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Mechanisms and fast kinetics of the catastrophic optical damage (COD) in GaAs-based diode lasers
(2011)
COD diagram determined for a batch of broad-area AlGaAs diode lasers. The time to COD within a single current pulse is plotted versus the actual average optical power in the moment when the COD takes place. Full circles stand for clearly identified COD events (right ordinate), whereas open circles (left ordinate) represent the pulse duration in experiments, where no COD has been detected. A borderline (gray) exists between two regions, i. e., parameter sets, of presence (orange) and absence of COD (blue). This borderline is somewhat blurred because of the randomness in filamentation of the laser nearfield and scatter in properties of the involved individual devices.
Complex special inspection of an old masonry arch bridge according to the Guideline on Inspection and Condition Assessment of Railway Bridges and numerical analysis of the structure are presented. The guideline summarises recommendations for the step-by-step investigation of railway bridges applying enhanced methods developed during the EU-funded project Sustainable Bridges. For the investigation of the arch barrel, the ballast parameters and the inner structure of the backfill behind the arch barrel a number of various advanced non-destructive and minor-destructive testing methods were applied. Deformation of the structure during load tests was measured using three independent measuring systems: laser vibrometer, LVDT and microwave radar. Results of calculations performed with 2D and 3D models based on FEM are compared with the field load tests. Sensitivity of the ultimate load of the structure to investigated parameters is studied in FE model. Some general conclusions according to methods of testing and modelling of masonry arch bridges are presented and discussed.
Single-pulse tests of the catastrophic optical damage (COD) are performed for three batches of diode lasers with different gain-regions. The tests involve in situ inspection of front, rear, and side of the devices by a thermocamera. Devices with an Al-containing gain-region show COD at the front facet, as expected for strong facet heating via surface recombination and reabsorption of laser light. In contrast, Al-free devices with low surface recombination rates tend to fail at the rear facet, pointing to a different heating scenario. The high carrier density at the rear facet favors heating and COD via Auger recombination processes.
The findings indicate that rolling contact fatigue with consecutive head checks develops preferentially in rail sections that have experienced operational work-hardening. Such hardening can be identified by instruments measuring the increased hardness values with respect to the base material. Eddy current testing was initially introduced with the aim to detect head checks and determine their damage depth. Because the material texture influences eddy current flow in the test objects very strongly, variations in hardness can easily be visualised using this method. Thus, in principle, it is possible to predict places where head checks will emerge later. This knowledge may be very helpful in improving our understanding of head check emergence under real conditions. This knowledge may also help in developing new and effective precautionary maintenance strategies.
In this work, the applicability of a new 3D micro X-ray fluorescence (3D Micro-XRF) laboratory spectrometer for the investigation of historical glass objects is demonstrated. The non-destructiveness of the technique and the possibility to measure three-dimensionally resolved fluorescence renders this technique into a suitable tool for the analysis of cultural heritage objects. Although absorption and resolution effects complicate qualitative analysis of the data, layered structures can be distinguished from homogeneous samples without the need for full quantification. Different manufacturing techniques were studied in this work with the help of hand-made reference samples. With the gained knowledge it could be shown for the investigated historical glass object, that black enamel as a stained glass contour colour was used in a cold painting. The object was not fired after the application of the black enamel, but instead the adhesion of the paint was solely provided through organic binding agents and the backing with metal foils. Thus, for the manufacturing of the object, a mixture of cold painting technique with a stained glass color was used. Quantitative measurements with a 3D Micro-XRF setup at the Berlin synchrotron BESSY II confirm the assumptions drawn on the basis of the qualitative investigation with the 3D Micro-XRF spectrometer with X-ray tube excitation.
Moisture ingress is one of major damaging factors for masonry buildings. As the complex resistivity (CR) is sensitive to textural properties as well as to the pore fluid chemistry of wet porous media, its non-destructive application can provide helpful information for conservators. In a comprehensive laboratory study it has been shown that CR might even be able to distinguish between salt content and saturation degree in only one measurement. The combined use of electrical and electromagnetic measurement techniques in two field-scale flooding experiments has shown some unexpected differences. Possible reasons are discussed and it is shown that bringing together the information of both methods leads to a clearer picture.
