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Warfarin ist seit den 1950er Jahren einer der bekanntesten Gerinnungshemmer. Beim Menschen wird es bis heute zur Vorbeugung von Thrombose und der Behandlung von Vorhofflimmern und Arrhythmie eingesetzt. Doch schon einige Jahre vor der FDA Zulassung (U. S. Food and Drug Administration) als Medikament wurde es zur Bekämpfung von Nagetieren eingesetzt. Bis heute wurde es nur teilweise durch weitaus wirksamere antikoagulante Rodentizide (ARs) der zweiten Generation, sogenannte Superwarfarine, ersetzt. In der Fachliteratur finden sich zahlreiche Beispiele für sekundäre und tertiäre Vergiftung mit ARs bei Wildtieren und anderen Nichtzieltieren. Bisher ist relativ wenig über die Bioakkumulation, Persistenz und Toxizität von ARs und deren Transformationsprodukten (TPs) in der terrestrischen und aquatischen Umwelt, sowie der Nahrungskette bekannt.
Um Einblicke in mögliche Transformations- und Abbauprozesse von Warfarin unter umweltrelevanten Bedingungen zu erhalten und um diese Einflüsse zu simulieren, wurde hierzu eine elektrochemische Reaktorzelle in Kopplung mit einem Massenspektrometer verwendet. So können mögliche Phase-I-Metabolite und sogenannte „oxidation products“ vorausgesagt werden. Hinsichtlich des Verhaltens während der Wasseraufbereitung in Kläranlagen wurden technisch relevante Prozesse wie Chlorung, UV-Bestrahlung und Ozonung in Modellen simuliert, um hier potenzielle Abbauwege und -prozesse aufzuklären. Gebildete Transformationsprodukte wurden daher mittels unterschiedlicher chromatografischer Verfahren getrennt und massenspektrometrisch identifiziert, charakterisiert und verglichen.
Wood-destroying pests such as Anobium punctatum and Xestobium rufovillosum cause damage to art and cultural objects as well as to buildings. Monitoring population dynamics of pest species as well as of their naturally occurring counterparts are an essential part in the development of biological control measures as alternatives to conventional wood protection. Therefore, both the dispersal and homogeneity of pest and beneficial insect populations across multiple sites and buildings were investigated in the present study using DNA barcoding. Specifically, beetles of Anobium punctatum (de Geer 1774) (Coleoptera, Ptinidae), Xestobium rufovillosum (de Geer, 1974) (Coloeptera, Ptinidae), and Korynetes caeruleus (de Geer 1775) (Coleoptera, Cleridae) were collected from buildings at four different sites in Mecklenburg-Western Pomerania, North-Eastern Germany. DNA analysis was performed using mitochondrial cytochrome c oxidase subunit I (COI). For A. punctatum, low base pair variability was found in the gene segment studied (4-5 SNPs) within one building (Greven) and between four spatially separated sites. Conversely, in X. rufovillosum, the sequences from two sites studied were homogeneous within a site but differed between locations by nine base pair positions (SNPs). The main result of this study is that the pests A. punctatum and X. rufovillosum showed a higher variability in the investigated gene segment than the natural counterpart K. caeruleus.
Häufig stellt sich die Frage, ob eine Materialinhomogenität kritisch für die strukturelle Integrität eines Bauteils ist. Dies ist häufig abhängig von der Größe und der Geometrie dieser Materialinhomogenität. Während die korrekte Bestimmung einer Defektgröße zweifelsfrei eine Messaufgabe darstellt, ist die Detektion eines Materialdefekts die Hauptaufgabe eines Prüfsystems. Allerdings sind manche Defekte zu klein, um detektiert zu werden. Es ist jedoch schwierig, etwas zu bemessen, was nur schwer gefunden werden kann, stellen sowohl die Detektion als auch die Fähigkeit den Defekt zu bemaßen, Teile der der Bewertung eines Prüfsystems dar. Die vorliegende Publikation beschäftigt sich zum einen mit der Notwendigkeit, die Auffindwahrscheinlichkeit von Prüfverfahren zu bewerten, und zum anderen mit den Schritten, mit denen das Konzept der Prüfunsicherheitsbewertung national und international vorangetrieben wird. Final werden die Methoden evaluiert, die den Schulterschluss zwischen Prüf- und Messunsicherheitsbestimmung ermöglichen. Ergänzt wird der Artikel mit Beispielen aus der Industrie, welche die aktuelle Relevanz des Themas untermauern.
