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This paper describes a wireless mobile prototype able to perform optical measurements by means of a miniatur-ized spectrometer for low light analysis, e.g. fluorescent sensors. Evaluations, calculations, calibration management and result display are performed by a computer or a standard tablet. The device was designed primarily to detect traces of oil in drinking or ground water and for the analyses of crude oils. However, it can also address a wide range of fluorescent sensors. The fast and user-friendly inspection of water quality or oil properties, as well as the adaptability and mobility, make the device attractive for a variety of users. Further application areas could be easily imple-mented by adapting the optics and the software (database, data processing and calibration plots, etc.)
A composite material is a combination of two or more materials with very different mechanical, thermal and electrical properties. The various forms of composite materials, due to their high material properties, are widely used as structural materials in the aviation, space, marine, automobile, and sports industries. However, some defects like voids, delamination, or inhomogeneous fiber distribution that form during the fabricating processes of composites can seriously affect the mechanical properties of the composite material. In this study, several imaging NDE techniques such as: thermography, high frequency eddy current, ultrasonic, x-ray radiography, x-ray laminography, and high resolution x-ray CT were conducted to characterize the microstructure of carbon fiber composites. Then, a 3D analysis was implemented by the destructive technique of serial sectioning for the same sample tested by the NDE methods. To better analyze the results of this work and extract a clear volume image for all features and defects contained in the composite material, an intensive comparison was conducted among hundreds of 3D-NDE and multi serial sections’ scan images showing the microstructure variation.
Validation of artificial defects for non-destructive testing measurements on a reference structure
(2018)
Non-destructive testing was established over the last decades as an important tool for assessing damages, material characterization and quality assurance in civil engineering. For example, Ground Penetrating Radar (GPR) can be used to scan large areas of concrete structures to determine the spatial position of the reinforcement. With the ultrasonic echo method, the thickness of concrete structures can be easily determined even if a high density of reinforcement is given. Various methods and processes have been developed for the validation of NDT procedures aiming at ensuring the quality of measurements in practical use. The Probability of Detection (POD) for example, is an available method to compare different technical devices with each other quantitatively regarding their performance. With this method, the best suited testing device for a specific inspection task under defined boundary conditions can be selected. By using the Guide to the Expression of Uncertainty in Measurement (GUM), it is possible to quantify the measurement uncertainty of an inspection procedure for a specific task. Another important aspect to improve the acceptance of Non-destructive testing methods is the development of reference specimens.
Reference specimens serve for the calibration and further development of NDT methods under realistic conditions in different laboratories under the same conditions. A particular challenge here is the most realistic representation of a damage that can occur at building sites. Possible damages include for example horizontal and vertical cracks or honeycombs in concrete. Such a reference structure was built for the development of a new design of power plant constructions. Comparative studies on the manufacturing of realistic honeycombs and delaminations were carried out in advance on a test specimen. The results of this study are presented here.
During the energy transformation from fossil fuels to renewable energy sources, the use of hydrogen as fuel and energy storage can play a key role. This presents new challenges to industry and the scientific community alike. The storage and transport of hydrogen, which is nowadays mainly realized by austenitic stainless steels, remains problematic, which is due to the degradation of mechanical properties and the possibility of phase transformation by hydrogen diffusion and accumulation. The development of materials and technologies requires a fundamental understanding of these degradation processes. Therefore, studying the behavior of hydrogen in austenitic steel contributes to an understanding of the damage processes, which is crucial for both life assessment and safe use of components in industry and transportation. As one of the few tools that is capable of depicting the distribution of hydrogen in steels, time-of-flight secondary ion mass spectrometry was conducted after electrochemical charging. To obtain further information about the structural composition and cracking behavior, electron-backscattered diffraction and scanning electron microscopy were performed. Gathered data of chemical composition and topography were treated employing data fusion, thus creating a comprehensive portrait of hydrogen-induced effects in the austenite grade AISI 304L. Specimens were electrochemically charged with deuterium instead of hydrogen. This arises from the difficulties to distinguish between artificially charged hydrogen and traces existing in the material or the rest gas in the analysis chamber. Similar diffusion and permeation behavior, as well as solubility, allow nonetheless to draw conclusions from the experiments.
We demonstrate narrow band spectral intensity switching in dual-core photonic crystal fibers made of highly nonlinear glass under femtosecond excitation. The fibers expressed dual-core asymmetry, thus the slow and fast fiber cores were unambiguously distinguished according to their dispersion profiles. The asymmetry effect on the dual-core Propagation in anomalous dispersion region was studied both experimentally and numerically. The experimental study was carried
out using femtosecond laser amplifier system providing tunable pulses in range of 1500 nm - 1800 nm. The obtained results unveiled, that it is possible to improve nonlinearly the coupling between the two waveguides by excitation of the fast fiber core. The results were obtained in regime of high-order soliton propagation and were verified numerically by the coupled generalized nonlinear Schrödinger equations model. The spectral analysis of the radiation transferred to the non-excited core revealed the role of effects such as third order dispersion, soliton compression and spectral dependence of the coupling efficiency. The simulation results provide reasonable agreement with the experimentally observed spectral evolutions in the both fiber cores. Under 1800 nm excitation, narrow band spectral intensity switching was registered with contrast of 23 dB at 10 mm fiber length by changing the excitation pulse energy in sub-nanojoule range.
