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Fire exposure tests of acetylene cylinders were performed. The purpose of the experiments was to gather information on the behavior in fire of such vessels, depending on the initial charge of acetylene. In fact "empty" acetylene cylinders still contain the solvent in which acetylene is dissolved plus the amount of acetylene to saturation at atmospheric pressure and ambient temperature and may still constitute a threat to safety. In the fire exposure tests performed the hazardousness of these vessels was demonstrated, since it was observed that not only fully charged acetylene cylinders but also cylinders with saturated solvent can explode, provided the heat transfer to the vessel is sufficient. The times to explosion were shorter for fully charged cylinders, due to the higher initial pressure and to the faster pressure increase. The effects of the explosions are comparable for both fully charged cylinders and for cylinders with saturated solvent, except for the smaller fireball which is produced in the second case, due to the smaller amount of fuel available. In both cases the cylinder walls or at least fragments can fly further than 100 m away from the burst location. Results of the experiments are presented in the paper. During the tests, temperature measurements at the cylinder walls and in the cylinder interior were performed. Furthermore, the pressure in the cylinder was recorded. The collected data will serve for the validation of a numerical model for the simulation of the heating of acetylene cylinders involved in fire and of the afterward cooling with water, which has been developed. The constitutive model equations and the results of some simulations are presented in the paper.
Simulation of the Crushing of Wood Filled Impact Limiters for Packages of Radioactive Material
(2008)
Mechanical and thermal safety assessment of packages for transport of radioactive material in Germany is carried out by the Federal Institute for Materials Research and Testing (BAM). Both experimental and computational (analytical, numerical) methods combined with material and/or component tests are the basis for the state of the art safety assessment concept at BAM. The required mechanical tests according to IAEA regulations include, among others, a 9-m-drop-test on an unyielding target. Impact limiting components, which are attached to the cask at both ends, limit forces applied on the cask body and lid system by absorbing a major part of the impact energy. In Germany, impact limiters of packages for transport of radioactive materials are typically of steel-wood-sandwich construction, combining a relatively stiff steel structure bolted to the cask body, outer steel plates and different types of wood. By crushing the wood-steel-sandwich-structure between an unyielding target and the cask, the kinetic energy of a 9-m-free-fall is absorbed. The main energy absorber is wood under a high level of deformation. Wood under large deformations exhibits destruction of the fibre matrix. By analysing compression of the impact limiter wood after the drop tests with prototype casks for radioactive material, underlying mechanisms of wood crushing and corresponding energy absorption under large deformations are identified. Softening occuring at compression of the wood is a function of the lateral strain restriction of wood. Against the background of continuum mechanics an analogous model for compression of the fibre bundle is presented. The model takes the lateral strain restriction as triaxiality of the stress state into account. Further modelling possibilities for wood with a continuum approach are described. Different material laws in the explicit finite element code LS-DYNA are analysed for possible application using the analogous model for the fibre bundle. Small scale compression tests with wooden specimens are modelled in order to evaluate the ability of different modelling techniques to simulate softening. Although modelling of the compression of wood under large deformations is possible, softening could not be simulated purposefully. A drop test of a cask with impact limiting devices similar to existing impact limiters is simulated with different material laws for wood. The behaviour of impact limiting devices could not be simulated universally including the influence of the lateral strain restriction; nevertheless loading of the cask by crushing of the impact limiter could be simulated purposefully. Verification with experimental results is essential.
The program PowderCell is a crystallographic tool for visualization of Crystal structures. However, it offers also non-conventional features like the fulautomatical generation of subgroups or the consideration of non-standard settings of space-group types. On the one Hand the program is very useful for non-crystallographers who like to get an impression of the atomic arrangement within the unit cell. But also for crystallographers it is recommendable because it contains a lot of additional information which can be extracted and used like data given in the International Tables for Crystallography, Vol. A. However, the most important advantage of the program is the simultaneous calculation of the X-ray or neutron diffraction powder patterns for a mixture of up to 10 crystalline phases. Between more than 7 different characteristic radiations can be chosen and their influence on the resulting powder pattern can be studied. Furthermore, experimental diffractograms can be analysed using a refinement procedure. The implemented LeBail-algorithm allows the investigation of unknown phases. In combination with the refinement algorithm an interface to Shelx offers the possibility for a step by step ab initio structure analysis. Certainly, the user-friendly shell is one reason that especially users who are not so familar with space-group symmetry, crystal structure data or diffractometry use this powerful tool for the solution of scientific or analytical problems as well as in teaching.