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We have studied the influence of gamma rays on physical properties of different commercially available silica optical fibers stepwise irradiated up to a total dose of 100 kGy. The detection of radiation-induced changes in silica glass offers the possibility of using selected optical fibers as distributed radiation sensors. The measurements performed by us were based on optical backscatter reflectometry and Brillouin distributed sensing. The measurement methods enable an analysis of radiation-induced modification of the group refractive index and density of the optical fibers. The most distinct physical effect observed by us concerns the increase of the optical attenuation with rising total radiation doses. Quantitative measurement results indicate a crucial impact of fiber dopants on radiation-induced physical and sensory characteristics of silica optical fibers affected by differences in fiber fabrication techniques. Based on the obtained results, the suitability of distributed Brillouin sensing for dosimetry applications seems to be improved by modifying the refractive index profile of the fiber core.
We have studied the influence of gamma rays on physical properties of different commercially available silica optical fibers stepwise irradiated up to a total dose of 100 kGy. The detection of radiation-induced changes in silica glass offers the possibility of using selected optical fibers as distributed radiation sensors. The measurements performed by us were based on optical backscatter reflectometry and Brillouin distributed sensing. The measurement methods enable an analysis of radiation-induced modification of the group refractive index and density of the optical fibers. The most distinct physical effect observed by us concerns the increase of the optical attenuation with rising total radiation doses. Quantitative measurement results indicate a crucial impact of fiber dopants on radiation-induced physical and sensory characteristics of silica optical fibers affected by differences in fiber fabrication techniques. Based on the obtained results, the suitability of distributed Brillouin sensing for dosimetry applications seems to be improved by modifying the refractive index profile of the fiber core.
High and ultra-high molecular weight polyethylenes are high performance materials, which are predestined for a wide range of applications due to characteristics like high density, low weight, good dimensional stability, high chemical resistance, and high hydrogen content. These polymers are used in two demanding areas: as implant material in medical technology (only ultra-high molecular weight polyethylenes) and as a component for neutron shielding purposes in casks for storage and transport of radioactive waste. In the medical field (joint replacements) as well as during neutron radiation shielding application, high and ultra-high molecular weight polyethylenes are exposed to gamma irradiation: in the first case requested as sterilization process and for surface-crosslinking and in the second case existing as a side effect of inserting the radioactive material in the cask.
Given that polyethylene as shielding material has to withstand any type of degradation affecting safety relevant aspects to be applicable for long-term radiation shielding purposes for instance over a period of 40 years, the durability of the material is of special interest. High molecular weight polyethylene (HMW-PE; LUPOLEN 5261Z; Lyondell Basell) and ultra-high molecular weight polyethylene (UHMW-PE; GUR 4120; Ticona) were subjected to gamma radiation and afterwards thermally treated. The gamma doses used are in the range of 50 to 600 kGy and irradiation takes place at RT using a Co-60 source. The planned thermal treatment will take place at a temperature of 125 °C for periods of minimum 30 days and maximum of five years. With the applied conventional analytical techniques it is possible to detect structural changes of both types of polyethylene induced by gamma irradiation and certainly of thermal treatment. Through gamma irradiation melting temperature, crystallinity, and density, respectively increased. Furthermore both polyethylenes get oxidized and cross-linked. With regard to the special application as neutron radiation shielding material in casks for storage and transport of radioactive materials, the impact of irradiation lead to changes of material properties. A consolidated view indicates that the detected changes of the irradiated (U)HMW-PE are not safety relevant for long-term neutron radiation shielding purposes over a period of 40 years in Germany.
