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Organisationseinheit der BAM
- 8 Zerstörungsfreie Prüfung (3)
- 8.2 Zerstörungsfreie Prüfmethoden für das Bauwesen (2)
- 8.4 Akustische und elektromagnetische Verfahren (2)
- 3 Gefahrgutumschließungen; Energiespeicher (1)
- 3.3 Sicherheit von Transportbehältern (1)
- 6 Materialchemie (1)
- 6.3 Strukturanalytik (1)
- 7 Bauwerkssicherheit (1)
- 7.5 Technische Eigenschaften von Polymerwerkstoffen (1)
- 9 Komponentensicherheit (1)
The moisture content of wood is known to have a significant influence on the wood's mechanical properties. Using wood as an energy absorber in impact limiters of packages for the transport of radioactive material, it is of particular importance to ensure the moisture content and thus relevant mechanical properties to be in specified limits. The paper surveys the influence of wood moisture content on the mechanical properties of wood. Different measuring methods are discussed with respect to in situ applicability, accuracy and effort. The results of an experimental analysis of the accuracy of hand held moisture metres using the electrical resistance method are discussed. Conclusions are drawn regarding the measurement of moisture content of wood upon delivery as well as of complete impact limiter assemblies. Requirements for quality surveillance during manufacturing of wood filled impact limiters are derived and it is exemplified how to meet them. Construction, manufacturing and inspection of impact limiter encapsulation with regard to leak tightness are addressed.
The temperature and gas concentrations in a
newly established pine-wood debris pile of 20 m × 15 m ×
6 m in dimensions (approximately 400 tons of fresh weight
material) were monitored for 150 days. Temperature was
measured at ten different positions within the pile, while
concentrations of CO2, O2, CO and CH4 were taken at four
different representative locations. The pile was characterized
by a strong temperature increase within the first 10–
12 days of storage. Results of the gas analysis in this period
suggest that the temperature increase was caused by microbial
processes. In particular, reduced oxygen concentration
and almost complete absence of methane indicate mainly
aerobic respiration processes. Effects of weather conditions
on the temperature/gas distribution and time evolution are
also discussed in the paper.
The method requires two parallel boreholes in the specimen in which two microwave antennae can be moved. The moisture content in the material can be calculated from the microwave intensity transmitted between the two boreholes. Moisture profiles along the boreholes can be obtained by moving the antennae in steps along the length of the boreholes and taking measurements at each step.
The microwave frequencies used in the laboratory measurements ranged from 8 to 16.5 GHz in steps of 0.5 GHz. The diameters of the antennae were between 7 and 9 mm, and of the boreholes between 8 and 12 mm. The microwave method produced measurement uncertainties between 0 and 2% by volume for all the materials studied in this report.
The site of Schöningen (Germany), dated to ca. 300,000 years ago, yielded the earliest large-scale record of humanly-made wooden tools. These include wooden spears and shorter double-pointed sticks, discovered in association with herbivores that were hunted and butchered along a lakeshore. Wooden tools have not been systematically analysed to the same standard as other Palaeolithic technologies, such as lithic or bone tools. Our multianalytical study includes micro-CT scanning, 3-dimensional microscopy, and Fourier transform infrared spectroscopy, supporting a systematic technological and taphonomic analysis, thus setting a new standard for wooden tool analysis. In illustrating the biography of one of Schöningen’s double-pointed sticks, we demonstrate new human behaviours for this time period, including sophisticated woodworking techniques. The hominins selected a spruce branch which they then debarked and shaped into an aerodynamic and ergonomic tool. They likely seasoned the wood to avoid cracking and warping. After a long period of use, it was probably lost while hunting, and was then rapidly buried in mud. Taphonomic alterations include damage from trampling, fungal attack, root damage and compression. Through our detailed analysis we show that Middle Pleistocene humans had a rich awareness of raw material properties, and possessed sophisticated woodworking skills. Alongside new detailed morphometrics of the object, an ethnographic review supports a primary function as a throwing stick for hunting, indicating potential hunting strategies and social contexts including for communal hunts involving children. The Schöningen throwing sticks may have been used to strategically disadvantage larger ungulates, potentially from distances of up to 30 metres. They also demonstrate that the hominins were technologically capable of capturing smaller fast prey and avian fauna, a behaviour evidenced at contemporaneous Middle Pleistocene archaeological sites.
Wood is widely used in impact limiters of Transport casks for radioactive material. Encapsulated by an outer and inner Steel structure, spruce wood is offen applied in layers of altemating direction. The friction at the interfaces between these layers is of crucial importance for the impact and energy absorption e.g., at an accidental impact of a cask against a hard component.
In order to get detailed Information for corresponding numerical calculations, in this study the friction coefficient for the combinations wood-wood and wood-steel was measured in the temperature ränge between -40 °C and 90 °C according to the relevant stress conditions for such casks. Results show decreasing friction with increasing temperature, ranging from 0.43 at -40 °C to 0.22 for 90 °C for wood-steel combinations and from 0.3 at -40 °C to 0.24 at 90 °C to for a wood-wood combination.
Impact limiting components of packages for the transport of radioactivematerials are often designed as wood filled steel constructions. Wood absorbs major part of the impact energy in order to minimise the impact load acting upon the containment. Dynamic impact experiments with wood filled impact limiters showed different crushing mechanisms for axially loaded wood depending on their lateral constraint. Tests on spruce wood samples (Picea abies) were performed in order to clarify the influence of strain rate from static to 30 s-1 on a) compression strength, b) stress at a global strain level of 50%, and c) energy absorption capacity at 50% deformation, including statistical evaluation of the results. Results were as follows: strain rate increase led to significantly higher compression strength, stress and strain energy at a strain level of 50%. Lateral strain restriction had no effect on compression strength; it had a significant effect on stress and strain energy at strain level of 50%. Therefore, the definition of a general yield curve for wood under large deformations is not possible, the yield curve has to be chosen taking into account lateral constraints.
