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Eingeladener Vortrag
- nein (1032)
Different, partly complementary and partly redundant characterization methods were applied to study the transition of magnetite, graphite and MoS2 powders to mechanically alloyed nanostructures. The applied methods were: Transmission electron microscopy (TEM), Mössbauer spectroscopy (MS), Raman spectroscopy (RS), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). The main objective was to prepare a model material providing the essential features of a typical tribofilm forming during automotive braking, and to assess the impact of different constituents on sliding behaviour and friction level. Irrespective of the initial grain size, the raw materials were transferred to a nanocrystalline structure and mixed on a nanoscopic scale during high energy ball milling. Whereas magnetite remained almost unchanged, graphite and molybdenum disulphide were transformed to a nanocrystalline and highly disordered structure. The observed increase of the coefficient of friction was attributed to a loss of lubricity of the latter ingredient due to this transformation and subsequent oxidation.
Tribofilms formed during dry sliding usually exhibit a nanocrystalline structure and complicated composition. In the present study, tribofilms consisting mainly of a solid lubricant, namely graphite nanoparticles, are considered. Systems providing such tribofilms are candidates for anti-friction applications. Since sliding action always leads to mixing of the materials at both sides of the tribological interface, it was of major interest to study the impact of different amounts of a hard constituent, SiC in the considered case, within the soft matrix systematically. Furthermore, the impact of normal pressure was considered. A mechanically mixed layer was observed for the whole range of normal pressures and SiC volume fractions. The calculated coefficient of friction decreased significantly with increasing thickness of this layer but was only marginally affected by SiC volume fraction, which is good news for anti-friction applications.
A model based on movable cellular automata has been applied to study the sliding behaviour of tribofilms formed during automotive braking. Since it is not possible yet to determine the composition of real tribofilms quantitatively, final verification of modelling results is needed. This was done by preparing artificial third bodies with compositions and nanostructures matching the ones assumed for modelling. Pin-on-disc tests were performed while applying the artificial third bodies to the contact. The results revealed that not only the structure of the third body but also the amount of the applied normal pressure determines the COF obtained by modelling and that much better correlation between experimental and modelling results was obtained while assuming high normal pressures at asperity contacts.
Many performance properties of devices or interacting machine parts are related to superficial layers which often show completely different or at least modified microstructures compared to the bulk materials. A quasi non-destructive technique will be described which enables us to obtain detailed information of a material's state at a certain site of interest down to a depth of 10 µm from the surface with nanometre or even atomistic resolution.
Dangerous goods are transported as air freight in commercial aircrafts. Using plastic jerrycans or plastic containers, liquids or gases can escape by leakage or permeation effects. Prior research by the German Federal Institute for Materials Research and Testing (BAM) showed that the lower explosion limit can be reached when transporting dangerous goods in sea-freight containers under normal transportation situations. This motivated the presented study of the transportation situation of dangerous goods in cargo compartments of commercial airplanes. The scope of this paper is to present the experimental method used for validating a numerical model for CFD (Computational Fluid Dynamics) simulations. The CFD model will be used in a future study to evaluate the potential risk from transporting dangerous goods.
The objective of this paper is to present the model mock-up of an aircraft cargo compartment and some examples of three dimensional velocity profiles of the air flow in the mock-up. The velocity profiles are calculated using numerical simulations and measured by Laser-Doppler-Anemometry (LDA) experiments. The mock-up is a generic model of a wide-body aircraft lower deck cargo compartment in a 1:10 scale. Geometry, air exchange rates and inlet as well as outlet flow conditions in the cargo compartment are modeled using realistic boundary conditions. The commercial CFD (Computational Fluid Dynamics) code ANSYS CFX 14 is used for numerical flow simulations applying RANS (Reynolds-Averaged-Navier-Stokes) equations and turbulence models. The turbulence models studied are the renormalization group k-ε-model (RNG), the Reynolds-Stress model by Launder, Reece and Rodi (LRR) and the SST-k-ω-model by Menter (SST).
The flow measurement with LDA in the mock-up of a cargo compartment proves to be a feasible method for producing data to validate CFD simulations. Qualitative evaluation of the results shows a good overall agreement between numerical and experimental results. The experimental validation indicates that the implemented CFD model is capable of reproducing the flow situation in the model mock-up.