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Paper des Monats
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To better understand the dynamics in hazardous environments, gas distribution mapping aims to map the gas concentration levels of a specified area precisely. Sampling is typically carried out in a spatially sparse manner, either with a mobile robot or a sensor network and concentration values between known data points have to be interpolated. In this paper, we investigate sequential deep learning models that are able to map the gas distribution based on a multiple time step input from a sensor network. We propose a novel hybrid convolutional LSTM - transpose convolutional structure that we train with synthetic gas distribution data. Our results show that learning the spatial and temporal correlation of gas plume patterns outperforms a non-sequential neural network model.
Simulating a Gas Source Localization Algorithm with Gas Dispersion Produced by Recorded Outdoor Wind
(2023)
This paper reports the use of the first gas dispersion simulator capable of introducing large wind fluctuations into simulations. The proposed simulator enables testing of a modification made to a gas source localization algorithm in a realistic scenario in order to study how the change affects it. Gas source localization in an outdoor environment is a challenging task mainly due to the complexity of the gas spread caused by the unpredictable nature of constantly changing wind. Therefore, a novel use of outdoor wind in developing a gas source localization system by simulation is presented in this paper. To consider the characteristic of sudden but large and unpredictable changes in wind direction, we propose to use recorded outdoor wind to simulate a realistic outdoor gas dispersion which has been done for the first time to the best of our knowledge. With the use of this simulator, we have tested a modification to a mobile robot-based gas source localization algorithm. Multiple simulations of the modified and the original particle filter-based algorithm have been done to study the effect of the tested modification. The results showed that a small difference in the algorithm can greatly impact the results. From this study, we show that the use of simulation consisting of the necessary traits to evaluate outdoor gas source localization, has the potential to accelerate the development of a reliable localization system.
Wasserstoff erfüllt die zentrale Rolle für die Umwandlung der bisherigen fossil-basierten Energieerzeugung und -nutzung auf eine dekarbonisierte, nachhaltige Form. Dazu muss der Wasserstoff erzeugt, gespeichert, transportiert werden, bevor er wieder der Nutzung zugeführt wird. Hierzu sind entlang der gesamtem Prozesskette Wasserstofftechnologien notwendig, die einen sicheren Betrieb erfordern. Hierbei kommt dem schweißtechnischen Anlagen- und Behälterbau wesentliche Bedeutung zu, insbesondere (aber nicht ausschließlich) für Speicherung und Transport des Wasserstoffes. Der vorliegende Beitrag gibt einen kurzen Überblick, wo und wie die konventionelle Schweißtechnik hierzu wichtige Beiträge leistet. Die additive Fertigung, also das „Drucken“ von Bauteilen wird dabei zunehmend wichtiger, entlang der gesamtem Prozesskette der Wasserstofftechnologien. Gleichwohl darf nicht unterschätzt werden, dass auch wesentlicher Bedarf an der Erweiterung und teilweiser Neufassung von bestehenden Regel- und Normenwerken besteht.
The current understanding of the carbonation of alkali-activated concretes is ham-pered inter alia by the wide range of binder chemistries used. To overcome some of the limitations of individual studies and to identify general correlations between their mix design parameters and carbonation resistance, the RILEM TC 281-CCC working group 6 compiled carbonation data for alkali-activated concretes and mortars from the literature. For comparison purposes, data for blended Portland cement-based concretes with a high percentage of SCMs (≥ 66 % of the binder) were also included in the database. A preliminary analysis of the database indicates that w/CaO ratio and w/b ratio exert an influence on the carbonation resistance of alkali-activated concretes but, contrary to what has been reported for concretes based on (blended) Portland cements, these are not good indicators of their carbonation resistance when considered individually. A better indicator of the carbonation resistance of alkali-activated concretes under conditions approxi-mating natural carbonation appears to be their w/(CaO + Na2O + K2O) ratio. Furthermore, the analysis points to significant shortcomings of tests at elevated CO2 concentrations for low-Ca alkali-activated concretes, indicating that even at a concentration of 1 % CO2, the outcomes may lead to inaccurate predictions of the carbonation coefficient under natural exposure conditions.
Since there is a continuously growing demand for complex, frequently heavy-sectioned spheroidal graphite cast iron (SGI) castings it is worth paying attention to the chunky graphite (CHG) degeneration which may occur under certain technological circumstances. Although a reference line for preventive actions in terms of general metallurgical and process measures could be drawn to avoid CHG in heavy-sectioned ferritic SGI castings, a broad majority of experts claim the avoidance of CHG in heavy sections cannot yet be rated a hundred percent process safe. A major reason may be seen in the fact that a universal, generally accepted explanation of CHG formation and growth has not yet been established, although several theories have been proposed. Nevertheless, metallurgical aspects are not in the focus of this paper.
This paper is about the current state of methods to detect CHG in SGI on the laboratory and component scales. Capabilities and limits of different metallographic, fractographic and non-destructive computer tomographic methods to recognize and quantify CHG are discussed. With respect to the characteristic fili-gree three-dimensional string-like, multi-branched CHG structure, which is non-isometric and non-dispersed, serious implications on the possibility to quantitatively characterize the amount of CHG must be considered.
In contrary to the metallurgical aspects, the knowledge about the impact of CHG on the materials and com-ponents properties is still surprisingly limited. Therefore, special emphasis of this paper is on the impact of CHG degeneration on the properties of ferritic SGI. Experimental results are reviewed to illustrate the effect of CHG on mechanical strength and ductility properties as well as fracture mechanics properties in terms of crack resistance and fracture toughness.
The present situation is characterized by discussions and uncertainty about the acceptance or rejection of SGI components containing CHG. Addressing this, conclusions from the materials engineering point of view are drawn for quality control, a safe operational strategy in the foundry and component safety.
The European Commission adopted an EU Energy Label for smartphones and tablets in June 2023. For the first time, the EU Energy Label will depict, among energy efficiency, also a reparability score, battery endurance, battery lifetime, drop resistance and dust and water ingress protection.
However, does the multitude of parameters bear the risk to confuse consumers instead of triggering environmentally sustainable purchase decisions? In a survey in Germany, consumers were asked to make a choice when the label does not clearly identify the environmentally better product. Instead, energy efficiency has to be valued against reparability, reliability against energy efficiency, and reparability against reliability. The sustainability lever of the different aspects is not the same, as e.g. lifetime extension has a much more positive environmental impact than energy efficiency in case of mobile devices. Therefore, the question remains, whether consumers intuitively make the right choice. Results of the survey indicate that consumers interpret the complex label in the desired manner and value those aspects higher, which indeed have a more positive effect on the environment.
Der Beitrag beschreibt die Entwicklung eines neuartigen in situ Nachweisverfahrens zur Beurteilung des Feuerwiderstandes von bestehenden Stahlkonstruktionen mit gealtertem reaktivem Brandschutzsystem (RBS). Derzeit ist ein solcher Nachweis ausschließlich anhand eines Bauteilbrandversuchs möglich. Hierzu muss ein Bauteil aus der Bestandskonstruktion entnommen und einer zerstörenden Brandprüfung unterzogen werden. In Zusammenhang mit der Dauerhaftigkeitsbewertung von RBS für Zeiträume von mehr als 10 Jahren besteht in der Praxis vermehrt der Bedarf an einem minimal invasiven Prüfverfahren, mit dessen Hilfe sich direkt am Bestandsbauwerk die tatsächlich vorhandene Leistungsfähigkeit des gealterten RBS überprüfen lässt. Durch einen erfolgreichen Funktionsnachweis wäre eine Weiternutzung der Bestandkonstruktion bei Aufrechterhaltung des bestehenden Sicherheitsniveaus möglich.
Duplexstähle besitzen ein zweiphasiges Gefüge und werden aufgrund ihrer verbesserten Schweißeignung gegenüber den Vollausteniten häufig im Anlagen- bzw. Apparatebau eingesetzt. Aufgrund der hohen Abkühlgeschwindigkeit und dem Abbrand von Legierungselementen kommt es zu einer Ferritisierung des Schweißguts und damit zu einer Degradation der mechanischen Eigenschaften. Zur Vorhersage des Phasenverhältnisses im Schweißgut wird das WRC1992-Diagramm genutzt. Dieses Diagramm zeigt einige Ungenauigkeiten und benötigt zur genaueren Vorhersage der Phasenverhältnisse eine Überarbeitung. Um den Einfluss einzelner Elemente auf das Schweißnahtmikrogefüge besser zu verstehen, wurden drahtförmige Schweißzusatzwerkstoffe mit dem Ferrit-Bildner Nb und dem Austenit-Bildner Cu beschichtet und für Schweißungen verwendet. Die Messmethode der Laser-induzierten Plasmaspektroskopie (LIBS) bietet hier eine gute Möglichkeit der in situ Überwachung der chemischen Konzentrationen, während des WIG-Schweißens von Duplexstählen. Die LIBS-Messergebnisse, konnten mit der Ferritnummer und der Schweißnahtmikrostruktur korreliert werden.