Gamma radiation induced effects in perfluorinated polymer optical fibers for sensing applications
(2015)
Radiation induced attenuation in perfluorinated polymer optical fiber was investigated as a potential mean for online. in situ gamma radiation monitoring. Spectral dependence of radiation induced attenuation was measured in the visible and near infrared range. Attenuation spectrum exhibits sharp increase both towards the ultraviolet and infrared side of the spectrum with 3 distinct peaks around 1400 nm. The fiber sensitivity to gamma radiation was further evaluated at two commonly used IR wavelengths (1310nm and l550nm} by pre- and post-irradiation optical time-domain reflectometry measurements. The examined fiber is sensitive up to lOO kGy of total absorbed dose with only minor saturation towards the large dose values. The influence of gamma radiation on the fiber mechanical properties was studied as well. Up to the maximal dose of 100 kGy, no significant deterioration of fiber strength and elasticity was observed.
The paper presents the first complex study of Gamma radiation effects on a low-loss perfluorinated polymer optical fiber (PF-POF) based on Cytop® polymer. Influence of gamma radiation on fiber’s optical, mechanical and climatic performance is investigated. The radiation-induced attenuation (RIA) in the visible and near-infrared region (0.4 μm-1.7 mm) is measured and its origins are discussed. Besides attenuation increase, radiation is also shown to decrease the thermal degradation stability of the fiber and to increase its susceptibility to water. With regard to complex fiber transmission performance upon irradiation, the optimal operation wavelength region of PF-POF-based systems intended for use in Radiation environments is determined to be around 1.1 μm. On the other hand, the investigated fiber holds potential for low-cost RIA-based optical fiber dosimetry applications with sensitivity as high as 260 dBm⁻¹/kGy in the visible region.
Impact of gamma radiation on transmission of a commercial Cytop polymer optical fibre (Lucina, Asahi Glass Company) is investigated. Spectral dependence of radiation induced attenuation in the investigated fibre is measured in the VIS-NIR spectral region. Besides attenuation increase, radiation is found to increase fibre susceptibility to water as well. While pristine Cytop fibre is rather humidity insensitive, strong humidity related absorption in the NIR region is observed after fibre irradiation. Selective irradiation of separate fibre sections is proposed as a way of fibre humidity sensitization and quasi-distributed water detection is demonstrated using optical time domain reflectometry at 1310 nm.
Sensitivity of two commercial perfluorinated (PF) polymer optical fibers (POFs) to gamma radiation was measured, compared and exploited for dosimetry purposes. Fiber radiation induced attenuation (RIA) was found to be highly wavelength dependent and pronounced towards the UV part of the spectrum. PF-POFs were shown to be highly radiation sensitive and RIA-based on-line radiation monitoring with sensitivity as high as 135 dBm-1/kGy was demonstrated at 460 nm with co-extruded PF-POF. In addition, thanks to low inherent attenuation in the near-infrared region, possibility of distributed radiation detection with PF-POFs was demonstrated for the first time, utilizing optical time domain reflectometry.
Application importance of ionizing radiation has been growing steadily over the last decades. Extensive utilization of ionizing radiation generates demand for development of suitable monitoring techniques. Radiation monitoring systems based on optical fibers offer several key advantages such as small footprint, possibility of remote and real-time measurement as well as electromagnetic immunity. In this contribution, we investigate radiation-induced attenuation (RIA)-based sensing with perfluorinated polymer optical fibers (PF-POFs). The RIA response of two commercial PF-POFs is assessed in a low dose region and performance and limitations of the system are discussed. The concept represents a potential high-sensitivity, low-cost and easy-to-use on-line radiation monitoring system with distributed detection capability
The sensitivity of low loss perfluorinated polymer optical fiber (PF-POF) to gamma radiation is investigated for on line radiation monitoring purposes. The radiation induced attenuation (RIA) of a commercial PF-POF based on Cytop material is measured in the visible spectral region. The fiber RIA shows strong wavelength dependence with rapid increase towards the blue side of the spectrum. The wide range of radiation sensitivities is available via careful selection of appropriate monitoring wavelength. The accessible sensitivities span from 1.99 ± 0.01 dBm⁻¹/kGy measured at 890 nm to 140.9 ± 0.6 dBm⁻¹/kGy measured at 460 nm. The fairly high radiation sensitivity as well as its wide tunability makes the fiber a promising candidate for a broad range of applications.