Fe K-edge XANES measurements were performed to determine the oxidation state of iron in iron gall inks. These data are used to investigate the relationship between the Fe oxidation state and ink corrosion in historical manuscripts. The oxidation state is determined using the pre-edge based on a general variation trend that was derived from model compounds and validated here independently on a suite of samples with known oxidation state and Fe in octahedral coordination (i.e. similar to Fe in gall ink). As long as suitable references for the pure ferric and ferrous state of iron gall inks cannot be pointed out, the analysis of the pre-edge of the Fe K-edge represents the only way to acquire absolute values for the Fe oxidation state (Fe3+/Fetot) with spatial resolution for this usually non-crystalline compound. Fe3+/Fetot values for the ink samples vary between ca. 0.7 and 1.0. Spatially resolved analyses performed across ink strokes of various historical manuscripts as well as newly made samples did not reveal any systematic spatial dependence. On average, historical samples that were exposed to conservation treatments show a more oxidized state. However, the measurements demonstrate explicitly that the exposure to X-rays during the XANES acquisition affects the oxidation state of Fe in most iron gall inks.
Collecting different geophysical data sets at the same object and site offers the opportunity to reduce uncertainties and ambiguities in data analysis and interpretation. To be effective, the different available data sets should be linked during the model-generation process, e.g. by cooperative inversion. In this study, we apply a recently developed zonal cooperative inversion approach based on fuzzy c-means cluster analysis to a non-destructive testing experiment. After briefly reviewing the fundamentals of the inversion strategy, we present a synthetic study investigating the potential of the method to detect air-filled voids in masonry by using ultrasonic and georadar traveltime data. Then, we present and discuss laboratory experiments including the results of cooperatively inverted ultrasonic and georadar traveltimes collected at a masonry test specimen. The geometry of the specimen is known and is thus an ideal test object for a first-time real application of the novel zonal cooperative inversion procedure. Compared to the results of separate inversions of ultrasonic and georadar traveltimes, the zonal cooperative inversion allows for an improved delineation of the size and position of the cavities. The P-wave and georadar velocities determined for the model regions corresponding to the cavities are also improved.
Validation of non-destructive testing methods is necessary to create a common basis where different systems can be compared and their applications and limitations be identified. This can be achieved through comparing the measurements taken by several systems used for a common diagnostic purpose under practical but controlled testing conditions. Well-designed small and large laboratory or field specimens promise such conditions.
The special concrete specimen (LCS) at BAM was constructed for validation purposes, in particular, to be used for evaluating the performance of echo methods. The thickness of the specimen is varying and it contains carefully designed built-in faults, such as voids, honeycombs and tendon ducts with various degrees of grouting defects. Since the geometry and condition of the defects are known, it can be used to compare the performance of radar, ultrasonic, impact-echo. The research was conducted within the Research group FOR384, sponsored by the German Research Society DFG.
This paper presents the progress of successful location of grouting faults in tendon ducts with ultrasonic imaging. The examples were obtained in the research group FOR 384 funded by DFG (German Research Foundation). The co-operation of experimental research and modeling allowed imaging and identification of grouted and ungrouted areas of tendon ducts (including strands) in a large test specimen (40 m²). In addition to the criteria for indicating grouting faults in post-tensioned ducts known until now the phase evaluation of reflected ultrasonic pulses is described. Experiments and modeling of wave propagation are presented for reflections at metal plates in concrete (thickness range 0.5 mm to 40 mm) and for tendon ducts including strands.
The main part of the progress was achieved by automated measurements using dry contact transducers, 3D-SAFT reconstruction including phase evaluation and modeling considering wave propagation for typical elastic parameters and exact experimental site conditions. The results for shear waves as well as for pressure waves are compared in the frequency range from 50 kHz to 120 kHz.