Einfluss der Schweiß- und Prüfparameter bei der Heißrissbewertung hochfester Schweißzusatzwerkstoffe
(2023)
Die Heißrissneigung beim Schweißen kann mittels einer ganzen Reihe von Prüfverfahren ermittelt werden. Eine etablierte Methode ist die sogenannte Varestraint-Prüfung, welche auch an der Bundesanstalt für Materialforschung und -prüfung (BAM) als modifizierter Varestraint/Transvarestraint-Test (MVT) zum Einsatz kommt. Die Ergebnisse von Varestraint-Prüfungen hängen jedoch stets in unter-schiedlichem Maße von der individuellen Prüfmaschinenauslegung und den verwendeten Prüfparametern ab. Dies kann zu einer uneinheitlichen Bewertung des Rissverhaltens führen, wenn die Risslänge konventionell als Kriterium für die Rissneigung herangezogen wird. Scheinbare Abhängigkeiten von Prozessparametern erschweren dann die Interpretation der Ergebnisse. Eine neuartige Bewertungsmethodik entkoppelt den Maschineneinfluss vom Materialverhalten und verwendet die Dehnrate als Risskriterium.
Since several years, magnetic sensor elements are available in fully flexible architectures that often reveal identical sensing properties, compared to their rigid counterparts, while being bent severely and repeatedly. Nowadays, a variety of magnetic senor principles, including well known Hall, AMR and GMR but also more exotic PHE and AHE sensors were demonstrated on such flexible platforms. The novel properties of being thin, lightweight, shapeable, and wearable enable magnetic sensory systems to be utilized in vicinities and conditions that are inaccessible for rigid and microchip-based sensors.
BAM acts as authority and for service in safety assessment of packages for transport and storage of radioactive materials. We offer extensive test capabilities and application of analytical methods for design verification and simulation for all types of packages for the transport and storage of radioactive materials according with the international IAEA Regulations for the safe transport and for national storage acceptance criteria. BAM operates several test facilities for drop and stacking testing, leak testing and thermal testing. The large drop test tower allows dropping full-scale specimens up to 200,000 kg in any drop orientation as requested. The comprehensive test facilities combined with long-term experience, newest equipment and measurement devices according to the latest state-of-the-art technology ensures realisation of complex test campaigns for package safety evaluation.
Beyond that, non-destructive and destructive material test devices and experts are available. Equipment and application of all kinds of typical measurement categories can be offered for testing campaigns.
In recent years we performed testing of full-scale type B package models with complex handling and preparation procedures. The results were contributed for different package design approval procedures. Type A packages mainly designed for medical related transport purposes, were continuously tested according to the transport regulations over recent years as well. Moreover, we work on research topics with relevance to package safety. The mechanical behaviour of lid closure systems under transport and storage conditions and the thermal behaviour of impact limiters were recently of special importance for the assessment competencies of BAM and were investigated under use of our test facilities.
The paper describes the test facilities and capabilities for package design safety evaluation at BAM and shows examples from our recent work.
The soil-foundation-structure interaction is always important when building vibrations due to train passages have to be considered. The frequency range for train vibrations is up to 100 Hz. Normally, soft surface soils are crucial so that the wavelength can be much smaller than the foundation dimensions. Three topics are of interest for the prediction and the under-standing of building vibrations. 1. The „kinematic interaction“ or the „added foundation ef-fect“, which is calculated either by the combined boundary-element finite-element method or by the wavenumber domain method, results in a reduction of the free-field vibration. The stiff-ness of the foundation resists the wave deformation, plates and walls for horizontally propa-gating waves or piles for vertically incident waves. 2. The „inertial interaction“ or the „added building effect“ yields an amplification around the vertical building resonance, which may be a rigid mode on the compliant soil or a flexible mode for high-rise buildings, and a reduction at higher frequencies. This has been analysed by detailed finite element models of apartment and office buildings. 3. Base isolation is a method to further reduce building vibrations. It is important to know the soil-foundation impedance for the possible reduction, as well as the correct building impedance. A high-rise building cannot be considered as a rigid mass model. It has a frequency-dependent behaviour with longitudinal waves travelling from the founda-tion to the top of the building which include the effect of floor vibrations. Experiences from building projects in Vienna, Frankfort and Berlin will give some additional results for the ex-citation from tunnel lines, the kinematic response of pile foundations, and the inertial re-sponse of the flexible multi-storey buildings.
The resonances of railway bridges have often been analysed for short bridges under periodical high-speed trains, for simply supported one-span bridges, for the fundamental bridge mode, and by time-domain analyses. Many time-consuming calculations have been performed to establish simplified rules for standards. In this contribution, the passage of different (existing, new and hypothetic) trains over different bridges will be analysed in frequency domain by using three separated spectra with the purpose to get a better physical insight in the phenomena. At first, the excitation spectrum of the modal forces is built by the mode shape and the passage time of the train over the bridge. The second spectrum is the frequency response function of the bridge which include the modal frequency, damping and mass. The third part is the spectrum of the axle sequence of an arbitrary train which is not limited to periodical or specific (conventional, articulated, regular or standard) trains and which does not include any bridge parameters. The final solution in frequency domain is obtained as the product of these three complex, strongly varying spectra for the dominating bridge mode or in general as the sum of these products over all relevant bridge modes. The time domain solution is obtained via the inverse Fourier transform, and the resulting time histories have been successfully compared with some measurement results. The method is applied to the vertical and torsional modes of a mid-long 1-span bridge on elastomeric bearings under standard train speeds, and to a long multi-span integral bridge under long periodical freight trains. Different resonance and cancellation effects have been found for systematically varied train speeds according to the axle sequence of the whole train which is dominated by the two locomotives in that case. To be more specific, the first torsional mode of the mid-span bridge is excited for a train speed of 100 km/h whereas the second bending mode is excited for a train speed of 160 km/h. In both cases, the other mode is suppressed by the minima of the axle-distance spectra. In addition, the case of the German high-speed train ICE4 and the very high-speed hyperloop case will be discussed briefly. In general, it is shown that resonance effects are also worth to be studied for freight and passenger trains with lower speeds.
Train-induced ground vibrations - the emission and transmission from tunnel and surface lines
(2023)
Train-induced ground vibrations are quite different for tunnel and surface lines. The excitation of the track and ground vibration by the vehicle-track-soil interaction maybe influenced by the stiffer track support of the tunnel invert. The excited waves are propagating on a different path compared to the surface line. The wave propagation in the interior of the soil is calculated by a wavenumber integral in a similar way as the propagation along the surface and a general reduction of < 0.5 has been found. An additional reduction has been found because of the missing Rayleigh wave. The different excitation of tunnel lines is analysed theoretically by the combined finite-element boundary-element method and some results about the influencing tunnel and soil parameters will be shown. Measurements have been made at the Mühlberg-Tunnel in Germany. The vibrations of the train, the track and the soil have been measured simultaneously at the tunnel and a nearby surface line. Spectra will be shown for different train speeds between 60 and 160 km/h. A clear reduction effect for the tunnel line compared to the surface line has been observed in a specific (train-speed-dependent) frequency range. This agrees well with the observations of other research institutes. The mid-frequency tunnel-surface reduction seems to be a consequence of the stiffer track structure which leads to a wider distribution of the axle loads. Therefore, the axle impulses due to the train passage are longer and have a lower frequency content. This will have an effect on the ground vibrations at some distance which are present in case of an irregular transmission path through a ballast and soil with varying stiffness. A similar reduction effect can also be found for other track forms where the axle impulses are distributed on a longer track segment, for example slab tracks, tracks with under ballast plates, under ballast mats or under sleeper pads.
