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Influence of Slip Viscosity on the Mechanical Properties of High Purity Alumina made by Gelcasting
(1997)
Polyvalent Ions - Their Behaviour in the Glass Melt and their Influence on Glass Crystallisation
(1998)
Laser ablation of single-crystalline indium phosphide (InP) was performed in air by means of linearly polarized Ti:sapphire femtosecond-pulses (800 nm, 130 fs, 10 Hz). As a result of the first laser pulses, several morphological changes (crater formation, rim formation, ripple structures and cones) were observed. These effects were explored using force modulation microscopy (FMM), a technique based on scanning force microscopy (SFM), allowing the simultaneous imaging of both topography and local stiffness at a high lateral resolution. The first laser pulse induces the formation of a protruding rim (height <20 nm, width ~300 nm) bordering the ablated crater. A Fourier-analysis of the multi-pulse generated topographies reveals the formation of wavelength-sized periodic ripples (modulation depth <100 nm) with an orientation perpendicular to that of the electric field vector of the laser radiation. Besides these morphological alterations, also material modifications were observed in the irradiated regions by means of the FFM technique. Within the ablated craters, local stiffness variations were found revealing an inhomogeneous material composition/structure as a consequence of the femtosecond pulse laser treatment.
Modern structural integrity assessment procedures in the field of nuclear related technology incorporate fracture
mechanical concepts. Therefore, they inevitably require the availability of both, loading parameters as well as material
characteristics in terms of fracture mechanical quantities. Especially in case of dynamic loading conditions, the methods
for the determination of the loading parameters need further improvement and there is a lack of material characteristics
as well. In Germany, ductile cast iron (DCI) is used for heavy-sectioned casks for radioactive materials. New developments
in cask design and efforts to extend the application limits require further investigations. The present study is part
of an ongoing fracture mechanics research programme of BAM which is focused on the systematic mechanical and
fracture mechanical material characterisation of DCI materials under dynamic loading conditions. In this study, results
of fracture mechanics investigations on ductile cast iron from an original DCI container with a wide variety of microstructure
under dynamic loading conditions in the temperature range from -50 °C to +22 °C are presented. Large scale
as well as small scale single edge crack bend specimens SE(B) with thicknesses of 140 mm and 15 mm, respectively
were tested. Furthermore, it is reported on the results of a finite element simulation of the dynamic large scale fracture
mechanics tests. Strength and deformation characteristics were determined in dynamic tensile tests. They are discussed
with respect to the influence of pearlite content and test temperature. The material specific experimental difficulties in
the determination of reliable dynamic crack initiation toughness values of DCI are outlined.
Structure formation on the surface of indium phosphide irradiated by femtosecond laser pulses
(2005)
Laser-induced periodic surface structures (LIPSS; ripples) with different spatial characteristics have been observed after irradiation of single-crystalline indium phosphide (c-InP) with multiple linearly polarized femtosecond pulses (130 fs, 800 nm) in air. With an increasing number of pulses per spot, N, up to 100, a characteristic evolution of two different types of ripples has been observed, i.e., (i) the growth of a grating perpendicular to the polarization vector consisting of nearly wavelength-sized periodic lines and (ii), in a specific pulse number regime (N = 530), the additional formation of equally oriented ripples with a spatial period close to half of the laser wavelength. For pulse numbers higher than 50, the formation of micrometer-spaced grooves has been found, which are oriented perpendicular to the ripples. These topographical surface alterations are discussed in the frame of existing LIPSS theories.
This paper deals with life prediction by observation and simulation of short fatigue cracks in cyclically loaded smooth and notched specimens made of 0.15 wt-% carbon steel SAE1017. The measured crack behaviour was simulated in a microstructural environment. Reference tests under constant amplitude loading allowed to determine model parameters and hence a reasonable life prediction by simulation resulted even for service loading. Short crack behaviour was a measurable property for damage also to compare smooth and notched specimens.