The effective high neutron scattering absorption coefficient of hydrogen (48.5 cm²/g) due to the scattering allows neutrons to reveal hydrocarbon structures with more contrast than X-rays, but at the same time limits the sample size and thickness that can be investigated. Many planar shaped objects, particularly wood samples, are sufficiently thin to allow thermal neutrons to transmit through the sample in a direction perpendicular to the planar face but not in a parallel direction, due to increased thickness. Often, this is an obstacle that prevents some tomographic reconstruction algorithms from obtaining desired results because of inadequate information or presence of distracting artifacts due to missing projections. This can be true for samples such as the distribution of glue in glulam (boards of wooden layers glued together), or the course of partially visible annual rings in trees where the features of interest are parallel to the planar surface of the sample. However, it should be possible to study these features by rotating the specimen within a limited angular range. In principle, this approach has been shown previously in a study with fast neutrons [2]. A study of this kind was performed at the Antares facility of FRM II in Garching with a 2.6×107/cm² s thermal neutron beam. The limit of penetration was determined for a wooden step wedge carved from a 2 cm×4 cm block of wood in comparison to other materials such as heavy metals and Lucite as specimens rich in hydrogen. The depth of the steps was 1 cm, the height 0.5 cm. The annual ring structures were clearly detectable up to 2 cm thickness. Wooden specimens, i.e. shivers, from a sunken old ship have been subjected to tomography. Not visible from the outside, clear radial structures have been found that are typical for certain kinds of wood. This insight was impaired in a case where the specimen had been soaked with ethylene glycol. In another large sample study, a planar board made of glulam has been studied to show the glued layers. This study shows not only the limits of penetration in wood but also demonstrates access to structures perpendicular to the surface in larger planar objects by tomography with fast neutrons, even with incomplete sets of projection data that covers an angular range of only 90° or even 60°.
Dynamic and quasi-static FE calculation of impact from 9 metre drop of spent fuel transport cask
(2009)
The drop from 9 m height onto a rigid target is one of the required proofs of safety for packages of radioactive materials. Direct dynamic finite element method (FEM) calculations and combined two step analytical quasi-static finite element (FE) calculations are both applied for the simulation of a 9 m drop test. This paper gives a comparative example of both approaches for the 9 m side drop simulation of the spent fuel transport cask with wood filled impact limiter. The model for dynamic FEM consists of cask body and impact limiter. Detailed material properties and geometry descriptions from each component of the impact limiter are required. The results (stress fields in the cask body) are obtained directly from the calculation. The combined method provides as intermediate results the force-deformation characteristic of impact limiter. The maximum impact limiter force determined by the law of energy conservation during the drop is then - in a second step - applied on the cask body in a quasi-static FE model in order to calculate the stresses. In this paper, the rigid body deceleration and the maximum stress in the middle of the cask body are used for the comparison between the dynamic FEM and the combined method. Similar maximum rigid body deceleration-time curves were obtained by both methods for the horizontal 9 m free fall. Concerning the stress in the cask body the dynamic FEM results oscillate about values calculated by the combined quasi-static approach. If the combined quasi-static approach is used in the safety assessment of a cask, a suitable factor has to be applied on its results to take into account the additional dynamic effects.
Until the end of the 1980s many wooden artworks underwent surface treatment by liquid preservatives, e.g. Hylotox-59. DDT (dichlorodiphenyltrichloroethane) crystal structures are formed on the wooden surfaces by the "blooming" of chlorine compounds by time. In addition to an aesthetic disturbance, it is assumed that DDT represents a health risk. Therefore, the removal of DDT crystals from the surfaces is requested. Contaminated wood with natural biocide ageing, gilded and wood carved elements and wooden samples with paint layers were provided by the Schlossmuseum Sondershausen, Germany. Laser cleaning on selected surface areas on the objects was done by means of femtosecond and nanosecond laser pulses. For the same object, cleaning results using 30-fs laser pulses at 800 nm wavelength are compared to findings utilizing 10-ns laser pulses at 1064 nm wavelength. Before and after laser treatment, chlorine measurements at the same surface position were done by X-ray fluorescence analysis (XRF) as an indicator for the presence of DDT. In this way, pointwise chlorine depletion rates can be obtained for the different pulse duration regimes and wavelengths. Additionally, the object surfaces were examined using optical microscopy and multi spectral imaging analysis.
Fire retardancy effects in single and double layered sol-gel derived TiO2 and SiO2-wood composites
(2012)
Sol–gel derived TiO2 and SiO2-wood inorganic composites are prepared by direct vacuum infiltration of silicon and titanium alkoxide based precursors in pine sapwood in one or two cycles followed by a controlled thermal curing process. The resulting flame retardancy effect is investigated under two different fire scenarios using cone calorimetry and oxygen index (LOI). Heat release rates (HRR) especially the values for the second peak, are reduced moderately for all single layered composites. This effect is more pronounced for double layered composites where HRR was reduced up to 40 % showing flame retardancy potential in developing fires. Beside this, smoke release was lowered up to 72 % indicating that these systems had less fire hazards compared to untreated wood, whereas no meaningful improvement is realized in terms of fire load (total heat evolved) and initial HRR increase. However impressively, the LOI of the composites were increased up to 41 vol% in comparison to 23 vol% for untreated wood displaying a remarkable flame retardancy against reaction to a small flame. An approximate linear interdependence among the fire properties and the material loading as well as fire residue was observed. A residual protection layer mechanism is proposed improving the residue properties for the investigated composites.