Unsafe tailings management facilities (TMFs) have caused serious accidents in Europe (e.g., Baia Mare, Romania, in 2000, Aznalcóllar, Spain, in 1998, and Stava, Italy, in 1985), threatening human health/life and the environment. While advanced design, construction and management procedures are available, their implementation requires greater emphasis. An integrated research project funded by the European Union was carried out between 2002 and 2005 with the overall goal of improving the safety of TMFs (Sustainable Improvement in Safety of Tailings Facilities-TAILSAFE, http://www.tailsafe.com/). The objective of TAILSAFE was to develop and apply methods of parameter evaluation and measurement for the assessment and improvement of the safety state of tailings facilities, with particular attention to the stability of tailings dams and slurries, the special risks inherent when such materials include toxic or hazardous wastes, and authorization and management procedures for tailings facilities. Aspects of tailings facilities design, water management and slurry transport, non-destructive and minimally intrusive testing methods, monitoring and the application of sensors, intervention and remediation options were considered in TAILSAFE. A risk reduction framework (the TAILSAFE Parameter Framework) was established to contribute to the avoidance of catastrophic accidents and hazards from tailings facilities. Tailings from the mining and primary processing of metals, minerals and coal were included within the scope of TAILSAFE. The project focused on the avoidance of hazards by developing procedures and methods for investigating and improving the stability of tailings dams and tailings bodies.
Application of synchrotron infrared radiation in the study of organic coatings in cross-sections
(2008)
Dielectric and electromechanical properties of the cellular polypropylene ferroelectret films (EMFIT), combining strong piezoelectric response with a low density and softness, evidence their high potential for the air-coupled ultrasonic applications. The disadvantage of the low coupling factor is compensated by the extremely low acoustic impedance, which provides excellent matching to air and promises efficient sound transmission through the airtransducer interface. The influence of the electrodes on the electromechanical properties was investigated. Electron beam evaporation technology was adapted to the EMFIT films, and films with both-sided Au and Al electrodes were prepared without reducing or suppressing of the electromechanical properties. Finally, prototype transducers based on the EMFIT films were developed. In spite of the simple construction and absence of matching layers, high sensitivity of the EMFIT transducers was proved in the air-coupled ultrasonic experiment. Amplitude and delay time scanned images of the polyethylene step wedge with holes, obtained in both pulse-echo and transmission modes, demonstrate that non-contact ultrasonic imaging and testing with EMFIT transducers is possible.
A new approach is discussed for characterizing the damage state of FRP with the appearance of micro cracking and its influence on the residual strength. For the quantitative analysis of micro cracking, X-ray refraction topography was used. Fatigue treatment of carbon fibre reinforced plastics (CFRP) laminates were performed to create defined damage states. With regard to real loading conditions of CFRP, studies on tube samples were performed to investigate two dimensional (tensiontorsion) loads. A rheological material model was presented which described the increase of micro cracking in ±45° CFRP laminates with a continuum mechanical approach. The correlation between the results of the X-ray refraction topography, the damage parameter of the rheological model and the decrease of residual strength were shown. The inter fibre fracture surface of the investigated CFRP materials was determined with tensiontorsion loaded tube specimens of 90°-laminate and a layer-wise strength analysis was done. Micro cracking occurs even at 50% inter-fibre fracture loading and can lead to a distinct strength reduction. The intralaminar fatigue effect itself seems to be an indication for the damage accumulation and the load history.
The low-strain pile integrity testing method is used for quality control of new piles as well as length and integrity check for old piles. If no other methods for calibration are available, the accuracy and reliability of the techniques depend on a good estimation of the elastic wave velocity. In practice it is assumed that piles can be tested 7 days after casting and that the velocity is almost constant in all piles of one kind in a construction project. Recent measurements at the BAM test site in Horstwalde, Germany, showed that the 7 day criterion is not generally applicable.
Impulse-thermography is an active method for quantitative investigations of the near surface region of various structures. It has recently been applied and optimised to applications in civil engineering. By using either an internal or external heat source, parts of the structure under investigation are heated up and the transient heat flux is observed by recording the temperature change at the surface as a function of time. This method is very well suited for the detection of voids and honeycombing in concrete, up to concrete covers of 10 cm as well as for the location of delaminations in multi-layered systems (e.g. plaster on concrete, CFRP-laminates on concrete, asphalt on concrete). Also safety relevant defects like voids in tendon ducts and cracks in concrete could be recognised.