QI-Digital is a joined project aiming at digitalising Quality Infrastructure (QI) processes involving standardization, conformity assessment, accreditation, metrology, and market surveillance [1]. Federal institute of material research and testing (BAM) is working on the creation of a digital calibration certifi-cate (DCC) to achieve digital metrological traceability and conformity assessment. The utilisation of machine readable and executable DCCs in the XML format is demonstrated on an example of a tem-perature measurement at a hydrogen refueling station. The certificates will be retrieved and analysed automatically at a Process Control System or at a Digital Twin.
Ultrasonic coda wave interferometry can detect small changes in scattering materials like concrete. We embedded ultrasonic transducers in the Gänstorbrücke Ulm, a monitored road bridge in Germany, to test the methodology. Since fall 2020, we've been monitoring parts of the bridge and comparing the results to commercial monitoring systems. We calculate signal and volumetric velocity changes using coda waves, and long-term measurements show that the influence of temperature on strains and ultrasound velocity changes can be monitored. Velocity change maps indicate that different parts of the bridge react differently to environmental temperature changes, revealing local material property differences. A load experiment with trucks allows calibration to improve detectability of possibly damaging events. Our work focuses on measurement reliability, potential use of and distinction from temperature effects, combination with complementary sensing systems, and converting measured values to information for damage and life cycle assessment.
Mikrolegierungselementen, wie Nb und Ti sind für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgrenze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung dieser Stähle geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Mikrolegierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Eine unerwünschte Eigenschaft ist dabei die Erweichung der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung.
Vor diesem Hintergrund werden im Rahmen eines DFG-Vorhabens systematisch Mikrolegierungs-routen mit variierenden Ti- und Nb-Gehalten des hochfesten und vergüteten Feinkornbaustahls S690QL untersucht. Dazu wird das MAG-Schweißen mit modifizierten Sprühlichtbogen verwendet, welches durch hohe Abschmelzleistung gekennzeichnet ist und schmalere Nahtöffnungswinkel (α = 30°) ermöglicht. An Dreilagen-Schweißungen wird der Effekt der metallurgischen Zusammensetzung in Kombination mit hoher Wärmeeinwirkung auf die Ausbildung einer kritischen WEZ-Gefügezone mit Erweichung und/oder exzessiver Aufhärtung untersucht. Ein besonderes Augenmerk wird auf die Phasenumwandlungen und das Ausscheidungsverhalten im Gefüge der Wärmeeinflusszone gelegt. Neben umfangreichen metallographischen Untersuchungen einzelner WEZ-Bereiche wurden, unter Variation der chemischen Zusammensetzung,
thermodynamische Phasenberechnungen mittels Thermo-Calc durchgeführt. Hierdurch wird ein Verständnis zur Phasentransformation und Ausscheidungswachstum und -auflösung während des Schweißens in Abhängigkeit von Temperatur und Abkühlbedingungen geschaffen. Das Ziel ist es, den Einfluss der Wärmeeinwirkung auf die Gefügeausbildung in der WEZ und dessen mechanischer Eigenschaften zu analysieren. Insbesondere wird hier auf die Auswirkung der unterschiedlichen Mikrolegierungskonzepte (Ti oder Nb) geachtet.
When reassessing existing concrete bridges, the challenge is often to obtain missing or incomplete information on the internal structure. In particular, the number and position of the existing reinforcement as well as the geometric dimensions of the components are of interest. Non-destructive testing methods, like radar or ultrasound, which work on the basis of the pulse-echo method, have been established for this purpose, as they only require access to the component from one side. The measurement data recorded on the structure require pre-processing to be able to reproduce the internal structure geometrically accurately. Besides different steps of data processing, the geometrical reconstruction of the measured data based on the Synthetic Aperture Focusing Technique (SAFT) is state of the art today. In this paper, the technical possibilities of the ultrasonic echo method are presented based on measurements in the laboratory and on a real bridge structure. The precision of the reconstruction and its limitations are shown. In addition to the state of the art SAFT technique, open questions and the latest research approaches, such as imaging by reverse time migration (RTM) including initial results are discussed.
Multi-sensory monitoring and ultrasound for quality assurance at underground sealing structures
(2023)
Within the safety concepts of underground disposal sites of nuclear waste, engineered barriers play an important role. As these sealing structures have high demands concerning integrity, we aim at advancing the available construction materials, monitoring, and inspection techniques within the project SealWasteSafe. A specifically developed alkali-activated material is compared to classical salt concrete. A comprehensive multi-sensory monitoring scheme is used at 150-340 l specimens to monitor setting and hardening of both materials. All sensors are demonstrated to resist the highly alkaline environments. Besides cabled and wireless temperature and humidity of the materials, strain variations using fibre optic sensors and acoustic emissions are recorded over periods of at least 28 days, partly for more than eight months. After hardening of the specimens, further nondestructive evaluations using ultrasonic echo and thermographic measurements are conducted.
Preliminary results proof the suitability of the tested sensors and clearly highlight differences between the tested materials. Particularly, the newly developed alkali-activated material shows lower acoustic emission activity indicating less cracking activity. Additionally, unique ultrasonic methods will enable better images of potential internal objects and cracks at in-situ sealing structures. A largescale ultrasonic system is optimised to reliably detect objects at a depth exceeding 9 m while still obtaining a good resolution. Modelling studies show the potential of further increasing the distance between individual transducer arrays. Additionally, a new ultrasonic borehole probe using phased arrays allowing for beam focussing is constructed and tested. Laboratory measurements at a halfcylindrical concrete specimen coincide well with the previous modelling. In total, the presented safe materials, detailed monitoring approaches and ultrasonic quality assurance methods will help to obtain safe sealing structures within salt as a host rock. The concepts can partly be transferred to sealing structures in alternative host rocks and will also be valuable for non-nuclear waste repositories.
Beginning in 1976 the former iron ore mine Konrad was geologically investigated concerning its suitability as a location for a German final repository for low and intermediate level waste. After a comprehensive licensing procedure it was approved and is now being prepared and equipped for the planned start of storage in 2027. At the end of the 1980s, the requirements for waste containers for storage in this repository were defined for the first time on the basis of an incident analysis of the on-site handling procedures, beginning with the unloading of the packages after the arrival at the site up to the final positioning in the underground storage galleries. A 5-meter drop onto the rock ground of the mine was identified as the covering case for high mechanical requirements (ABK II container class). In contrast to the 9-meter drop according to the IAEA Regulations for the Safe Transport of Radioactive Material, the 5-meter drop is performed onto a hard but not essentially unyielding target. The container is typically not protected by an impact limiter. The requirements for a potential test facility are described in the regulations for the Konrad repository. The mechanical strength of the target is defined as a concrete strength equivalent to the identified properties of the rock ground of the mine.
Since 1991 BAM has consistently used precast reinforced concrete slabs as target for drop tests in the framework of licensing procedures as well as in research projects. While the original design fulfilled the requirement for the integrity of the concrete slab in most cases, it failed when drop tests onto an edge of a container were performed. A redesigned concrete slab developed in a research project and suggested as a reference target in 2009 has been successfully used in Konrad licensing procedures since then.
The paper gives a brief overview of the historical development and it describes BAM’s efforts and approaches to continuously guarantee a concrete slab of defined quality and to provide a test setup for valid drop tests from the applicants and the authorities view.
The prevention of brittle fracture of spent fuel claddings during long-term dry interim storage is based on experimental investigations, numerical analyses and assessment methods for predicting the mechanical behavior and determining limiting conditions. The ring compression test (RCT) is an established experimental method for characterizing cladding material. Test results for various high-burnup pressure water reactor zirconium-based fuel cladding alloys (e.g., ZIRLO®, M5®) are publicly available. To reduce the effort associated with irradiated samples in hot cells, it is helpful to perform studies on unirradiated surrogate cladding material. Based on such experimental data, load-displacement curves were numerically analyzed for selected cladding materials. In the presence of radial hydrides, a sample may suddenly fail by fracture even at small deformations. Noticeable load drops in the RCT occur associated to unstable crack propagation through the radial hydride network. The failure mechanism is quasi-cleavage in the hydrides and micro-void nucleation, growth, and coalescence in the zirconium matrix, with ductile tearing patches connecting neighboring hydrides. The failure process was simulated by cohesive zones controlled by the fracture energy and the cohesive strength. A modeling approach is presented in which the radial hydride morphology is taken into account. Based on the developed fracture mechanics approach with cohesive zone modeling, not only the deformation behavior but also the failure behavior of irradiated as well as unirradiated claddings with radial hydrides under RCT loading conditions can be adequately described.
