Filtern
Erscheinungsjahr
- 2023 (510) (entfernen)
Dokumenttyp
- Zeitschriftenartikel (510) (entfernen)
Sprache
- Englisch (472)
- Deutsch (32)
- Mehrsprachig (4)
- Französisch (1)
- Russisch (1)
Schlagworte
- Additive manufacturing (17)
- SAXS (11)
- Microstructure (9)
- Corrosion (8)
- Fluorescence (8)
- X-ray scattering (8)
- Concrete (7)
- LIBS (7)
- Laser beam welding (7)
- MOUSE (7)
Organisationseinheit der BAM
- 6 Materialchemie (118)
- 8 Zerstörungsfreie Prüfung (93)
- 1 Analytische Chemie; Referenzmaterialien (86)
- 7 Bauwerkssicherheit (75)
- 5 Werkstofftechnik (62)
- 9 Komponentensicherheit (55)
- 6.3 Strukturanalytik (46)
- 4 Material und Umwelt (40)
- 8.5 Röntgenbildgebung (33)
- 5.1 Mikrostruktur Design und Degradation (24)
Paper des Monats
- ja (50)
It is proposed to model the experimentally observed weld pool boundary with superellipses (Lamé curves) and to find the unknown parameters of the curves using optimization methods. It has been shown experimentally that during laser welding of austenitic stainless steel with a thickness of 2 mm at a speed of 20 mm/s, the rear weld pool part has a shape close to triangular which can be accurately approximated by a superellipse. Analytical dependences of the trajectory and growth rate of the crystal and its cross-sectional area on the geometry of the rear weld pool part are obtained.
Agar gel pads have been used for electrochemical measurements for some time. For zinc in particular, a standard method for measuring the stability of the corrosion product layer is being established. The main interpretation factor is the corrosion product layer resistance RL, as it is easy to determine and interpret. A high corrosion product layer resistance indicates a high level of protection. However, it is not yet known how low the corrosion product layer resistance is for freshly produced zinc samples. As zinc is highly active, it reacts immediately with the environment to form a corrosion product layer, which affects the corrosion product layer resistance. The addition of zinc acetate to the agar gel pads prevents the formation of a surface layer and destroys existing ones.
This makes it possible to measure an almost corrosion product-free zinc surface. This is important in defining the range of corrosion product layer resistance for a protective surface.
Cryoadsorption on the inner surface of porous materials is a promising solution for safe, fast, and reversible hydrogen storage. Within the class of highly porous metal−organic frameworks, zeolitic imidazolate frameworks (ZIFs) show high thermal, chemical, and mechanical stability. In this study, we selected ZIF-8 synthesized mechanochemically by twin-screw extrusion as powder and pellets. The hydrogen storage capacity at 77 K and up to 100 bar has been analyzed in two laboratories applying three different measurement setups showing a high reproducibility. Pelletizing ZIF-8 increases the packing density close to the corresponding value for a single crystal without loss of porosity, resulting in an improved volumetric hydrogen storage capacity close to the upper limit for a single crystal. The high volumetric uptake combined with a low and constant heat of adsorption provides ca. 31 g of usable hydrogen per liter of pellet assuming a temperature−pressure swing adsorption process between 77 K − 100 bar and 117 K − 5 bar. Cycling experiments do not indicate any degradation in storage capacity. The excellent stability during preparation, handling, and operation of ZIF-8 pellets demonstrates its potential as a robust adsorbent material for technical application in pilot- and full-scale adsorption vessel prototypes.
X‑ray emission during the ablative processing of biological materials by ultrashort laser pulses
(2023)
The ablative laser processing with ultrashort pulsed laser beams may cause secondary emission of hazardous X-rays. While the effect has recently been proven to be considered in working safety regulations when processing technical materials, such as metals, the X-ray emission rates during the ablative processing of biological tissue materials are widely unexplored yet.
Therefore, biological materials like water, isotonic saline solution, pig eyes, and human teeth were ablated with ultrashort laser pulses of 1030 nm wavelength, 600 fs pulse duration and 5 kHz pulse repetition rate, aiming to mimic typical surgery situations. Simultaneously, in-situ X-ray dose rate measurements were performed at a short distance from the plasma to display potential X-ray emission. For all four studied biological materials, our measurements prove the secondary emission of laser-induced X-rays.
