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In this communication a novel concept for pH sensing is introduced which is specifically adapted to monitor carbonation induced corrosion in concrete structures. The method is based on a ratiometric measurement principle, exploiting the pH sensitive colour switching of thymol blue in the basic pH regime and the emissive properties of two different (Zn)CdSe/ZnS core shell quantum dots. The transition point of thymol blue in a Hydrogel D4 matrix was determined to be at around pH 11.6, which fits ideally to the intended application. Next to the fundamental spectroscopic characterization of the ratiometric response, a new design for a sensor head, suitable for the incorporation into concrete matrices is presented. Toward this, a manufacturing process was developed which includes the preparation of a double layer of polymers containing either thymol blue or a quantum dot mixture inside a porous ceramic tube. Results of a proof-of-priciple performance test of the sensor head in solutions of different pH and in cement specimens are presented, with encouraging results paving the way for future field tests in concrete.
Challenging new constructions and ageing infrastructure are increasing the demand for permanent monitoring of loads and condition. Various methods and sensors are used for this purpose. But the technologies available today have difficulties in detecting slowly progressing locally confined damages. Extensive investigations or instrumentations are required so far for this purpose. In this study we present new sensors and data processing methods for ultrasonic transmission, which can be used for non-destructive long term monitoring of concrete. They can be mounted during construction or thereafter. Larger volumes can be monitored by a limited number of sensors for changes of material properties. The principles of ultrasonic transmission and influencing factors are presented. This latter include load, damages as well as environmental parameters as temperature or moisture. Various methods for data processing, e. g. coda wave interferometry are introduced. They allow the detection of very small changes in the medium. The embedded sensors are shown including mounting and operation. Application examples so far include small scale laboratory freeze-thaw experiments, localizing loads in larger concrete models, monitoring load effects on real structures as well as detecting acoustic events. Some sensors are operating already for several years. The sensors can be used as transmitter or receivers or switched between both roles. While most of the previous experiments have been active (at least one sensor serving as transmitter), new studies show that the sensors are useful as well for passive measurements, e. g. in acoustic emission or time reversal experiments. Besides application in civil engineering our setups can also be used for model studies in geosciences.
Reinforced concrete and several other building materials deteriorate during their service life. Almost all deterioration processes are related to moisture. For understanding those processes, knowing the exact amount of the moisture content and the moisture transport characteristics is crucial. In fact, the moisture transport in porous materials is a two-phase flow; consisting of the vapour and the liquid phase. The two corresponding parameters are the diffusion coefficient and the hydraulic conductivity. By means of an inverse approach, these two coefficients are experimentally determined. The moisture transport of eight different screed types during hydration and evaporation is monitored based on embedded humidity sensors. The measured humidity profiles are converted into a pore saturation by adapting the approach of Hillerborg to the measured pore volume distribution. The summation of all pore saturations yields the total moisture content including the ink-bottle effect during desorption. The pore volume distribution was determined by mercury intrusion porosimetry as well as by gas adsorption. The measurement of the humidity and the pore saturation in the entire sample enables to invert the mass balance in order to extract the diffusion coefficient and the hydraulic conductivity. The determined diffusion coefficients of the eight investigated screeds are between m2s-1 and m2s-1.
In civil engineering, many structures are made of reinforced concrete. Most Degradation processes relevant to this material, e.g., corrosion, are related to an increased level of material moisture.
Therefore, moisture monitoring in reinforced concrete is regarded as a crucial method for structural health monitoring. In this study, passive radio frequency identification (RFID)-based sensors are embedded into the concrete. They are well suited for long-term operation over decades and are well protected against harsh environmental conditions. The energy supply and the data transfer of the humidity sensors are provided by RFID. The sensor casing materials are optimised to withstand the high alkaline environment in concrete, having pH values of more than 12. Membrane materials are also investigated to identify materials capable of enabling water vapour transport from the porous cement matrix to the embedded humidity sensor. By measuring the corresponding relative humidity with embedded passive RFID-based sensors, the cement hydration is monitored for 170 days.
Moreover, long-term moisture monitoring is performed for more than 1000 days. The Experiments show that embedded passive RFID-based sensors are highly suitable for long-term structural health monitoring in civil engineering.