The number of cars which use a battery for propulsion, like BEV (battery electric vehicle) or PHEV (plug-in hybrid electric vehicle), is increasing. Following, the probability of these car types being involved in car accidents will increase. In a worst-case accident scenario, the installed batteries could go under thermal runaway (TR). A TR could be initiated by various causes, e.g., high temperatures from outside, mechanical damage of the cells/modules/batteries or internal and external short circuits. During such an event, large amounts of heat and toxic and/or flammable gases are released. This poses a great hazard to people and property in the immediate vicinity. The paper describes a large-scale test series on the lithium-ion battery TR consequences of automobile cells and modules up to E = 6.85 kWh. Near field temperatures of ΔT > 800°C in a distance of l = 2 m were measured. During an overcharge test, fragment throwing distances of l > 30 m were detected. Subsequent gas explosions of the released gases were documented. Hydrogen fluoride (HF) was measured in all tests, from cell to module. The highestmeasured concentration was cHF = 76 ppm, which is significantly higher than the 30-min-level for AEGL 2 (acute exposure guideline level 2). Based on the experimentally determined consequences, concrete measures for the accident analysis are subsequently drawn.
Normung und Standardisierung in der zerstörungsfreien Prüfung finden auf nationaler, europäischer und internationaler Ebene statt. Durch die Übernahme von Leitungsfunktionen in diesen Gremien kann ein deutlicher steuernder Einfluss auf Themen und Inhalte der Normen genommen werden. Unabdingbar für den Erfolg ist zusätzlich das persönliche Engagement der Fachexpert*innen in den nationalen Gremien und den europäischen und internationalen Arbeitsgruppen. Denn wer nicht normt wird genormt und muss letztlich Regeln verwenden, die andere entsprechend ihrer eigenen Interessen gestalten. Voraussetzung für die Teilnahme in europäischen und internationalen Normungsgremien ist die Mitwirkung in den entsprechenden nationalen Spiegelgremien der nationalen Normungsinstitute, welche die europäischen und internationalen Aktivitäten spiegeln und die Fachexperten für die Mitarbeit autorisieren.
Gezeigt werden die relevante Gremienstruktur auf internationaler Ebene (ISO/TC 135 “Non-destructive testing”, ISO/TC 44/SC 5 “Testing and inspection of welds”), auf europäischer Ebene (CEN/TC 138 “Zerstörungsfreie Prüfverfahren”), die Struktur der nationalen deutschen Spiegelgremien, das Zusammenspiel der Gremien, und die Einflussmöglichkeiten.
Im DIN-Normenausschuss Materialprüfung (NMP) wurde das Normungsgremium NA 062-08-28 AA „Qualifizierung von zerstörungsfreien Prüfungen“ reaktiviert. Das Ziel der Reaktivierung ist die Erarbeitung einer Norm für einen standardisierten Prozess zur probabilistischen Bewertung von Prüfverfahren.
In der zerstörungsfreien Prüfung (ZfP) führt die Ermittlung von Mess- / Prüfunsicherheiten von Prüfverfahren, in normativer Hinsicht in Deutschland und Europa, noch ein Schattendasein. Die Norm ISO IEC 17025 und auch der VDA-Band 5 wurden weiter in Richtung Messunsicherheit entwickelt, allerdings führt ihre Anwendung in der ZfP zu Problemen.
Der Arbeitsausschuss NA 062-08-28 AA soll hier den Brückenschlag zwischen Messunsicherheit, objektiver statistischer Bewertung für ZfP-Verfahren und eine weitere Stärkung der probabilistischen Bruchmechanik erreichen. Geplant ist daher die Erarbeitung einer DIN-Norm, welche die Kriterien für eine korrekte Versuchsplanung, ein praktikables Vorgehen zur Bewertung der Prüfergebnisse und die mathematische Überführung in eine Zuverlässigkeitsaussage enthält. Es soll ein Leitfaden erstellt werden, der für ein möglichst breites Branchenspektrum eingesetzt werden kann, unabhängig von den Besonderheiten verschiedener Industriezweige.
Dargestellt werden das relevante Normungsgremium sowie der Hintergrund des zu erstellenden Dokuments.
In recent years, the use of simulation-based digital twins for monitoring and assessment of complex mechanical systems has greatly expanded. Their potential to increase the information obtained from limited data makes them an invaluable tool for a broad range of real-world applications. Nonetheless, there usually exists a discrepancy between the predicted response and the measurements of the system once built. One of the main contributors to this difference in addition to miscalibrated model parameters is the model error. Quantifying this socalled model bias (as well as proper values for the model parameters) is critical for the reliable performance of digital twins. Model bias identification is ultimately an inverse problem where information from measurements is used to update the original model. Bayesian formulations can tackle this task. Including the model bias as a parameter to be inferred enables the use of a Bayesian framework to obtain a probability distribution that represents the uncertainty between the measurements and the model. Simultaneously, this procedure can be combined with a classic parameter updating scheme to account for the trainable parameters in the original model.
This study evaluates the effectiveness of different model bias identification approaches based on Bayesian inference methods. This includes more classical approaches such as direct parameter estimation using MCMC in a Bayesian setup, as well as more recent proposals such as stat-FEM or orthogonal Gaussian Processes. Their potential use in digital twins, generalization capabilities, and computational cost is extensively analyzed.
Die sprunghaft zunehmende Wichtigkeit von FAIR- und Open-Data für die Qualitätssicherung, aber auch für die Nachnutzbarkeit von Daten und den Erkenntnisfortschritt führt zu enormem Flandlungsbedarf in Forschung und Entwicklung. Damit verbunden laufen derzeit vielfältige, ambitionierte Aktionen, z. B. bezüglich der Erstellung von Ontologien und Wissensgraphen. Das Knowhow entwickelt sich rasant, die Ansätze zur Implementation entstehen in verschiedenen Fachwelten bzw. mit
unterschiedlichen Zielsetzungen parallel, so dass recht heterogene Herangehensweisen resultieren.
Diese Veröffentlichung fokussiert auf Arbeiten, die derzeit als möglichst ganzheitlicher Ansatz für Materialdaten im Rahmen der Digitalisierungsinitiative „Plattform MaterialDigital" vorangetrieben werden. Die Autoren bearbeiten baustoffbezogene Aspekte im Verbundprojekt „LeBeDigital - Lebenszyklus von Beton". Zielsetzung ist die digitale Beschreibung des Materialverhaltens von Beton über den kompletten Herstellungsprozess eines Fertigteils mit einer Integration von Daten und Modellen innerhalb eines Workflows zur probabilistischen Material- und Prozessoptimierung.
Es wird über die Vorgehensweise und die dabei gewonnenen Erfahrungen berichtet, nicht ohne den Blick auf die oft unterschätzte Komplexität der Thematik zu lenken.
FAIR (findable, accessible, interoperable and reusable) data usage is one of the main principals that many of the research and funding organizations include in their strategic plans, which means that following the main principals of FAIR data is required in many research projects. The definition of data being FAIR is very general, and when implementing that for a specific application or project or even setting a standardized procedure within a working group, a company or a research community, many challenges arise. In this contribution, an overview about our experience with different methods, tools and procedures is outlined.
We begin with a motivation on potential use cases for the applications of FAIR data with increasing complexity starting from a reproducible research paper over collaborative projects with multiple participants such as Round-Robin tests up to data-based models within standardization codes, applications in machine learning or parameter estimation of physics-based simulation models.
In a second part, different options for structuring the data are discussed. On the one hand, this includes a discussion on how to define actual data structures and in particular metadata schema, and on the other hand, two different systems for storing the data are discussed. The first one is the openBIS system, which is an open-source Lab notebook and PostgreSQL based data management system. A second option are a semantic representations using RDF based ontologies for the domain of interest.
In a third section, requirements for workflow tools to automate data processing are discussed and their integration into reproducible data analysis is presented with an outlook on required information to be stored as metadata in the database.
Finally, the presented procedures are exemplarily demonstrated for the calibration of a temperature dependent constitutive model for additively manufactured mortar. Metadata schemata for a rheological measurement setup are derived and implemented in an openBIS database. After a short review of a potential numerical model predicting the structural build-up behaviour, the automatic workflow to use the stored data for model parameter estimation is demonstrated.
