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Alkali-activated fly ashes have been proposed for various applications where resistance against high temperatures is required, yet several details regarding the response of these materials to heat-exposure need to be clarified. In the present study, heat-induced cracking in fly ash-based alkali-activated pastes and lightweight mortars was analyzed by in-situ acoustic emission (AE) detection during complete heating-cooling cycles (up to ∼1100 °C), augmented by thermogravimetry and ex-situ SEM and XRD analyses. The applicability of the lightweight mortars as passive fire protection coatings was assessed by recording temperature-time curves of mortar-coated steel plates. Cracking during heating was limited and associated exclusively with the dehydration of the materials in the temperature range ∼90–360 °C. However, samples heated to temperatures above ∼600 °C exhibited intense cracking on cooling. This was attributed to differential deformations caused by local sintering and partial melting at the glass transition temperature, and subsequent quenching on cooling.
Aluminium alloy 6060 is typical of a family of Al-Mg-Si extrusion alloys, which are considered weldable only
when using an appropriate filler alloy such as 4043 (Al-5Si) or 5356 (Al-5Mg). This study concerns the
thermal analysis and solidification path determination of aluminium alloy 6060 diluted with variable amounts
of 4043. Casting of controlled mixtures of alloys 6060 and 4043 was used to simulate different weld dilutions
in order to facilitate thermal analysis. Thermal analysis and metallography were applied in order to reveal
solidification reactions and phases, and allow calculation of solid fraction versus temperature curves.
Although the liquidus temperature was little affected, different phases formed with increased 4043 dilution,
with a trend toward lower temperature reactions and a larger fraction interdendritic constituent.
A 3D electro-thermomechanical model is established in order to investigate liquid metal embrittlement.
After calibration to a dual phase steel of the 1000 MPa tensile strength class, it is used to analyse the thermo-mechanical system of an experimental procedure to enforce liquid metal embrittlement during resistance spot welding. In this procedure, a tensile stress level is applied to zinc coated advanced high strength steel samples during welding. Thereby, liquid metal embrittlement formation is enforced, depending on the applied stress level and the selected material.
The model is suitable to determine and visualise the corresponding underlying stresses and strains responsible for the occurrence of liquid metal embrittlement. Simulated local stresses and strains show good conformity with experimentally observed surface crack locations.
Methods to obtain weld discontinuities in spot-welded joints made of advanced high-strength steels
(2011)
Resistance spot welding is the major joining technique in mass car production. This applies in particular to high-strength steel and advanced high-strength steel (AHSS) joining of thin sheet steel components for lightweight body shell structures. Joining of AHSS in mass production might lead to weld discontinuities under certain circumstances. Those discontinuities in form of cracks might be an initial start of cracking in the spot-welded joints regarding fatigue loads. It is of great interest to figure out, if, in comparison to specimens without weld discontinuities, the crack initiating point changes and if the fatigue resistance might be reduced by the discontinuities. In this contribution, an overview of potential discontinuities is given. Their possible causes are discussed and means for their detection are highlighted. Among the possible causes of weld discontinuities, two major groups are distinguished: the welding parameters as primary influences in the welding process, and the production-specific influences as secondary ones. With emphasis on major cracks penetrating the weld nugget, these influences are analysed. Finally, a combination of extreme welding parameters with production-specific influences is chosen in order to establish a method which enables the preparation of fatigue test specimens with reproducible major cracks in different locations of the spot-welded joints. This method is than applied in order to prepare spot weld specimens for fatigue tests.
Hot crack prevention in materials production and processing is an essential prerequisite for welded component safety. The causes of hot cracking can ultimately be attributed to the occurrence of metallurgical effects and to structural loads. More than 140 hot cracking test procedures have hitherto been developed for determining the hot cracking resistance. In principle, they are divided in self-restraint and externally loaded hot cracking tests with diverse process variants. Only some of the hot cracking tests are international standardized. Although various factors are known that encourage or prevent hot cracking, it is often not possible even with defined welding conditions to draw immediate conclusions about the hot cracking resistance of a welded component alone from a metallurgical composition of the base and filler materials. Based on an evaluation of the existing theories relating to hot cracking susceptibility assessment, this study summarizes the major hot cracking test procedures and highlights the application limits of the test procedures by presenting overviews along with explanations. It shows that weld hot cracking tests can generally be used to rank materials, welding consumables, and welding conditions. The evaluation of hot cracking test results and of their transferability among one another and to real components always requires consideration of the close relationships between metallurgy, welding process, and parameters, respectively, and prevailing restraint conditions.