Monitoring of the absolute water content in porous materials based on embedded humidity sensors
(2018)
Moisture transport monitoring may indicate the onset of deterioration in porous building materials Prior to damage occurring. Most moisture measurement systems provide only qualitative values, require extensive calibration, or are destructive. Thus, non-destructive and calibration-free monitoring Systems are required. Our approach of moisture monitoring is to embed sensors that measure the relative humidity.
In our experiment, screed samples are monitored during the Hydration and evaporation process. Every test sample is equipped with 10 embedded sensors which measure the relative humidity across the sample thickness. Based on Hillerborg’s approach, the relative humidity is converted into the corresponding pore saturation. In our study, the free water is computed without knowledge of the Sorption isotherm. The free water in the pore system is predicted and validated. The predicted weight decrease corresponds conclusively to gravimetrically measured weights. The embedded sensors yield the absolute liquid water content and enable an experimental, non-destructive monitoring of liquid water in porous materials.
Die immer komplexere Konstruktionsweise von Neubauten einerseits und die alternde Infrastruktur andererseits erfordern in manchen Fällen eine dauerhafte Überwachung, um besondere Einwirkungen und gegebenenfalls Schädigungen rechtzeitig und genau zu erkennen. Hierfür ist eine Vielzahl von Methoden und Sensoren verfügbar. Das Portfolio weist aber insbesondere bei der Detektion langsamer, räumlich begrenzter Veränderungen Lücken auf. Hierfür sind bisher sehr aufwändige Untersuchungen oder Installationen notwendig.
In der vorliegenden Arbeit werden Sensoren und zugehörige Auswertemethoden für die Ultraschalltransmission vorgestellt, die sich für die zerstörungsfreie, dauerhafte Überwachung von Beton eignen. Direkt oder nachträglich in Betonkonstruktionen eingebaut, ermöglichen sie eine nicht nur lokale, sondern größere Raumbereiche umfassende Dauerüberwachung von Änderungen der Materialeigenschaften.
Das Prinzip der Ultraschalltransmission und die verschiedenen Einflussparameter werden vorgestellt. Zu letzteren gehören neben der Belastung und Schädigung auch Umweltparameter wie Temperatur und Feuchte. Verschiedene Methoden zur Datenanalyse, wie z. B. die Codawelleninterferometrie, ermöglichen eine Detektion kleinster Veränderungen. Die in den Beton einzubettenden Ultraschallsensoren werden vorgestellt und ihr Einbau und Betrieb beschrieben. Als Beispiele für Anwendungen werden Frost-Tauwechsel-Experimente im Labor, die Detektion von lokalen Lasten im Technikumsmaßstab und der Einsatz an realen Brücken diskutiert. Die Sensoren sind zum Teil bereits seit mehreren Jahren in Probeobjekte eingebettet und liefern zuverlässig wertvolle Daten.-------------------------------------------------------------------------------------------------------------------------------------------------------------
Monitoring of concrete constructions by embedded ultrasonic sensors:
Challenging new constructions and the ageing infrastructure are increasing the demand for permanent monitoring of loads and damages. Various methods and sensors are used for this purpose. But the technologies available today have difficulties in detecting slowly progressing locally confined damages. Extensive investigations or instrumentations are required so far for this purpose.
In this study we present new sensors and data processing methods for ultrasonic transmission, which can be used for non-destructive permanent monitoring of concrete. They can be mounted during construction or thereafter. Larger volumes can be monitored by a limited number of sensors for changes of material properties.
The principles of ultrasonic transmission and influencing factors are presented. This latter include load, damages as well as environmental parameters as temperature or moisture. Various methods for data processing, e. g. coda wave interferometry are introduced. They allow the detection of very small changes in the medium. The embedded sensors are shown including mounting and operation. Application examples so far include small scale laboratory freeze-thaw experiments, localizing loads in larger concrete models and monitoring load effects on real structures. Some sensors are operating already for several years.
This study evaluates the sensitivity of embedded ultrasonic sensors to detect propagating cracks within concrete. Because of the sensors constant coupling to the medium, highly sensitive data analysis techniques, such as the correlation between signals and their attenuation, are applied to detect changes in the signal due to propagating cracks.
The accuracy of the detected onset of the crack is evaluated with the nondestructive testing methods acoustic emission and Digital Image Correlation. It shows that with embedded ultrasonic sensors crack propagation can be detected before it is visible on the surface of the concrete.