Gas source localization (GSL) helps mitigate the impact of industrial accidents and natural disasters. While GSL may be dangerous and time-consuming when performed by humans, swarms of agile and inexpensive nano aerial robots may increase the safety and efficiency of gas source localizations. Since the small payloads of nano aerial robots limit the sensing and computing resources, strategies adapted from biological swarms, such as colonies of social insects, are used to coordinate robot swarms. Most swarm GSL strategies are based on the assumption that the maxima of gas concentrations are sufficiently close to the gas sources. However, prior studies have indicated that the occurrence of “bouts”, a metric for the intermittency of gas distributions, may advantageously be used as a more accurate gas source proximity indicator. This paper presents a swarm GSL strategy employing bouts as source proximity indicators and a bio-inspired pheromone system for communication. Nano aerial robots, deployed in this study, act as agents and emit pheromone markers in an artificial environment upon detecting bouts. Leveraging the concept of artificial potential fields, the agents switch between exploiting the knowledge of the swarm by following pheromone gradients and exploring the search space by targeting a random point. The agents are repelled by each other and by walls to avoid collisions. The swarm GSL strategy is implemented into three nano aerial robots and validated in a real-world experiment in an indoor environment with a single gas source. The results indicate that the the swarm GSL strategy presented in this paper is capable of GSL in indoor environments and that the intermittency of gas distributions is a better source proximity indicator than the mean concentration.
This paper presents an automatic damage imaging technique by employing a signal processing approach based on applying hierarchically clustered filters across different domains. The technique involves time-frequency-wavenumber filter banks which are applied sequentially to ultrasonic guided wave (UGW) data. The study is conducted for a single lap joint composite specimen with a special focus on small voids which were formed due to manual adhesive component mixing. UGW data are acquired with a 3D Scanning Laser Doppler Vibrometer (LDV) over the scan area of the bonded plate. UGWs are excited at the central frequency of 100 kHz by a single piezoelectric transducer mounted on the surface of the single plate. Within each domain of time, frequency, and wavenumber, four filters are designed which results in 64 distinct filtered wavefields. From each filtered wavefield, an image is obtained by using root-mean-square (RMS) calculation of the signals. The obtained results are then combined to create a final, improved-resolution image of the scan area. The final image is compared to the image obtained through RMS calculation of full wavefield with interpolation through Delaunay triangulation and the image obtained by X-ray radiography. The results show that the smallest void that could be detected has a diameter of 2.14 mm.
Numerical study on the formation of a bulging region in partial penetration laser beam welding
(2023)
A transient three-dimensional thermo-fluid dynamics numerical model was developed to study the formation of a bulging region in partial penetration laser beam welding. The model accounts for the coupling between the fluid flow, the heat transfer, and the keyhole dynamics by considering the effects of multiple reflections and Fresnel absorption of the laser beam in the keyhole, the phase transitions during melting and evaporating, the thermo-capillary convection, the natural convection, and the phase-specific and temperature-dependent material properties up to the evaporation temperature. The validity of the model was backed up by experimentally obtained data, including the drilling time, the weld pool length, the local temperature history outside the weld pool, the process efficiency, and a range of metallographic crosssections.
The model was applied for the cases of partial penetration laser beam welding of 8 mm and 12 mm thick unalloyed steel sheets. The obtained experimental and numerical results reveal that the bulging region forms transiently depending on the penetration depth of the weld, showing a tendency to transition from a slight bulging to a fully developed bulging region between penetration depths of 6 mm and 9 mm, respectively.
A three-dimensional numerical model was developed to accurately predict the steady-state weld pool shape in full penetration laser beam welding. The model accounts for the coupling between the heat transfer and the fluid dynamics by considering the effects of solid/liquid phase transition, thermo-capillary convection, natural convection, and phase-specific and temperature-dependent material properties up to the evaporation temperature. A fixed right circular cone was utilized as a keyhole geometry to consider the heat absorbed from the laser beam. The model was used to analyze the influence of the thermodynamic activity of solutes and turbulence on the weld pool shape. A mesh sensitivity analysis was performed on a hybrid mesh combining hexahedral and tetrahedral elements. For the case of full penetration laser beam welding of 8 mm thick unalloyed steel sheets, the dependence of the weld pool shape on the surface-active element sulfur was found to be negligible. The analysis of the results showed that a laminar formulation is sufficient for accurately predicting the weld pool shape since the turbulence has a minor impact on the flow dynamics in the weld pool. The validity of the numerical results was backed up by experimental measurements and observations, including weld pool length, local temperature history, and a range of metallographic crosssections.
The contactless magnetohydrodynamic technology has been considered as a potential and promising method to improve the weld qualities of deep penetration laser beam welding. In this paper, numerical investigations are conducted to study the influence of the auxiliary oscillating magnetic field on the porosity suppression in laser beam welding of 5754 aluminum alloy. To obtain a deeper insight into the suppression mechanism, a three-dimensional transient multi-physical model is developed to calculate the heat transfer, fluid flow, keyhole dynamic, and magnetohydrodynamics. A ray tracing algorithm is employed to calculate the laser energy distribution on the keyhole wall. A time-averaged downward Lorentz force is produced by an oscillating magnetic field. This force acts in the molten pool, leading to a dominant downward flow motion in the longitudinal section, which blocks the bubble migration from the keyhole tip to the rear part of the molten pool. Therefore, the possibility for the bubbles to be captured by the solidification front is reduced. The electromagnetic expulsive force provides an additional upward escaping speed for the bubbles of 1 m/s ~ 5 m/s in the lower and middle region of the molten pool. The simulation results are in a good agreement with experimental measurements. Based on the results obtained in this study, a better understanding of the underlying physics in laser beam welding enhanced by an auxiliary oscillating magnetic field can be provided and thus the welding process can be further optimized reducing the porosity formation.
Numerical analysis of ultrasonic vibration enhanced friction stir welding of dissimilar Al/Mg alloys
(2023)
The ultrasonic vibration enhanced friction stir welding (UVeFSW) process has unique advantages in joining dissimilar Al/Mg alloys. While there are complex coupling mechanisms of multi-fields in the process, it is of great significance to model this process, to reveal the influence mechanism of ultrasonic vibration on the formation of Al/Mg joints.
In this study, the acoustic-plastic constitutive equation was established by considering the influence of both ultrasonic softening and residual hardening on the flow stress at different temperatures and strain rates. And the ultrasonic induced friction reduction (UiFR) effect on friction coefficient in different relative directions at the FSW tool-workpiece interface was quantitatively calculated and analyzed.
The Al/Mg UVeFSW process model was developed through introducing the above acoustic effects into the model of Al/Mg friction stir welding (FSW). The ultrasonic energy is stronger on the aluminum alloy side. In the stirred zone, there is the pattern distribution of ultrasonic sound pressure and energy. The heat generation at the tool-workpiece contact interface and viscous dissipation were reduced after applying ultrasonic vibra-tion. Due to the UiFR effect, the projection of friction coefficient and heat flux distributions at the tool-workpiece interface present a "deformed" butterfly shape. The calculated results show that ultrasonic vibra-tion enhanced the material flow and promoted the mixing of dissimilar materials.
The weld quality and the possible defect formation are directly determined by the weld pool shape and the thermo-fluid dynamics therein. In this paper, an untypical weld pool profile, i.e., elongated at its top and bottom but narrowed at the middle, is found experimentally and numerically in the wire feed laser beam welding. The detrimental influence of the weld pool narrowing on the element transport is analyzed and discussed. A magnetohydrodynamic technique is utilized to suppress the narrowing, aiming at a more homogenous element distribution. It is found that a low-temperature region is formed in the middle of the weld pool due to the interaction of the two dominant circulations from the top and bottom regions. The weld pool is significantly narrowed due to the untypical growth of the mushy zone in the low-temperature region, which results in a direct blocking effect on the downward flow and the premature solidification in the middle region. The Lorentz force produced by a transverse oscillating magnetic field shows the potential to change the flow pattern into a single-circulation type and the low-temperature-gradient region is mitigated.
Therefore, the downward transfer channel is widened, and its premature solidification is prevented. The numerical results are well validated by experimental measurements of metal/glass observation and X-ray fluorescence element mapping.
