critical hydrogen concentrations in a specific weld is difficult and not very precise. Numerical simulations of hydrogen uptake and diffusion developed within the last twenty years have to be regarded as much more effective to determine local hydrogen concentrations in crack critical regions of welds. As an overview of existing theories of the state of the art in modelling of hydrogen cracking in steels, the present contribution shows that the development of a comprehensive numerical model for both types of hydrogen assisted cracking in welds, hydrogen assisted stress corrosion cracking and cold cracking, is still a major research task. As a first step towards that direction, a basic procedure for numerical simulation of crack initiation and propagation has been developed and experimentally verified. The approach can be extended to a comprehensive quantitative model for life time prediction and risk based inspection of welded steel components. (Steel specimen used was S355 along with other materials such as AISI 321, Incoloy 800, Inconel 690 and 600.)
This chapter introduces conceptually Part C of the Handbook Technical Diagnostics of Machines and Plants. Although various prescriptions for organization and performing failure analyses are existing in literature [1–6], up to the present no approach is consistent to the concept of technical systems in the Sects 2.2 and 2.3 (Fig. 2.6) and thus, a comprehensive concept is outlined in this section, with a special attribute to the VDI-Guideline 3822 Failure Analysis.
More than 400 iron hydrogen storage containers (also called bottles or cylinders exploded on the air strip Berlin-Tempelhof on May 25, 1894, leaving immense destruction. The Royal Prussian Materials Testing Institute was requested to investigate the material properties and to furnish an expertise, how an increased safety of such cylinders might be achieved for the future under protection of the interests of the air ship service, as for instance by improvement of delivery specifications or respective material inspections.
The studies conducted personally by the director Prof. Adolf Martens and his deputy Prof. M. Rudeloff represent one of the first comprehensive failure case investigations in history and initiated BAMs long tradition in failure analysis. Martens and his colleague elaborated quite detailed specimen plans and investigated original failure parts with a special emphasis on conspicuous fracture appearance, but also made comparison experiments with hardened as well as annealed samples. Experienced investigators might identify some first routines how to conduct failure analyses and the importance of Adolf Martens as a pioneer in this field becomes evident.
Martens publications about the original expertise Martens, 1896 [1] and [2] include detailed descriptions about the experimental procedures and specimen preparation. Also, quite modern materials testing technologies and machines have been utilized, as for instance light microscopy as well as the tensile testing machines developed by Werder and Pohlmeyer. As special features developed by Martens, precision strain measurements have been applied during respective tensile tests and the so-called micro-photographic apparatus has been adopted to produce photos of the investigated microstructures. Additionally, the publications contain at that time very valuable advices regarding appropriate materials selection for gas storage cylinders.
The present contribution provides a nearly complete and as exact as possible translation of the original report Martens, 1896 [1] written in Old German language. Only little changes have been made in the text for a better understanding.
Short Term Metallurgy and Hot Cracking During Laser Beam Welding of Austenitic Stainless Steels
(2011)
Industrial application of high alloyed austenitic stainless steel laser welding has grown significantly in the recent time due to the continuous improvement of compact and high power density lasers systems. The application of such processes meanwhile ranges from pipeline or railway car body manufacturing to the production of household wares. The largest advantages of the laser application to welding production are much higher welding speeds, reduction or complete exclusion of welding consumables, easy design of the weld joints, decrease of thermal distortions and thus, costs saving. In contrast to arc welding, laser beam welding might particularly be associated with metallurgical defects, like the formation of hot cracks. Such phenomena are related to an order of magnitude higher temperature gradients and cooling rates in the solidification zone, providing rapid solidification kinetics which may cause significant segregation of alloying elements such as Ni and Cr and respective undercooling of the solute at the solidification front. In specific metastable austenitic stainless steels alloys in vicinity of the so called eutectic rim of the Fe-Cr-Ni constitutional diagram, such effects might entail a change of solidification mode from primary ferrite to austenite, providing an increased risk of solidification cracking. Previous studies has shown that the primary solidification mode change during laser beam welding of Cr-Ni austenitic stainless steels such alloys could be effectively influenced by nitrogen absorption as well as by the laser plasma type and also proved the occurrence of metastable primary ferritic solidification. In the present contribution, such results are compared to recent investigations of laser welding newer austenitic Fe-Cr-Mn-Ni steel grades by identification of respective hot cracking critical welding parameter intervals and strain rates in the Controlled Thermal Weldability (CTW) Test.
Hydrogen might cause severe degradation of supermartensitic stainless steels, if they are activated during exposure to sour environments. Consistent and comprehensive data for hydrogen transport in these materials are thus required to support, in particular, modelling of hydrogen assisted cracking as a part of life time assessment of welded steel components. In addition to previously published diffusion coefficients and subsurface concentrations of a supermartensitic stainless steel further data dependent on heat treatment are provided by this contribution. Furthermore, a higher alloyed material has been investigated in the state as received and also in the quenched condition, in order to approach the influences of chemical composition on hydrogen transport in supermartensitic stainless steels. With respect to welding it turned out that the diffusion coefficient and the subsurface concentration are markedly dependent on heat treatment of the materials.