Der zukünftige Eurocode 7 wird ausdrücklich die Nutzung zuverlässigkeitsbasierter Methoden in der geotechnischen Planung und Bemessung erlauben. In Deutschland gibt es bisher kaum Erfahrung in der praktischen Anwendung derartiger Verfahren und entsprechend sind die Vorbehalte gegenüber diesen Methoden oft groß. Der neue DGGT-Arbeitskreis (AK) 2.15 „Zuverlässigkeitsbasierte Methoden in der Geotechnik“ hat sich zum Ziel gesetzt, durch praxisorientierte Anleitungen und Empfehlungen sowie begleitende Aus- und Weiterbildungsangebote den praktischen Zugang zu diesen Verfahren zu unterstützen. Ziel ist es, Möglichkeiten und Grenzen zu verdeutlichen sowie vor allem ihre Potenziale zu erschließen. In dem vorliegenden Beitrag werden allgemeine Grundlagen und die zukünftigen Arbeitsfelder des AK 2.15 vorgestellt. Ausgehend von der Einführung relevanter Fachbegriffe wird zunächst die Einbettung zuverlässigkeitsbasierter Verfahren in den aktuellen Normungs- und Regelungskontext aufgezeigt. Anschließend werden anhand des Lebenszyklus eines geotechnischen Bauwerks die Unsicherheiten in den geotechnischen Prognosen und Bewertungen beschrieben. Daran anknüpfend wird aufgezeigt, an welchen Stellen zuverlässigkeitsbasierte Methoden als mögliches Werkzeug sinnvoll genutzt werden können, um Ingenieur:innen, Bauherr:innen und Prüfer:innen in Nachweis- und Entscheidungsprozessen zu unterstützen. Zu den sich daraus ableitenden Arbeitsthemen werden durch den AK 2.15 zukünftig Empfehlungen erarbeitet und sukzessive veröffentlicht
A collaborative trial involving 16 participants from nine European countries was conducted within the NORMAN network in efforts to harmonise suspect and non-target screening of environmental contaminants in whole fish samples of bream (Abramis brama). Participants were provided with freeze-dried, homogenised fish samples from a contaminated and a reference site, extracts (spiked and non-spiked) and reference sample preparation protocols for liquid chromatography (LC) and gas chromatography (GC) coupled to high resolution mass spectrometry (HRMS). Participants extracted fish samples using their in-house sample preparation method and/or the protocol provided. Participants correctly identified 9-69% of spiked compounds using LC-HRMS and 20-60% of spiked compounds using GC-HRMS. From the contaminated site, suspect screening with participants’ own suspect lists led to putative identification of on average ~145 and ~20 unique features per participant using LC-HRMS and GC-HRMS, respectively, while non-target screening identified on average ~42 and ~56 unique features per participant using LC-HRMS and GC-HRMS, respectively. Within the same sub-group of sample preparation method, only a few features were identified by at least two participants in suspect screening (16 features using LC-HRMS, 0 features using GC-HRMS) and non-target screening (0 features using LC-HRMS, 2 features using GC-HRMS). The compounds identified had log octanol/water partition coefficient (KOW) values ranging from -9.9 to 16 and mass-to-charge ratio (m/z) of 68 to 761 (LC-HRMS and GC-HRMS). A significant linear trend was found between log KOW and m/z for the GC-HRMS data. Overall, these findings indicate that differences in screening results are mainly due to the data analysis workflows used by different participants. Further work is needed to harmonise the results obtained when applying suspect and non-target screening approaches to environmental biota samples.
Wet-mechanical treatment: Processing of bituminous road construction waste in a jigging machine
(2023)
Jigging machines are used in processing technology in many areas. Examples are the processing of coal, ores, and primary and secondary raw and waste materials. Even small differences in density are offen sufficient for successful sorting. In the work presented here, milled material from road construction waste contaminated with bitumen is to be separated from uncontaminated material. In this way, scarce landfill space could be saved and mineral material be returned to the material cycle.
Weather-dependent passive thermography and thermal simulation of in-service wind turbine blades
(2023)
. To cope with the increase in the manufacturing and operation of wind turbines, wind farm operators need inspection tools that are able to provide reliable information while keeping the downtime low. Current inspection techniques require to stop the wind turbine. This work presents the current progress in the project EvalTherm, in which passive thermography is evaluated as a possible non-destructive inspection tool for operational wind turbine blades (WTBs). A methodology to obtain thermal images of rotating WTBs has been established in this project. However, the quality of the results is heavily dependent on various aspects such as weather conditions, information on the inspected WTB, damage history, etc. In this work, a section of a used WTB is simulated using finite-element modelling (FEM) as well as experimentally tested for evaluating the accuracy of the model. Such a model will provide insight into the potential thermal response of a certain structure (with specific material properties) in given weather (boundary) conditions. The model is able to provide satisfactory predictions of the thermal response of the structure, as well as indicate what thermal contrast(s) result from artificial defects introduced in the structure.