THz and mid IR spectroscopy of high-molecular PE (HMW) and ultra high-molecular PE (UHMW) reveals modifications of the molecular structure. Characteristic absorption bands are changed if the two materials are exposed by γ-Co60 radiation up to 600 kGy and subsequently stored at an annealing temperature of 398 K until for 729 days.
Among the photothermal methods, full-field thermal imaging is used to characterize materials, to determine thicknesses of layers, or to find inhomogeneities such as voids or cracks. The use of classical light sources such as flash lamps (impulse heating) or halogen lamps (modulated heating) led to a variety of nondestructive testing methods, in particular, lock-in and flash-thermography. In vertical-cavity surface-emitting lasers (VCSELs), laser light is emitted perpendicularly to the surface with a symmetrical beam profile. Due to the vertical structure, they can be arranged in large arrays of many thousands of individual lasers, which allows power scaling into the kilowatt range. Recently, a high-power yet very compact version of such a VCSEL-array became available that offers both the fast timing behavior of a laser as well as the large illumination area of a lamp. Moreover, it allows a spatial and temporal control of the heating because individual parts of the array can be controlled arbitrarily in frequency, amplitude, and phase. In conjunction with a fast infrared camera, such structured heating opens up a field of novel thermal imaging and testing methods. As a first demonstration of this approach, we chose a testing problem very challenging to conventional thermal infrared testing: The detection of very thin subsurface defects perpendicularly oriented to the surface of metallic samples. First, we generate destructively interfering thermal wave fields, which are then affected by the presence of defects within their reach. It turned out that this technique allows highly sensitive detection of subsurface defects down to depths in excess of the usual thermographic rule of thumb, with no need for a reference or surface preparation.
This paper addresses the effects of the deterioration on the value of damage detection information. The quan-tification of the value of damage detection information for deteriorated structures is based on Bayesian pre-posterior decision analysis, comprising structural system performance models, consequence, benefit and costs models and damage detection information models throughout the service life of a structural system. The value of damage detection information accounts for the relevance and precision of the information to ensure the structural integrity and to reduce the potential structural system risks and expected costs throughout the ser-vice life before implementing damage detection system. With the developed approach, the value of damage detection information for a statically determinate Pratt truss bridge girder subjected to different deterioration models is calculated. The analysis shows the impact of the deterioration model parameters on the value of damage detection information. The results can be used to develop optimal maintenance strategies before im-plementation of the damage detection system.
In this paper, a nonlinear three-dimensional finite element (FE) model was developed and validated to study the effect of seismic damage location on the response of concrete filled tube (CFT) columns at fire after earthquakes. Three analyses were conducted consecutively in the modelling, namely, cyclic, thermal and structural. Results of the cyclic loading analysis comprising residual deformations were applied as the Initial condition to the thermal-stress model, replicating the seismic performance of column.
Following, a nonlinear sequentially coupled-thermal stress Analysis was carried out to investigate the fire response of CFT columns after the seismic event. Three damage scenarios were contemplated, considering any possible potential damages that could be generated by the earthquake loading on CFT columns. The accuracy of the proposed FE model was examined by comparing the numerical results with that of available tests on fire and cyclic loading. By means of the validated model, the performance of damaged CFT columns was then investigated under fire after earthquakes. The level of damage was assumed as a high damage level, presuming that the column reached 50% of ist lateral resistance while still maintaining its overall stability after the earthquake. The results were presented broadly, including the axial deformation history as well as the fire resistance time for CFT columns. To have a comprehensive insight on the influence of damage location in columns, the fire response of damaged specimens was compared with that of an intact one.
Systematic errors in the evaluation of uncorrected data from thermographic lock-in measurements
(2018)
Lock-in thermography (LT) is based on the correct evaluation of phase differences between the temperature oscillations at different surface regions of the object under test during periodic heating. Since the usual heating procedures contain a DC component, the actual heating pattern achieved is not harmonic. This causes systematic deviations when phase differences are determined by means of harmonic analysis, e.g. with FFT analysis. The resulting errors depend clearly on the ratio between DC and AC amplitude, which is demonstrated at simulated and experimentally recorded temperature transients. Further experimental LT data obtained by different oscillating energy inputs showed a variety of possible shapes of transients with different DC components.