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A round robin test on flash thermography was organized within the scope of a standardization research project. This test gives information on reliability, comparability and efficiency of different testing situations. Data recorded on metal and CFRP test specimens with flat bottom holes (FBH) were analysed by evaluating the detectability and by calculating the signal-to-noise ratio (SNR) of the defect signatures as a function of defect parameters. For the investigation of the influence of material properties on the spatial resolution as well as on penetration depth, test specimens made of steel and copper with crossed notches and a notch ramp were constructed and investigated. Here, the minimum resolvable notch distance and the maximum detectable depth of the ramp were analysed.
The determination of the blast protection level of civil engineering buildings components
against explosive effects represents a topic of crucial importance, in current practice. However, some key aspects of blast resistant structures design have been only marginally considered in the last decade, and currently still require appropriate regulations. This is especially true in the case of windows and facades, where the intrinsic material brittleness is the major influencing parameter for blast-resistant assemblies. While blast assessment of buildings and systems is usually achieved by means of experimental investigations, as well as numerical simulations, general regulations and guidelines are currently missing.
In this regard, the European Reference Network for Critical Infrastructure Protection (ERNCIP) Thematic Group “Resistance of Structures to Explosion Effects” attempts to develop guidelines and recommendations aimed to harmonise test procedures in experimental testing of glass windows under blast, as well as standardized approaches for their vulnerability assessment via numerical modelling. In this paper, major Thematic Group outcomes and next challenges are briefly summarized.
Due to the market needs on steel for high demanding applications non-destructive methods for the determination of steel cleanliness using ultrasound have to be adapted to increase sensitivity respectively.
The basic idea is that the new standard proposal should follow the basic line outs from SEP 1927 and ASTM E588. Additional to these relatives the standard should be open to different types of specimen and inspection frequencies to cover a wide range from bars, rings and plates as well as different inspection sensitivities. For an enhance in resolution the standard draft focuses on immersion focal beam probes which should be selected according to the geometry of the specimen. The selection should be proved with the aid of simulation tools. The frequency shall be at least 10 MHz. For specimen thicknesses of less than 6 mm a frequency of at least 25 MHz shall be used.
Calibration procedures had to be improved significantly compared to the old standards to allow proper sizing of indications. Therefore calibration procedures shall take signal processing into account. For detailed evaluation of the amplitude dependency and for calibration a reference block with a sufficient number of reflectors has to be used. The recorded echo height shall be directly transferred into an equivalent disc shaped reflector EDSR by a distance amplitude curve.
The novelty in this standard draft will be that based on 3D measurements and 3D evaluation the amplitude criterion of an indication becomes just one among some other criteria. This standard takes the signal amplitude, signal amplitude distribution and signal travel time for classification into account.
The standard draft will be open to the definition of the volume to be investigated to be set by the user. This will make evaluation more comparable to other methods because the inspected area has to be user defined.
We recommend CEN/TC 138 to decide on a work item for this proposal to become an EU and an ISO standard using Vienna agreement.
The research leading to these results has received funding from the European Union's Research Fund for Coal and Steel (RFCS) research programme under grant agreement n° RFSR-CT-2013-00014.
The accumulation of plastics leaked into the environment achieve a high perception in the last years. It is uncontroversial that often an uncontrolled, high consumption of plastic products and a poor waste management resulted in plastic findings all over in the environment. However, less is known about the relevant pathways and fate of plastic in the environment. Especially plastic fragments smaller 5 mmm, so called microplastics, achieve a high attention, because their amount and risks arising from these fragments are still unknown. The basic mechanisms of plastic or more precise, of different polymer degradation processes are often not considered, resulting in unrealistic statements.
For generation of fundamental understanding of this problem we developed in the last years a fast thermoanalytical method for identification and mass quantification of microplastics in complex samples. The presentation will also give a short introduction about polymer degradation.
The main objectives of the new EMPIR project nPSize are to establish EU capability of traceable measurement of NP size and shape, lower uncertainties of NP size measurement by developement of new nano-CRMs, new models (physical and machine learning), 3D method combination, and also by new ISO and CEN standards on accurate NP size measurement and guidance and knowledge transfer. The envisaged outcomes of the project will be presented and their suitability will be discussed to be taken over as pertinent contributions to normative projects within CEN/TC 352 Nanotechnologies.