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While the absorption of X-rays and gamma radiation is determined by the Z-number of the elements a specimen is composed of, it is the hydrogen making an effective contrast with neutron imaging. As a consequence, interrogating with neutrons presents a suitable tool to study the distribution of organic consolidants in materials such as wood as encountered in impregnated wooden artworks.
Four different examples of objects are presented here to demonstrate the potential of neutron CT: 1) small wooden pieces of ship wrecks (< 2 cm thickness) interrogated with cold neutrons (0.5 meV at the ANTARES facility of the FRM II in Garching) to demonstrate the potential and the limitation of using low energy neutrons, 2) a wooden statue soaked with carbolineum (fission neutrons 1.8 MeV at the NECTAR facility of the FRM II), 3) a smaller wooden figure of a skull heavily soaked with carbolineum so it was too tight for the fission neutrons used before with accelerator neutrons (broad range about 5.5 MeV at the PTB in Braunschweig) and 4) pieces of charred wood to study the impregnation with a consolidant (NECTAR, FRM II). With the exception of the last example, all results have been combined with X-ray tomography (BAM 8.3 in Berlin). In the case of the charred wood specimens (example 4) the density histograms of the neutron tomography results were compared with those obtained from untreated references. The observed gain in specific density of the soaked specimens corresponded with an increase of specific weight. All results obtained so far showed distinct distribution patterns attributable to structural peculiarities or organic consolidants providing valuable support for subsequent restoration works.
Rare events are understood to be events occurring once in a while but with dramatic consequences. Their occurrence cannot be predicted precisely, only a probability might be estimated, for example from past experiences. However, it might be rather misleading to attempt to describe them by distribution curves that apply for frequent or repeated observations, such as the Gaussian bell shape. Alternative distributions have been introduced to characterise the intervals at which a certain event may occur. It is the aim of technical safety and public security to prevent adverse events. Detectable indications that are typical for their course and are observable have to be identified before an incident occurs. Since they should be characteristic for such cases, they themselves also constitute rare events. The problem encountered in any detection system is that nothing is perfect. As in medical diagnostics, true indications may be missed or false test responses may pretend to be something that does not exist. Balancing missed indications with false positive calls is achieved with the aid of the so-called receiver operating characteristics (ROC). However, with the aid of Bayes’ inference it can be shown that identifying signs of a rarely occurring indication is like looking for a needle in a haystack, even with an excellent detection Approach with a low miss rate and an even lower probability of false calls. The inclusion of additionally available information may lead to a more effective search strategy. When employing imaging methods for detecting flaws or illicit items, the identification of rare indications can be impeded by blurring noise or overlapping items. The identification of the features sought can be supported by including information on their typical characteristics
by regularisation algorithms. The strategy of such an approach is demonstrated in a simplified example with a plain geometric figure (circle) corrupted with structural noise. The shape of the original figure was clearly recovered. In general, search strategies should aim at an indication typical for the event to be prevented; otherwise, alternative approaches have to be considered, including, perhaps, serendipity.
The baroque epitaph Reyer (1704) at the St. Laurentius church in Tönning was treated with carbolineum as a wood preservation agent in 1903. The subsequent constant migration of carbolineum through the layers of paint to the surface has had a detrimental effect on the aesthetic appearance of the epitaph. Carbolineum is an oily, water-insoluble, flammable, dark brown mixture of coal tar oil components. Due to its content of polycyclic aromatic hydrocarbons (PAH), which are classified as carcinogenic and harmful to the environment, the use of carbolineum has been forbidden. The aim of the project is to develop an exemplary Conservation treatment (hat will reduce the toxic contents of the historical wooden object. The new method should be applicable to similar objects that are also contaminated with carbolineum. The historic carbolineum was identified by the GC-MS method and the X-Ray computed tomography revealed the biological wood damage and previous restoration measures. Several decontamination methods such as the extraction with supercritical C02, with dichloromethane vapour/fluids, with 1,3-dioxolane or with petrol ether by vaccum impregnation were investigated. This project is founded by the Deutsche Bundesstiftung Umwelt (DBU).
The objects of this investigation were sculptures taken from a ca. three hundred years old baroque epitaph of a church in Tonning, a town in Northern Germany. Around 1900 it was found in a disastrous state heavily damaged by wood-worm. At that time, the whole artwork was treated with the tar extract carbolineum as a remedy. Nowadays, this substance has been identified as carcinogenic, and its presence can be perceived by its stench and visually at certain spots on the surface where it has penetrated the covering paint.
A gold-painted sculpture of a massive wooden skull was interrogated with X-rays and fast neutrons to investigate the internal distribution of the carbolineum. The X-ray tomography, with its excellent spatial resolution revealed galleries left over from the worm infestation in the outer areas and cracks in the central region. The golden color coating appeared as a thick and dense layer. In comparison the tomography with fast neutrons, though being of lower resolution and yet unresolved artefacts revealed sections of slightly different densities in the bulk of the wood. These differences we attribute to the differences in the distribution of the impregnant in the wood, visible due to its higher hydrogen content making it less transparent for neutrons.
