Zitieren Sie bitte immer diesen URN: urn:nbn:de:kobv:b43-647405
Beyond conventional calorimetry: Unlocking thermal characterization with fast scanning techniques
- Fast scanning calorimetry (FSC) has emerged as a transformative technique in thermal analysis, enabling the investigation of rapid and kinetically driven thermal transitions that are inaccessible to conventional differential scanning calorimetry. This review highlights the capabilities enabled by FSC for studying a wide range of materials under extreme thermal conditions, including polymers, pharmaceuticals, metallic glasses, nanocomposites, and hydrogels. By employing ultrafast heating and cooling rates, FSC allows for the suppression of crystallization, resolution of weak transitions, and analysis of thermally labile or size-limited samples. The technique is particularly valuable for probing glass transitions, relaxation phenomena, and phase behavior in systems with complex morphologies or confined geometries. Case studies demonstrate the use of FSC in characterizing vitrification, physical aging, and interfacial dynamics, as well as its application in emerging fields such asFast scanning calorimetry (FSC) has emerged as a transformative technique in thermal analysis, enabling the investigation of rapid and kinetically driven thermal transitions that are inaccessible to conventional differential scanning calorimetry. This review highlights the capabilities enabled by FSC for studying a wide range of materials under extreme thermal conditions, including polymers, pharmaceuticals, metallic glasses, nanocomposites, and hydrogels. By employing ultrafast heating and cooling rates, FSC allows for the suppression of crystallization, resolution of weak transitions, and analysis of thermally labile or size-limited samples. The technique is particularly valuable for probing glass transitions, relaxation phenomena, and phase behavior in systems with complex morphologies or confined geometries. Case studies demonstrate the use of FSC in characterizing vitrification, physical aging, and interfacial dynamics, as well as its application in emerging fields such as additive manufacturing, supramolecular systems, and neuromorphic materials. Together, these examples underscore the role that FSC plays in advancing the understanding of structure-property relationships across diverse material classes.…


| Autor*innen: | Mateusz Dudziak, Birte Riechers, Robert MaaßORCiD, Adam MichalchukORCiD, Andreas SchönhalsORCiD, Paulina SzymoniakORCiD |
|---|---|
| Dokumenttyp: | Zeitschriftenartikel |
| Veröffentlichungsform: | Verlagsliteratur |
| Sprache: | Englisch |
| Titel des übergeordneten Werkes (Englisch): | Thermochimica Acta. Special issue: Recent advancements on application of calorimetric techniques to characterize the glass transition and physical aging of glasses |
| Jahr der Erstveröffentlichung: | 2025 |
| Organisationseinheit der BAM: | 5 Werkstofftechnik |
| 5 Werkstofftechnik / 5.0 Abteilungsleitung und andere | |
| 6 Materialchemie | |
| 6 Materialchemie / 6.1 Oberflächen- und Dünnschichtanalyse | |
| 7 Bauwerkssicherheit | |
| 7 Bauwerkssicherheit / 7.5 Technische Eigenschaften von Polymerwerkstoffen | |
| Veröffentlichende Institution: | Bundesanstalt für Materialforschung und -prüfung (BAM) |
| Verlag: | Elsevier B.V. |
| Jahrgang/Band: | 754 |
| Aufsatznummer: | 180177 |
| Erste Seite: | 1 |
| Letzte Seite: | 14 |
| DDC-Klassifikation: | Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Ingenieurwissenschaften und zugeordnete Tätigkeiten |
| Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Sanitär- und Kommunaltechnik; Umwelttechnik | |
| Freie Schlagwörter: | Calorimetry; Flash DSC; Glass transition |
| Themenfelder/Aktivitätsfelder der BAM: | Material |
| Material / Advanced Materials | |
| Umwelt | |
| Umwelt / Circular Economy | |
| DOI: | 10.1016/j.tca.2025.180177 |
| URN: | urn:nbn:de:kobv:b43-647405 |
| ISSN: | 1872-762X |
| Verfügbarkeit des Dokuments: | Datei für die Öffentlichkeit verfügbar ("Open Access") |
| Lizenz (Deutsch): | Creative Commons - CC BY - Namensnennung 4.0 International |
| Datum der Freischaltung: | 19.11.2025 |
| Referierte Publikation: | Ja |
| Datum der Eintragung als referierte Publikation: | 27.05.2026 |
| Schriftenreihen ohne Nummerierung: | Wissenschaftliche Artikel der BAM |