Through experimental observation and auxiliary numerical simulation, this investigation studies the different types of grain refinement of 5754 aluminum alloy laser beam welding by applying a transverse oscillating magnetic field. Scanning electron microscope results have proved that the application of a magnetic field can reduce the average crystal branch width and increase its number. The interaction between the induced eddy current generated by the Seebeck effect and the applied external magnetic field produces a Lorentz force, which is important for the increase of the number of crystal branches. Based on the theory of dendrite fragmentation and the magnetic field-induced branches increment, the grain size reduction caused by the magnetic field is studied. Furthermore, the effects of the magnetic field are analyzed by combining a phase field method model and simulations of nucleation and grain growth. The grain distribution and average grain size after welding verifies the reliability of the model. In addition, the introduction of a magnetic field can increase the number of periodic three-dimensional solidification patterns. In the intersection of two periods of solidification patterns, the metal can be re-melted and then re-solidified, which prevents the grains that have been solidified and formed previously from further growth and generates some small cellular grains in the new fusion line. The magnetic field increases the building frequency of these solidification structures and thus promotes this kind of grain refinement.
The effect of the oscillating metal vapor plume on the keyhole and molten pool behavior during the laser beam welding of AlMg3 aluminum alloys is investigated by the experimental and numerical method. The real-time height of the metal vapor plume is measured by high-speed camera observation. The obtained experimental results are used to evaluate the additional heating source and laser beam attenuation caused by the scattering and absorption based on the Beer-Lambert theory. Furthermore, the dynamic behavior of the metal vapor plume is incorporated into a 3D transient heat transfer and fluid flow model, coupled with the ray tracing method, for the laser beam welding of the AlMg3 alloy. It is found that the additional heating resulting from the scattered and absorbed laser beam energy by the metal vapor plume significantly expands the shape of the molten pool on the top region. Moreover, the oscillating metal vapor plume caused the fluctuation of the molten pool shape. The probability of keyhole collapse at the bottom increases significantly to 72% due to the oscillating laser power induced by the laser beam attenuation. The internal interplay between the metal vapor plume, molten pool shape, and the keyhole collapse are obtained. The developed model has been validated by the experiments, which shows a good agreement.
Robotic Measurement System Concept for Greenhouse Gas Tomography in Wastewater Treatment Plants
(2023)
This paper introduces a conceptual framework for a robotic greenhouse gas (GHG) measurement system designed for wastewater treatment plants (WWTPs). The emphasis is on accurate gas tomography measurement of emissions, crucial for national emission assessments. The proposed system is movable, semi-autonomous, and employs a combination of ground and air robots equipped with integral remote gas sensors and in-situ sensors. Employing a two/two configuration ensures comprehensive coverage of WWTPs, overcoming obstacles. The system concept lays the foundation for future implementation and evaluation, addressing the need for enhanced understanding of GHG emissions from WWTPs.
Das Master Curve (MC) Konzept nach ASTM E1921 wird momentan u.a. in der Kerntechnik für die bruchmechanische Sicherheitsbewertung ferritischer Stähle eingesetzt.
Für ferritisches Gusseisen mit Kugelgraphit (GJS) fehlt jedoch eine Validierung dieser Methode und ggf. eine systematische Überprüfung möglicher Modifikationen grundlegender Ansätze des MC-Konzepts. Aus diesem Grund soll in einem kürzlich gestarteten BMUV-Verbundprojekt zwischen der MPA Stuttgart und der BAM Berlin die Anwendbarkeit des MC-Konzepts auf GJS bei dynamischer Beanspruchung untersucht werden. Ziel ist es, eine effektive und effiziente Methodik bereitzustellen, mit der mittels einer vergleichsweise kleinen Stichprobe bruchmechanischer Kleinproben eine Referenztemperatur T0 zur werkstoffspezifischen Temperaturjustierung der MC ermittelt werden kann.
Energy efficient products often have a higher purchase price than less efficient alternatives. However, the life cycle costs are often lower due to the lower operating costs. From a purely economic point of view, efficient appliances are not only more ecological but often also more economical and, accordingly, should be purchased more frequently than less efficient appliances. However, this is not always the case. Information deficits are one of the major reasons of this discrepancy: the purchase price is visible during the purchasing process, but the follow-up costs are not, at least not in their exact amount. The EU Energy Label can be considered as a solution to close this gap. During the past decades, there has been a discussion on whether it would be better to communicate the monetary costs associated with energy consumption, since their calculation by the consumer is difficult or needs a high level of cognitive effort.
In this study, experiments and field studies on a total of 19 product groups were evaluated with regard to the question of whether the indication of costs instead of physical units affects the decision-making process of the consumer. It has been assessed under which circumstances it might positively influence the purchase decision of the customer, i.e. helping him or her to arrive at a more “energy efficient” decision. Overall, the results indicate that monetary claims possibly exceed the effect of claims on a physical basis when the costs or the differences between the alternatives available seem “relevant” to the consumer.
Die Europäische Kommission präsentierte am 11. Dezember 2019 den European Green Deal, ein Konzept mit dem Ziel, bis zum Jahr 2050 als erster Kontinent Klimaneutralität zu erreichen. Mit Inkrafttreten der Verordnung (EU) 2021/1119 des Europäischen Parlaments und des Europäischen Rates am 29. Juli 2021 zur Schaffung des Rahmens für die Verwirklichung der Klimaneutralität („Europäisches Klimagesetz“), ist dieses, sowie das Ziel der Reduzierung der Nettotreibhausgasemissionen um mindestens 55 % bis 2030 in der Gesetzgebung der Europäischen Union verankert. Die Stahlindustrie in der Europäischen Union mit ca. 57 Mio. t Nettotreibhausgasemissionen im Jahr 2020, die annähernd 2 % der Emissionen der Europäischen Union ausmachen (Inklusive Energie: 127 Mio. t; 4 %), bekennt sich zur erheblichen Reduzierung der CO2-Emissionen bis zum Jahr 2030 und zum Erreichen der Klimaneutralität bis zum Jahr 2050. Als Schlüsselwege zur Verwirklichung dieser Zielstellung hat sie zum einen Smart Carbon Usage (SCU) und zum anderen Carbon Direct Avoidance (CDA) in einer Roadmap formuliert. SCU umfasst CO2-reduzierende Maßnahmen in bestehenden Eisen- und Stahlproduktionsprozessen, Carbon Capture and Storage- (CCS) sowie Carbon Capture and Usage-Technologien (CCU). Wohingegen bei CDA CO2-Emissionen durch erneuerbare elektrische Energie sowie wasserstoffbasierte Reduktion des Eisenerzes gar nicht erst entstehen sollen. Der CDA-Weg, der voraussichtlich beschritten werden muss, um eine klimaneutrale Stahlproduktion zu erreichen [38], geht mit einer kostenintensiven Transformation der Stahlproduktion einher, die bereits von vielen Unternehmen der Stahlindustrie eingeleitet wurde und von der im Wesentlichen die beiden in Europa vorherrschenden Stahlproduktionsrouten Hochofen-Konverter-Route und Elektrolichtbogenofen-Route betroffen sind. Die CO2-Emissionen der Hochofen-Konverter-Route, von denen der überwiegende Anteil auf den Hochofen fällt, liegen laut einer für das Jahr 2015 erstellten Studie bei 1921 kg CO2/t Rohstahl inklusive der CO2-Last der Pellets als Einsatzmaterial sowie der Emissionen der nachgelagerten Stranggießanlagen und Walzwerke. Im Hochofen wird das Eisenerz durch Kohlenstoff (C) bzw. Kohlenstoffmonoxid (CO) – welche größtenteils aus dem Koks, der dem Hochofen zusammen mit dem Möller über die Gicht zugeführten wird, stammen – unter Entstehung von Roheisen und Kohlenstoffdioxid (CO2) reduziert. Das neben dem CO2 im Prozessgas enthaltene CO wird zum Beispiel zur Energiegewinnung in peripheren Prozessen ebenfalls unter Bildung von CO2 verbrannt. Zusätzlich zur Reduktion hat der Koks unter anderem physikalische Aufgaben, wie die Errichtung eines Stützgerüstes und die Gewährleistung der Permeabilität im Hochofenprozess. Somit ist eine vollkommene Substitution des Kokses zur Vermeidung der CO2-Emissionen im Hochofen nicht denkbar. Viele Strategien der Stahlunternehmen zum Erreichen der Klimaziele verfolgen daher den Wechsel von der Rohstahlproduktion aus der Hochofen-Konverter-Route hin zur Rohstahlproduktion im Elektrolichtbogenofen (EAF – Electric Arc Furnace) mit dem Einsatz von direkt reduziertem Eisen (Eisenschwamm, DRI – Direct Reduced Iron) aus vorgelagerten Direktreduktionsanlagen, die mit Wasserstoff (H2) als Reduktionsmittel betrieben werden können. Dabei ist die Elektrostahlerzeugung kein neuer Prozess und nimmt in der europäischen Union bereits jetzt einen Anteil von ca. 44 % der Rohstahlproduktion ein, jedoch überwiegend mit Schrott als Einsatzmaterial. Bei der Elektrostahlerzeugung mit Schrotteinsatz fallen laut der oben genannten Studie von Lüngen für das Jahr 20152 410 kg CO2-Emissionen pro Tonne Rohstahl an, von denen der Großteil auf die CO2-Last der fremd bezogenen elektrischen Energie zurückzuführen ist und daher nicht im Produktionsprozess selbst entsteht. Auch die Direktreduktion wird schon seit 1972 in der weltweit zweiten und bis heute in Westeuropa einzigen Direktreduktionsanlage in Hamburg betrieben. Während hier noch mit einem Reduktionsgas gearbeitet wird, das hauptsächlich aus einem aus Erdgas gewonnenen Wasserstoff-Kohlenstoffmonoxid-Gemisch besteht, liegt eine aktuelle Kernherausforderung in der Bereitstellung des in der Größenordnung der von der Transformation betroffenen Rohstahlproduktionskapazitäten notwendigen, mit erneuerbarer elektrischer Energie hergestellten Wasserstoffs. Wird zusätzlich der Strom für das Einschmelzen im Elektrolichtbogenofen aus erneuerbaren Quellen gewonnen und werden schließlich als Brennstoff verwendete Kohle und als Brennstoff verwendetes Erdgas durch CO2-neutrale Bio-Brennstoffe ersetzt, sind sowohl für den Einsatz von mit Wasserstoff reduziertem und auf Pellets ohne CO2-Last basiertem Eisenschwamm als auch für den Einsatz von Schrott CO2-Emissionen von jeweils nur 60 kg CO2/t Rohstahl erreichbar, was eine Reduktion der Emissionen, ausgehend von der Konverter-Hochofen-Route um 97 % und ausgehend von der Schrott-Elektrolichtbogenofen-Route um 85 % bedeuten würde.
Der Betrieb von Elektrolichtbogenöfen macht die an den Standorten vorhandenen Konverter sowie die Infrastruktur für Behandlung und Transport des Roheisens überflüssig. Die fortwährende Nutzung dieser bestehenden Anlagenstruktur dient daher unter anderem als Motivation für die Entwicklung einer zweiten Transformationsstrategie, die einen sogenannten Einschmelzer (SAF – Submerged Arc Furnace) als der Direktreduktionsanlage nachgelagerten Prozess vorsieht, in dem wiederum Roheisen erschmolzen wird, das anschließend im Konverter zu Rohstahl veredelt wird.
Die Transformation der Stahlindustrie beeinflusst einen weiteren CO2-intensiven Industriesektor, nämlich die Zementindustrie die verantwortlich ist für rund 4 % der CO2-Emissionen in der EU. Etwa zwei Drittel dieser Emissionen entfallen als Prozessemissionen auf die Entsäuerung des Rohstoffs Kalkstein (CaCO3), also auf die Abspaltung von CO2 unter Entstehung des für die Herstellung von Zementklinker notwendigen Branntkalks (CaO) als Zwischenstufe bei der Bildung der hydraulischen Phasen Tri- und Dicalciumsilikat. Als eines der fünf Themenfelder (5C-Ansatz: Clinker, Cement, Concrete, Construction, Carbonation), welche die europäische Zementindustrie entlang ihrer Wertschöpfungskette zum Erreichen der gesetzlichen Vorgaben der europäischen Union erarbeitet hat, umfasst das Feld "Cement" zum größten Teil die Reduzierung des Klinker-Zement-Faktors. Im Jahr 2017 betrug er 77 %, das heißt, dass 23 % des Klinkers durch alternative Materialien ersetzt wurden. Bis zum Jahr 2030 wird ein Faktor von 74 % und bis zum Jahr 2050 von 65 % angestrebt. Den größten Anteil an den Klinkersubstituten hat mit 33 % der Hüttensand aus der Stahlindustrie. Bei der Roheisenproduktion im Hochofen entsteht als Nebenprodukt Hochofenschlacke, die unter Zugabe von Schlackebildnern die Gangart des Möllers und mineralische Koksbestandteile abbindet, sowie weitere unerwünschte Begleitelemente wie Schwefel und Alkalien aufnimmt. Allein in Deutschland wurden im Jahr 2021 6,90 Mio. t – das entspricht 90 % der gesamten produzierten Hochofenschlacke – zu glasig erstarrtem Hüttensand granuliert. Dieser Hüttensand besitzt latent hydraulische Eigenschaften und wird daher seit mehr als 140 Jahren als Zementbestandteil eingesetzt, wodurch in Deutschland jährlich rund 4,5 Mio. t CO2-Emissionen eingespart werden. Alle Transformationsstrategien der Stahlindustrie beinhalten die notwendige Außerbetriebnahme der CO2-intensiven Hochöfen. Dies hat unter anderem zur Folge, dass die Hochofenschlacke als Nebenprodukt der Rohstahlerzeugung im Hochofen nicht mehr zur Verfügung stehen wird, wodurch die weitere Reduzierung des Klinker-Zement-Faktors erhebliche Zusatzmengen alternativer Materialien benötigen wird. Derzeit ist noch unklar, ob z.B. calcinierte Tone im benötigten Umfang erzeugt werden können.
Der Fachbereich Thermochemische Reststoffbehandlung und Wertstoffrückgewinnung der Bundesanstalt für Materialforschung und -prüfung (BAM) und das Institut für Baustoffforschung FEhS forschen zusammen mit Industriepartnern und weiteren Forschungseinrichtungen im Rahmen zweier Projekte in den Kooperationssphären der Stahl- und Zementindustrie, die zur Bewältigung dieser Herausforderungen beitragen. Im Projekt SlagCEM wird die Produktion eines hydraulischen Zementbestandteils durch Reduktion von Konverter- bzw. Linz-Donawitz-Schlacke (LDS) untersucht. Die mit den zusätzlich aufgenommen Lichtbogenofenkapazitäten steigenden Mengen an Elektrolichtbogenofenschlacke (EOS, engl. electric arc furnace slag, EAFS) werden im Projekt DRI-EOS behandelt, welches die Produktion eines latent hydraulischen Hüttensandsubstituts zum Ziel hat.
Packages for the transport of radioactive materials shall fulfil the requirements of the IAEA regulations for the safe transport. The requirements define mechanical and thermal test conditions including criteria ensuring the package design’s ability to withstand severe accidents and provide a high level of technical safety. Different methods can be used for safety demonstration showing compliance with the regulations.
The central part of a safety demonstration which is presented in this paper was a comprehensive drop test program with a full-scale model of a transport package accompanied by pre- and post-test FE analyses. Using full-scale drop test models allow the benefit that similarity and scaling issues become a significant smaller issue, additional material investigations can be limited and analyses for transferring test results to the original package design are reduced. Additionally, experience for the future serial packaging manufacturing and handling procedures can be collected in a very early state of the design approval process. The pre-test finite element analyses derived and justified the drop test program consisting of several drop sequences with different drop orientations of the specimen. The performance and the results of the drop test sequences shows the manageability and the advantage e.g., in view of the direct availability of test results for the package licensing. On the other hand, the drop test performance shows the difficulties during handling and the need for additional equipment during preparation of the specimen.
The package presented was intended for the transport and storage of compacted radioactive waste from reprocessing of spent nuclear fuel assemblies - designed and applied for approval by the AGC consortium. The project ended in 2021. The package design was characterized by a cask body made of a forged thick stainless-steel shell, a bolted double lid system with metallic gaskets and wood filled shock absorbers at both ends. The total mass of the entire transport package including content was 120,000 kg, the total length was about 7000 mm and the diameter approximately
3000 mm, both measures include the shock absorbers.