Realization and safe operation of modern welded structures are progressively requiring for base and filler materials to cope with continually increasing loads, Analyses with a view to crack prevention therefore need to accommodate particularly the structural design (restraint intensity) and the thermomechanical effects in terms of stresses introduced during welding, Against this background, multi-run welding experiments were carried out in an IRC - (Instrumented Restraint Cracking) Test under defined restraint intensity in order to examine the influence of heat control (preheating and interpass temperatures) on the weldinq-specific forces and stresses, The experiments revealed significant rises in the reaction force and stress after welding with increasing preheating and interpass temperature, Furthermore, various concepts for calculating the preheating temperature are discussed, It is demonstrated that the hitherto existing concepts for high-strength finegrained structural steels can lead to divergent results.
Offshore wind turbines continuously increase in size and weight and demand adequate offshore foundations concepts like monopiles, tripods or jackets. These components are typically submerged arc welded (SAW) high-strength thick steel plates like the S420ML. During welding, the occurrence of delayed hydrogen assisted cracking (HAC) must be anticipated. HAC is a critical combination of the local hydrogen concentration within a susceptible microstructure under certain mechanical load, i.e., the occurring (welding) residual stresses. The welding sequence of the thick-walled plates complicate the residual stress distribution due to the necessary repeated thermal cycling, i.e., welding seam / layer deposition to fill the joint. For that purpose, SAW with two-wire-technique was used to weld a specially designed and prototype-like mock-up of a real component with a thickness of 50 mm, filled with 22 passes and a seam length of 1,000 mm. Additional welded stiffeners simulated the effect of a high restraint, to stimulate critical HAC conditions. The residual stresses were determined by a robot XRD goniometer. A least square regression analysis of the sin²ψ-law by using multiple ψ- and φ-tilts was applied. Tensile residual stresses up to the yield limit are found both in the weld metal and in the heat-affected zone. Numerical modelling allowed the qualitative estimation of the hydrogen diffusion in the weld, enabling the determination of critical conditions for the formation of HAC. In a future step, a structural simulation will allow the assessment of the welding residual stresses and the comparison to the XRD-values.
Non-destructive testing methods are mostly applied and established for the detection of embedded mounting parts or structural defects in building elements. The assessment of the concrete microstructure or microstructural changes like chemical alterations or the formation of microcracks, e.g. due to material aging, freeze-thaw cycles, alkali-silica reaction and ettringite, is not in the focus of ndt research though. Concrete moisture and enhanced salt contents, which usually trigger all chemical microstructural changes, are other material properties, lacking reliable ways of measuring. But, the assessment of such material properties, on the long term also in a depth resolved manner, is definitely important, when the sustainability of our concrete infrastructure buildings shall be evaluated.
New consideration like the potential use of ndt, in particular the combination of different methods and alternate ways of data analysis are subject of research currently undertaken at BAM. These approaches involve for example working towards (i) a deeper understanding of how to measure moisture distributions reliably and follow transport phenomena, (ii) the use of stray phenomena in radar and ultrasound to locate material inhomogeneities or (iii) the application of LIBS for the delineation of diffusion and migration processes but also (iv) the use of new tools for data analysis like data fusion. First results are presented and new ideas discussed.
Since ancient times, marble has been the preferred material for monuments, sculptures, Ornaments and architecture. Though the stone is often a Chosen material, long-term exposure of marble results in cumulative deterioration of the rock fabric. The rate and extent of deterioration depends on the rock fabric and the climatic conditions. Besides the thermal vulnerability of marble, a combination of thermal and hygric fluctuation accelerates the deterioration process. The weathering sensitivity of marbles can be characterised by the irreversible length change of samples after heating under thermohygric conditions as residual strain. This residual strain is a non-reversible deterioration and caused by microcracking induced by a pronounced anisotropy of the thermal dilatation coefficient of calcite.
In brittle materials like marble, cracking and crack growth or friction on crack surfaces are accompanied by release of acoustic waves. The analysis of these acoustic emissions can give a deeper insight into the deterioration mechanism of marble.
In this study, acoustic emissions of thermohygric treated marble were analysed and correlated with ultrasonic velocities, thermal dilatation and residual strains. Therefore, different types of calcitic marble were cyclically heated from 20 °C to 90 °C and after equilibration of the samples cooled down again to 20 °C. While the first cycles were performed under dry conditions, the following were
executed in a humid environment. The analysis of acoustic emissions enables one to determine when cracking occurs during the thermal treatment. It is also possible to differentiate microcracking from internal friction. Furthermore, the evolution of Deterioration can be estimated based on ultrasonic velocities. The combination of acoustic Methods and strain measurement gives an insight into the disintegration mechanism and Supports the development of prevention strategies.
