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Detailed investigation of capillary active insulation materials by 1H nuclear magnetic resonance (NMR) and thermogravimetric drying

  • Capillary active interior insulation materials are an important approach to minimize energy losses of historical buildings. A key factor for their performance is a high liquid conductivity, which enables redistribution of liquid moisture within the material. We set up an experiment to investigate the development of moisture profiles within two different interior insulation materials, calcium-silicate (CaSi) and expanded perlite (EP), under constant boundary conditions. The moisture profiles were determined by two different methods: simple destructive sample slicing with subsequent thermogravimetric drying as well as non-destructive NMR measurements with high spatial resolution. The moisture profiles obtained from both methods show good agreement, when compared at the low spatial resolution of sample slicing, which demonstrates the reliability of this method. Moreover, the measured T2- relaxation-time distributions across the sample depth were measured, which may give further insightCapillary active interior insulation materials are an important approach to minimize energy losses of historical buildings. A key factor for their performance is a high liquid conductivity, which enables redistribution of liquid moisture within the material. We set up an experiment to investigate the development of moisture profiles within two different interior insulation materials, calcium-silicate (CaSi) and expanded perlite (EP), under constant boundary conditions. The moisture profiles were determined by two different methods: simple destructive sample slicing with subsequent thermogravimetric drying as well as non-destructive NMR measurements with high spatial resolution. The moisture profiles obtained from both methods show good agreement, when compared at the low spatial resolution of sample slicing, which demonstrates the reliability of this method. Moreover, the measured T2- relaxation-time distributions across the sample depth were measured, which may give further insight into the saturation degree of the different pore sizes. In order to explain differences in the moisture profiles between CaSi and EP, we determined their pore-size distribution with different methods: conversion of the NMR T2 relaxationtime distribution at full saturation, mercury intrusion porosimetry and indirect determination from pressure plate measurements. CaSi shows a unimodal distribution at small pore diameters, while in EP, a bi-modal or wider distribution was found. We assume that the smaller pore diameters of CaSi lead to a higher capillary conductivity, which causes a more distributed moisture profile in comparison with that of EP.zeige mehrzeige weniger

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Metadaten
Autor*innen:Thilo Bintz
Koautor*innen:Sarah Munsch, Rüdiger Heyn, Hauke Hirsch, John Grunewald, Sabine Kruschwitz
Dokumenttyp:Vortrag
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2022
Organisationseinheit der BAM:8 Zerstörungsfreie Prüfung
8 Zerstörungsfreie Prüfung / 8.0 Abteilungsleitung und andere
DDC-Klassifikation:Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Ingenieurwissenschaften und zugeordnete Tätigkeiten
Freie Schlagwörter:Capillary conductivity; Insulation material; Nuclear magnetic resonance; Pore-size distribution
Themenfelder/Aktivitätsfelder der BAM:Chemie und Prozesstechnik
Material
Veranstaltung:NDT-CE
Veranstaltungsort:Zurich, Switzerland
Beginndatum der Veranstaltung:16.08.2022
Enddatum der Veranstaltung:18.08.2022
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:17.07.2023
Referierte Publikation:Nein
Eingeladener Vortrag:Nein
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