Results of reconstructed and fused NDT-data measured in the laboratory and on-site at bridges
(2006)
Non-destructive testing (NDT) of concrete structures plays an increasing role in civil engineering. This paper presents the results of measurements carried out in the laboratory at BAM and on-site at several bridges using reconstructed and fused radar and ultrasonic echo data sets. In this context different scanning systems, developed for the on-site application of NDT-methods (e.g. reinforced concrete bridges) are introduced. The main object was the demonstration of the improved effectiveness of radar and ultrasonic pulse echo technique due to the automated measurements and the application of new software for the data processing and data visualisation. The results of these measurements show the high potential of reconstruction and data fusion for the improvement and simplification of the interpretability of large data sets measured with impulse-echo methods.
New thermography systems enable the application of active investigation techniques, i.e. the observation of the cooling down process after heating the surface of a structure under investigation. Defects like voids in concrete having a different thermal diffusivity in comparison to the bulk material are visualised by different surface temperatures. The differences between temperature transient curves above sound regions and above inhomogeneities are expected to include information about the defect parameters.
Experimental investigations with impulse thermography and radar on a concrete test specimen containing voids were analysed. Radar was used to determine the depth of the voids. The influence of size and depth of the voids on the temperature transient curves was studied for different heating times. The transient curves were also fitted with a simple semi-empirical model.
Non-destructive testing (NDT) of concrete structures is performed using pulse-echo methods. According to the type of the applied waves it can be classified as acoustic (Impact-Echo, Ultrasonics) and electromagnetic methods (Radar). The results are visualised through different imaging processes. This work is performed in the frame of a research project promoted by Deutsche Forschungsgemeinschaft (FOR384). The objective of data fusion is to use the complementary information of the different methods. Radar can detect metallic reflectors in concrete (metallic ducts and concrete reinforcement) very well. This method is not able to locate defects behind these reflectors (injecting defects, defects behind close concrete reinforcement), because the electromagnetic waves are completely reflected at metals. The acoustic methods are able to compensate this deficit i.e. Acoustic waves can penetrate through metal. But acoustic waves in the ultrasonic range are completely reflected by air layers. Air layers have smaller influence on radar propagation, so that both methods complement each other. In order to be able to combine the NDT-data from several methods records at the same volume, the different data setsmodes of signals must be adapted. The ultrasonic and radar data have to be reconstructed with programs based on the Synthetic Aperture Focusing Technique (SAFT) before data fusion. Subsequently, a conversion of the data into a uniform format has to be carried out. This is a prerequisite in order to keep the data exchange between the project partners as simple as possible. After the data sets are imported and transferred into a common reference system, they can be processed with operations according to the purpose of the investigation. Results, which have been achieved in concrete test specimen with radar and ultrasonics, will be presented and will show the feasibility of the data fusion method.
Determination of chloride content in concrete structures with laser-induced breakdown spectroscopy
(2005)
An important criterion for the evaluation of reinforced concrete structures is the measurement of the chloride content. This will normally be done by time consuming standard chemical methods. We propose the application of a spectroscopic technique, the laser-induced breakdown spectroscopy (LIBS), which provides the advantages of a fast measurement, the potential for on-site application and the possibility to investigate a wide range of different measuring points. The surface can be scanned, or depth profiles are available from cores. Measurements can be performed directly on the sample surface and the results are available in near real time. We present LIBS results measured on concrete cores as well as on grinded and pressed material in comparison with the results of standard chemical methods. The optimum LIBS set-up and the experimental conditions to detect and measure chlorine in building materials are reported. The limits of detection were determined and calibration curves were measured.
Impulse-thermography has been established as a fast and reliable tool in many areas of non-destructive testing. In recent years several investigations have been done to apply active thermography to civil engineering. For quantitative investigations in this area of application, finite difference calculations have been performed for systematic studies on the influence of environmental conditions, heating power and time, defect depth and size and thermal properties of the bulk material (concrete). The comparison of simulated and experimental data enables the quantitative analysis of defects.
Impulse-thermography is an active method for quantitative investigation of the near surface region of various structures which has recently been applied to civil engineering. It is well suited for the detection of voids and honeycombing in concrete up to concrete covers of 10 cm and more. For quantitative analysis, a computer program for numerical simulation of the heating up and cooling down processes was developed based on Finite Differences. With this program parameter studies have been performed for investigating the influence of environmental conditions, material parameters and geometry on the thermal behaviour. The comparison between experimental and simulated results enables the Inverse Solution.