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- Hydrogen absorption (2)
- Hydrogen desorption (2)
- Thermal desorption spectroscopy (TDS) (2)
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The relation between microstructure and corrosion behavior of GTA welded AZ31B magnesium sheet
(2007)
Welding of AZ31B magnesium alloy was carried out using gas-tungsten arc (GTA) welding. The microstructure and the corrosion behavior of welded magnesium AZ31B alloy were investigated. ac and dc polarization tests were carried out on the welded Mg sheet. The microstructure was examined using optical and electron microscopy (TEM and SEM), X-ray analysis and EDS. Scanning Kelvin probe force microscopy (SKPFM) was used in order to measure the Volta potential of different phases relative to the matrix. The results showed that the GTA process effected both the microstructure and the corrosion behavior. These results can be explained by the effects of the process on microstructure of AZ31B Mg alloy sheet such as grain size and precipitates caused by the change in precipitation and recrystallization behavior.
Different characteristics of hydrogen's absorption/desorption behavior and trapping in ß-21S titanium alloy are studied by means of thermal desorption spectroscopy (TDS). Spectra analysis is supported by data from variety of other experimental techniques, such as LECO hydrogen determinator, XRD and microstructure investigations by means of optic and electronic microscopy. In contrast to many past considerations, the complex process of hydrogen evolution has been found to be significantly affected by the way hydrogen introduction into the alloy. The different trapping sites, as well as phase transformations, have to be considered as the reasons for the different hydrogen evolution behavior.
Based on its excellent combination of a high strength/weight ratio and good corrosion behavior, Ti6Al4V alloy is ranked among the most important advanced materials for a variety of industrial applications. However, in many of these technological applications, this alloy is exposed to environments which can act as sources of hydrogen, and severe problems may arise based on its susceptibility to hydrogen embrittlement. Even small hydrogen concentrations might lead to failure. Consequently, a comprehensive knowledge of hydrogen's absorption/desorption behavior and interactions between hydrogen and different microstructural features is necessary to better understand the desorption and trapping mechanisms, the types of the trap sites, and the trapped hydrogen content, in order to determine the safe service conditions of this alloy in the industry. In this paper, different characteristics of hydrogen's absorption/desorption behavior and trapping in a duplex-annealed Ti6Al4V alloy are studied by means of thermal desorption spectroscopy (TDS). Spectra analysis is supported by data from a variety of other experimental techniques, such as LECO hydrogen determinator, XRD and microstructure investigations by means of optical and electron microscopy. Hydrogen evolution is found to be a very complex process, being affected by the way hydrogen was initially introduced to the alloy, the phase transformations that may occur during the thermal analysis and the presence of potential trapping sites.