Wooden artworks residing in churches for centuries inevitably suffered from decaying processes such as Wood worm infestation. About 100 years ago, this process was ceased with a polluting coal tar extract 'Carbolineum', a treatment usually applied to railway sleepers. Nowadays, this lead to undesired effects not only of causing dark stains on the surface of the treated sculptures but also in unimpaired release of traces of harmful substances into the atmosphere perceptible as the typical smell of coal tar oil. To resolve this problem, the knowledge of the internal structure could provide a support for this effort. As an example, sculptures from an epitaph in a church in northern Germany were subjected to X-ray and neutron computed tomography (CT). The purpose of using neutrons was to get information about the distribution of the impregnant Carbolineum. It consists of a mixture of polycyclic aromatic hydrocarbons which should increase the absorption of neutrons. In contrast, X-rays are rather poorly absorbed by such substances as compared to the wood matrix. All radiographic approaches
revealed traces of previous conservation measures that were not always documented in detail. Comparing the neutron images with those from the X-ray interrogation some differences became obvious indicating varied material compositions. Nails e.g. were clearly visible in the X-ray images rather than in the neutron ones. Some less visibly stained parts of the sculptures correspond with obviously replaced materials in the inside. These results will be used to identify ways how to treat the infested artworks.
EFNDT working group 5 'NDT technology for public security and safety', two areas with the same aim
(2014)
It is a quite common and understandable wish to make the world a safer place. This entails both freedom from danger, and thus encompasses both, safety and security. However, it is a trivial fact that public security and technical safety are commitments to distinct social entities that might be quite understandable due to the various kinds of threats. On the other hand, it is a common justifiable interest to have effective methodologies to detect them in time, i.e., before something disastrous might happen. It is rather obvious that particularly non-destructive inspection technologies, namely radiological methods, are applied in both areas. As a logical consequence, sharing the technical knowledge and experiences could be of benefit for both of them. However, the different areas of activities cleave the information exchange between them. In order to overcome this gap, the EFNDT Working Group 5 'NDT Technology for Public Security and Safety' (EFNDT WG 5) has taken an initiative to bring together actors of both areas of activities, symbolized as building a 'bridge'. The activities of the EFNDT WG 5 range from identifying features exhibiting certain threats that are detectable with available NDT technologies, adapting and improving them according to their specified applications and to search for alternative technologies or ways of applications where deemed to be applicable. Successful exchanges of information and experiences have been achieved in recent workshops, where also new ideas have been raised for future common projects. This kind of work is far from being completed; it is more or less at its beginning. In future workshops it is intended to follow up these ideas and to pave the way for future common interdisciplinary projects. Therefore, all groups involved in such projects are welcome, not only researchers and NDT-specialists, but also all endusers of the respective technologies as well as theoreticians for risk assessment, performance evaluation, modelling, statistics etc. All the addressed areas are deemed to play an important role in making the world a safer place, cooperatively.
As a matter of fact, avoiding unexpected events with an undesired outcome is an element of survival strategies.
Such events are encountered unexpectedly mainly because they occur rarely. Both, safety and security measures are the main pillars to prevent them by appropriate inspections. Common tools in both areas e.g. are radiological technologies enabling an insight into objects to detect suspicious features without even touching them. Since any of these measures is linked to efforts, costs or even obstructions of ongoing processes, it needs a rationale to invest into an appropriate activity. A putative objection to take action in this direction always could be the question 'when and how often it could happen'. This gave rise to find approaches how to define 'rare events' and how to deal with them. Since they entail both, the frequency of occurrence and the unpleasantness of the possible outcome make them to have something in common with the definition of risk: a combination of the probability of occurrence of harm and the severity of that harm. Tackling putative consequences is one side of the coin whereas understanding the rareness of an event is the other, an aspect that worries but not always fully understood.
As a first step in approaching the subject 'rare events', the putative occurrence rate is considered in terms of probability distribution functions or their cumulative ones, resp. The problems of estimating an incidence of such an event will be tackled subsequently with the problem of assessing the reliability of diagnostic measures.
Any numeric approach of dealing with rare events inevitably remains an ill defined or 'ill-posed' problem that needs additional information for a reasonably satisfying solution. Ways to ease this situation can be found in utilizing additional information, also commonly called prior knowledge, that might be introduced via the Bayesian inference or by regularization algorithms. Simplified models will demonstrate how to apply such tools.
As a consequence, there are ways helping to avoid unexpected ad 'surprises' by taking adequate measures in due time upon the correct perception of certain indications.