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Präsentation im Rahmen eines BAM-internen Kolloquiums über den aktuellen Stand der Forschung im ZIM-Vorhaben "Tieftemperatzr-Transporteinheit aus Faserverbundkunststoffen"
Pulsed thermography is a well-known non-destructive testing technique and has proven to be a valuable tool for examination of material defects, to determine thermal material parameters, and the thickness of test specimens through calibration or mathematical models. However, the application to semitransparent materials is quite new and demanding, especially for semitransparent materials like epoxy, polyamide 12, or glass fiber reinforced polymers with epoxy or polyamide matrix.
In order to describe the temporal temperature evolution in such materials, which are recorded with an infrared camera during pulse thermography experiments, much more influences have to be considered, compared to opaque materials:
- The wavelength of the excitation source and the spectral range of the infrared camera
- The angles between the specimen, the excitation source and the infrared camera
- The area behind the specimen
- The roughness of the material surface
- The scattering mechanism within the material
Here, we will consider all these influences and describe how they can be treated mathematically in analytical or numerical models (using COMSOL Multiphysics software). These models describe the temperature development during the pulse thermography experiment in reflection and transmission configuration. By fitting the results of the mathematical models to experimental data it is possible to determine the thickness or the optical and thermal properties of the specimen.
This presentation describes the testing methods used to determine the thermal properties of insulation materials and mechanical properties of materials used for the load-bearing structure for pressure tanks (up to 4 bar) and cryogenic liquids (LNG, -162 °C at atmospheric pressure). Goal is to design a transportation tank that does not exceed 4 bars (relative) within 10 h, starting at atmospheric pressure. PUR-foam is a suitable material for the insulation. A 12,5 l small scale tank prototype reached 4 bar (relative) within 87 minutes, which is, regarding the influence of the size, a satisfying result. The mechanical properties change significantly at cryogenic temperatures. The bending modulus is similar at first, but decreases at a certain point by 2/3. However, the maximum stress is much higher and could not be reached within this testing setup.