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The tensile behavior of strain-hardening cement-based composites (SHCC) is usually investigated on macroscopic scale by means of direct tension tests or bending tests. Additionally, the micromechanical properties of the composites are often described based on single fiber tension and pull-out tests. Such investigations, performed both on macroscopic and microscopic scales, are based on ‘classical’ force and displacement measuring techniques. Advanced test methods such as digital image correlation (DIC) and acoustic emission analysis (AE) may facilitate the identification and the analysis of the failure mechanisms in SHCC, which is important for both monitoring loaded SHCC elements and
further material development and optimization. In this study, these two techniques are combined to characterize the failure mechanisms of three different types of SHCC in direct tension tests. The results are related to data of stress and strain measurements. It is shown that DIC provides detailed spatially resolved and stress related strain measurements. Furthermore, it is demonstrated that AE allows for the localization of active cracks, quantification of the damage accumulation under increasing stresses, and characterization of the dominant crack bridging mechanisms and failure modes observed in the different types of SHCC.
Typically, the near-eutectic Al-Si alloys consist of highly interconnected three-dimensional network of the eutectic Silicon (Si) and intermetallics embedded into Aluminium (Al) matrix. For further improvement of the mechanical properties of such alloys, often, one single ceramic reinforcement phase, e.g. silicon carbide (SiC) or aluminium oxide (Al2O3) in the form of fibres or particles is added. However, hybrid reinforcements (fibres and particles) can further improve wear resistance and fracture toughness, and additionally, reduce anisotropy of the material. The engineering of metal matrix composites (MMC) for specific application requirements benefits from a comprehensive knowledge of the failure behaviour. Therefore, damage evolution under compression was investigated on:
- pure near-eutectic AlSi12CuMgNi matrix alloy
- type I: matrix reinforced with random-planar oriented Al2O3 short fibres (15 vol.%)
- type II: matrix reinforced with random-planar oriented Al2O3 short fibres (7 vol.%) and additional SiC particles (15 vol.%)
The analysis of damage mechanism was carried out in two rather independent but complementary studies. First, selected sister samples of every material were exposed to quasi-static compression (traverse control). The compression tests were interrupted at different strain levels. Miniature cylinders with a diameter of 1mm were extracted from the pre-strained samples and investigated by synchrotron computed tomography (SX-µCT) with a spatial resolution of about 0.7 µm. For the pure matrix alloy, microcracks are confined to the intermetallic particles and to the eutectic Si, hence no damage was observed in the Aluminium. The composite type II revealed a more effective strain accumulation (less damage) than type I at low plastic strain (up to 5 %), but a more catastrophic damage development due to cracking of the SiC clusters at higher strain levels.
The second approach to study the damage initiation and accumulation in the materials subjected to compressive load was Acoustic Emission (AE) analysis. In this case the in-situ monitoring of the acoustic emission signal was performed during compression tests on specimens with dimension of several mm. For all three material types, AE activity set at 2% strain. Differences in AE behaviour of the three materials was proven based on AE hitrate, signal peak amplitudes as well as weighted peak frequencies (WPF). Future work focuses on combination of AE and SX-µCT aiming for more detailed knowledge on damage mechanism of metal matrix composites.