The paper provides an insight into the performance of a full-scale drop testing campaign within the package safety evaluation and shows some selected test results.
We present a temperature sensor based on a polymer exhibiting a Lower Critical Solution Temperature (LCST) in aqueous solution encapsulated in a capillary. Parameters are chosen such that the solution exhibits a cloud point in a temperature range of 30° C to 39°C. The characteristic of thermoresponsive polymers with an LCST, is that above that temperature phase separation of the polymer takes place which leads to a temperature-dependent formation of a cloudy suspension. An optical intensity measurement over the desired temperature range is established by an increase of optical attenuation inside the polymer solution caused by a rising temperature. For our purpose, the polymer capillary is connected to transmitter and receiver via a Polymer Optical Fibre (POF). Our intensity measurement is, to the best of our knowledge, a novel method and can be considered simple when compared to existing fibre-based temperature measurement techniques. Due to the lack of electrical components at the probe, this sensor is suitable for measurements in strong electromagnetic fields and environments for which flying sparks are hazardous, i.e., inflammable fluids or gases. Furthermore, all manufactured sensors share the same temperature dependence and, therefore, are well-suited for comparative measurement, e.g., flow measurement systems. With the given temperature range, a body temperature measurement is also suitable.
The decommissioning or refurbishment of nuclear facilities necessitates either the storage or disposal of large radioactive components such as steam generators, pressurizers, reactor pressure vessels and heads, and coolant pumps, to list the major contributors. These components or objects are large in size and mass, measuring up to approximately 6 meters in diameter, up to 20 meters in length, and weighing over 400 000 kg. In many situations, the components are transported off-site to a storage, disposal or recycling/treatment facility. Previously, many large objects had to be transported under special arrangement.
Based on state-of-the-art research and regulations, the application of the fracture mechanics master curve (MC) concept to ferritic ductile cast iron (DCI) is being investigated in a recently started German joint research project between BAM Berlin and MPA Stuttgart. This paper outlines the research approach and the planned investigations and provides first results.
According to the IAEA guidelines SSG 26, the safety assessment of DCI containers for transport as well as interim and final storage of radioactive materials is based on the fracture mechanics criterion of general crack initiation exclusion. Within this context, the focus of the current research project is on the further development of brittle fracture safety assessment methods under dynamic loading conditions. Within fracture mechanics safety assessments for steels in nuclear technology, the probabilistic MC concept according to ASTM E1921 is currently used for quasi-static loading conditions as a supplement to the established deterministic ASME reference curve concept. The MC concept allows for an effective statistical consideration of the scatter of the material toughness in the transition regime. Furthermore, the MC can also be used for elevated loading rates as they occur in accident or crash scenarios. However, for DCI, a systematic review of potential modifications to the MC assumptions and procedure according to ASTM E1921 and an associated validation are still lacking. Therefore, a corresponding methodology shall be established to determine and assess dynamic fracture toughness values of DCI in the ductile-to-brittle transition regime, using samples extracted from a component.
For the experimental program, a DCI material was produced as it is generally used for transport and storage containers. A basic mechanical-technological material characterization consisting of tensile, Charpy, and Pellini tests is planned. A comprehensive fracture mechanics test program was compiled covering dynamic testing of DC(T)9, C(T)25, C(T)50, SE(B)10, SE(B)25, and SE(B)140 specimens. Moreover, numerical analyses of different specimen geometries and test setups are planned to investigate the influences of stress triaxiality and loading rate. Throughout the experimental program, the microstructure-property relationship will be investigated based on quantitative metallographic and fractographic analyses. Finally, different MC assessment strategies will be considered, and modifications will be made if necessary.
The consideration of ageing mechanisms is with integration of the new para 613A into IAEA SSR-6 (Rev. 1) now obligatory for the design of transport packages. In addition, para 809(f) requires for packages intended to be used for shipment after storage the consideration of the effects of ageing mechanisms during storage in safety analyses and the implementation of corresponding instructions for operation and maintenance. Para 503(e) requires that all packaging components and radioactive contents have been maintained during storage in a manner that all requirements specified in IAEA SSR-6 (Rev.1) and in the applicable certificates of approval have been fulfilled.
The evaluation of ageing mechanisms and their effects including monitoring are part of BAM’s authority assessment tasks related to the mechanical and thermal package design and quality assurance aspects. BAM has compiled a guideline for the implementation of ageing assessment and of the measures for ageing management of the approval procedure based on requirements of IAEA SSR-6 (Rev.1). The guideline is applicable only for packages requiring a competent authority approval.
The paper aims to describe the structure of the guideline and the general approach for ageing management requirements. The type and amount of measures for ageing management depend mainly on the use of the package and on the ageing effects for the component, which result from relevant ageing mechanisms during package operation time.
The implementation of measures for ageing management is divided into three levels – systemic measures, package design related measures and documentation. The systemic measures are attributed to the general management system and define the whole activities for organization of ageing management like structure, responsibilities, documentation, reports and evaluation. The package design related measures are defined in an ageing management plan (AMP). These measures shall ensure that the anticipated changes of the package design under consideration of ageing effects still complies with the design approval specification. Therefore, an ageing surveillance program (ASP) and, if necessary, a gap analysis program shall be developed. The ageing management documentation (AMD) ensures the continuous documentation of the compliance of a specific package to the approved package design, comprising mainly records resulting from operation and surveillance.
In accordance with the IAEA transport regulations, the design of special form radioactive material (SFRM) shall resist a severe transport accident without undue loss or dispersal of radioactive material. The safety assessment for design approval includes besides the program for physical tests (impact, percussion, bending and heat test) also the evaluation of the management system for design, manufacture, testing, documentation, use, maintenance, and inspection.
SFRM source design plus management system shall ensure, that every specimen of the approved design is able to survive the severe mechanical and thermal tests at any time of its SFRM-working life.
Due to the long-term use of SFRM designs in most cases, the assessment of the source ageing behavior is an important aspect in the approval procedure. Different fields of application imply a wide range of environmental conditions, from clean room atmosphere to highly aggressive industrial conditions. Besides of radioactive content, corrosion is a main factor for possible SFRM design degradation.
Although the IAEA Advisory Material SSG-26 already implies an indication of the need for considering ageing mechanisms, suitable amendments in the regulatory requirements of SSR-6 should be introduced to make the approval procedure more transparent and help to reduce rounds of questions by the authority. A supplementary requirement for considering of ageing mechanisms could be a helpful contribution to an international harmonization of the approval procedure.
This paper will describe major influencing factors to be considered to assess the ageing behavior of a SFRM design and will identify the need for a regulatory specification of a SFRM-working life as basis for the assessment of the SFRM design regarding time-dependent weakening. A proposal for an explicit requirement for consideration of ageing mechanisms in safety assessment of SFRM, which should be considered in the ongoing SSR-6 revision cycle, will be explained.
New developments in nickel-based superalloys and production methods, such as the use of additive manufacturing (AM), can result in innovative designs for turbines. It is crucial to understand how the material behaves during the AM process to advance industrial use of these techniques. An analytical model based on reaction-diffusion formalism is developed to better explain the solidification behavior of the material during laser metal deposition (LMD). The well-known Scheil-Gulliver theory has some drawbacks, such as the assumption of equilibrium at the solid-liquid interface, which is addressed by this method. The solidified fractions under the Scheil model and the pure equilibrium model are calculated using CALPHAD simulations. Differential scanning calorimeter is used to measure the heat flow during the solid-liquid phase transformation, the result of which is further converted to solidified fractions. The analytical model is compared with all the other models for validation.
Rapidly advancing technologies and progressive digitisation are posing challenges to the established quality infrastructure (QI). In response, the key stakeholders of the German QI established the initiative QI-Digital aimed at developing new solutions for modern quality assurance. One of the central use cases herein is quality assurance for additive manufacturing, in which a fully interlinked additive manufacturing process chain is established. The intention is to collect and process data from each production step, allowing for a comprehensive digital view of the physical material flow. Within this process chain, prototypes of digital QI tools like machine readable standards and digital quality certificates are being demonstrated, tested, and evolved. This is complemented by research on the process level, comprising the evaluation and refinement of methods for in-situ and ex-situ quality assurance, as well as algorithms for registration, reduction, and analysis of process data. This paper presents the status, goals, and vision for the QI-Digital use case additive manufacturing.