Characterization of Hydrogen Diffusion in a Thick-walled Submerged Arc Multi-Layer Weld Joint
(2021)
The energy production of the future will be dominated by CO2-emission free techniques like wind turbines and become essential in scope of the planned hydrogen economy. As onshore installation capacity is limited, the in-crease of the number of offshore wind turbines (OWT) is a major goal. In that connection, the OWTs continuously increase in size and weight and demand adequate foundations concepts like monopiles or tripods. These compo-nents are typically manufactured from welded mild steel plates with thickness up to 200 mm. The predominant welding technique is submerged arc welding (SAW) with up to five wires. In accordance with the standards, the occurrence of delayed hydrogen assisted cracking is anticipated by either a hydrogen removal heat treatment (HRHT) or a so-called minimum waiting time (MWT) before non-destructive testing (NDT) of the respective weld joint is allowed. The reason for the MWT is the necessary time for the hydrogen diffusion at ambient temperature due the high plate thickness. Both the effectiveness of a HRHT at elevated temperatures or the MWT at ambient temperature can be estimated by calculation of the diffusion time. This time depends on reliable hydrogen diffu-sion coefficients and these are rare in literature. For that reason, this study presents the hydrogen diffusion coef-ficients obtained from a multi-layer SAW joint of an offshore steel grade. Two different experimental techniques were used to identify the respective diffusion behavior: (1) hydrogen desorption experiments with a carrier gas hot extraction analyzer at elevated temperatures for the characterization of a HRHT and (2) the electrochemical permeation technique at ambient temperature for the characterization of an MWT. From both experiments, the respective diffusion coefficients were calculated. The obtained DCs are different from those reported in literature, i.e., the duration or applicability of a HRHT or MWT must be critically discussed.
Multi-element systems with defined entropy (HEA - High Entropy Alloy or MEA - Medium Entropy Alloy) are rather new material concepts that are becoming increasingly important in materials research and development. Some HEA systems show significantly improved properties or combinations of properties, e.g., the overcome of the trade-off between high strength and ductility. Thus, the synthesis, the resulting microstructures, and properties of HEA have been primarily investigated so far. In addition, processing is crucial to achieve a transfer of potential HEA/MEA materials to real applications, e.g. highly stressed components. Since fusion welding is the most important joining process for metals, it is of vital importance to investigate the weldability of these materials. However, this has rarely been the subject of research up to date. For that reason, in this work the weldability depending on the surface preparation of a CoCrFeMnNi-HEA and a CoCrNi-MEA for TIG welding is investigated. The fusion welding of longer plates is described here for the first time for the CoCrNi alloy. The welds of both materials showed distinct formation of cracks in the heat affected zone (HAZ). Optical and scanning electron microscopy analysis clearly confirmed an intergranular fracture topography. But based on the results, the crack mechanism cannot be conclusively clarified as either a liquid metal embrittlement (LME) or hot cracking like liquid film separation occurred.
Influence of Surface Preparation on Cracking Phenomena in TIG-Welded High and Medium Entropy Alloys
(2022)
Multi-element systems with defined entropy (HEA—high entropy alloy or MEA—medium entropy alloy) are rather new material concepts that are becoming increasingly important in materials research and development. Some HEA systems show significantly improved properties or combinations of properties, e.g., the overcoming of the trade-off between high strength and ductility. Thus, the synthesis, the resulting microstructures, and properties of HEA have been primarily investigated so far. In addition, processing is crucial to achieve a transfer of potential HEA/MEA materials to real applications, e.g., highly stressed components. Since fusion welding is the most important joining process for metals, it is of vital importance to investigate the weldability of these materials. However, this has rarely been the subject of research to date. For that reason, in this work, the weldability depending on the surface preparation of a CoCrFeMnNi HEA and a CoCrNi MEA for TIG welding is investigated. The fusion welding of longer plates is described here for the first time for the CoCrNi alloy. The welds of both materials showed distinct formation of cracks in the heat affected Zone (HAZ). Optical and scanning electron microscopy analysis clearly confirmed an intergranular fracture topography. However, based on the results, the crack mechanism cannot be conclusively identified as either a liquid metal embrittlement (LME) or hot cracking-like liquid film separation.
Offshore wind turbines (OWT) are a major goal of the energy strategy of Germany encompassing the increase of the installed wind power. OWT components are manufactured from welded steel plates with thicknesses up to 200 mm. The underlying standards and technical recommendations for construction of OWTs encompass specifications of so-called minimum waiting time (MWT) before non-destructive testing of the weld joints is allowed. Reason is the increased risk of time-delayed hydrogen assisted cold cracking as hydrogen diffusion is very slow due to the very thick plates. The strict consideration of those long MWT up to 48 h during the construction of OWTs leads to significant financial burden (like disproportionately high costs for installer ships as well as storage problems (onshore)). In this study, weld joints made of S355 ML were examined in comparison with the offshore steel grade S460 G2+M. The aim was to optimize, i.e., reduce, the MWT before NDT considering varied heat input, hydrogen concentration and using self-restraint weld tests. This would significantly reduce the manufacturing time and costs of OWT construction. To quantify the necessary delay time until hydrogen-assisted cold cracks appear, acoustic emission analysis was applied directly after welding for at least 48 h.