Concrete-glass windows or commonly referred to as “Dalle de Verre” windows are prevalent in historical monuments across Europe. “Dalle de Verre” windows were made by placing cut stained glasses, of various shapes and sizes, into a steel reinforced concrete frame. In addition to the steel reinforcement, a few steel wires run across the concrete elements to hold the glass windows into place. Much of these structures have been damaged due to carbonation of the thin concrete covers and consequent corrosion of the steel reinforcement; and exhibit several cracks due to the expansive nature of corrosion products formed at the steel–concrete interface. This study focussed on understanding the efficacy of electrochemical realkalisation in reinstating the passive state of the steel reinforcement embedded in such concrete glass windows. Simulant “Dalle de Verre” windows (representative of windows at Kaiser-Wilhelm Gedächtniskirche) were produced using different cements with a water/cement ratio of 0.6 and carbonated under accelerated conditions. Post carbonation, the concrete glass windows were electrochemically realkalised using a sacrificial anode. The influence of highly alkaline conditions due to electrochemical realkalisation on the glass-concrete interface has also been investigated. This study shows that the passive state of the steel reinforcement in “Dalle de Verre” windows, particularly at the Kaiser-Wilhelm Gedächtniskirche (memorial church) in Berlin, can be reinstated using the electrochemical realkalisation method.
The study deals with the influence of the heat input on the thermal cycles and Charpy impact toughness for hybrid laser-arc welding of 25 mm thick structural steel S355J2 using a 20-kW high-power laser in combination with an electromagnetic weld pool support. The main focus is on the change of the mechanical properties over the entire seam thickness. The cooling times were measured using a pyrometer in combination with an optical fibre in three different locations near to fusion lines corresponding to different heights of the seam. Also, Charpy impact specimens were taken from different parts of the weld joint corresponding to the different heights. The influence of the heat input was investigated for 1.8 kJ mm-1 and 3.2 kJ mm-1. Despite the observed decreased values of both t8/5-cooling time and the Charpy impact toughness in the root part of the seam, the required values could be reached in dependance on applied heat input.
This paper presents first advances in the area of aerial chemical trail following. For that purpose, we equipped a palm-size aerial robot, based on the Crazyflie 2.0 quadrocopter, with a small lightweight metal oxide gas sensor for measuring evaporated ethanol from chemical trails. To detect and localize the chemical trail, a novel detection criterion was developed that uses only relative changes in the transient phase of the sensor response, making it more robust in its application. We tested our setup in first crossing-trail experiments showing that our flying ant robot is able to correlate an odor hit with the chemical trail within 0.14 m. Principally, this could enable aerial chemical trail following in the future.
Ultrashort pulse laser materials processing can be accompanied by the production of X-rays. Small doses per laser pulse can accumulate to significant dose rates at high laser pulse repetition rates which may exceed the permitted X-ray limits for human exposure. Consequently, a proper radiation shielding must be considered in laser machining. A brief overview of the current state of the art in the field of undesired generation of X-ray radiation during ultrashort pulse laser material processing in air is presented.
This article presents a solid cohesion model for the simulation of bonded granular assemblies in the frame of 3D discrete element approaches (DEM). A simple viscoplastic cohesion model for 2D geometries is extended to 3D conditions, while its yield criterion is generalized as a hyper-surface in the space of bond solicitations to include torsional moments. The model is then calibrated using experimental results of uniaxial traction at both the microscopic and macroscopic scales with an artificial granular cohesive soil. The paper finally presents some simulated results on the macromechanical sample traction application and briefly discusses the model's current limitations and promising prospects for subsequent works.
Wireless sensor networks provide occupational health experts with valuable information about the distribution of air pollutants in an environment. However, especially low-cost sensors may produce faulty measurements or fail completely. Consequently, not only spatial coverage but also redundancy should be a design criterion for the deployment of a sensor network. For a sensor network deployed in a steel factory, we analyze the correlations between sensors and build machine learning forecasting models, to investigate how well the sensor network can compensate for the outage of sensors. While our results show promising prediction quality of the models, they also indicate the presence of spatially very limited events. We, therefore, conclude that initial measurements with, e.g., mobile units, could help to identify important locations to design redundant sensor networks.
In this work, we present our results achieved in several research activities for development of distributed fiber optic radiation sensors using glass and polymer optical fibers. The findings show that both the measurement of the radiation-induced attenuation (RIA) along the entire sensing fiber and the accompanying change in the refractive index of the fiber core can be used for distributed radiation monitoring.