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Determining the pore size distribution in synthetic and building materials using 1D NMR

  • The detection of moisture in building materials has a high priority in civil engineering to locate and prevent possible moisture damages, e.g. mold, corrosion, delamination etc. Furthermore, it is of great significancy to achieve a better understanding of moisture transport and pore space in different materials. To prevent the degeneration of structures and materials, non-destructive testing methods are more and more deployed. As a non-destructive method in this work, nuclear magnetic resonance (NMR) is applied using a strayfield open magnet device that enables one-dimensional measurements in a defined volumen. By using NMR, the water content of the sample can be determined and also the pore size distribution can be deduced from the relaxation time distribution when having a comparison method like mercury intrusion porosimetry. In this study different synthetic homogenous materials with defined and almost unimodal pore size distributions are investigated as well as building materialsThe detection of moisture in building materials has a high priority in civil engineering to locate and prevent possible moisture damages, e.g. mold, corrosion, delamination etc. Furthermore, it is of great significancy to achieve a better understanding of moisture transport and pore space in different materials. To prevent the degeneration of structures and materials, non-destructive testing methods are more and more deployed. As a non-destructive method in this work, nuclear magnetic resonance (NMR) is applied using a strayfield open magnet device that enables one-dimensional measurements in a defined volumen. By using NMR, the water content of the sample can be determined and also the pore size distribution can be deduced from the relaxation time distribution when having a comparison method like mercury intrusion porosimetry. In this study different synthetic homogenous materials with defined and almost unimodal pore size distributions are investigated as well as building materials like screed. For analyzing the pore space, the samples were measured at different saturation levels and the building materials at different hydration states as well.zeige mehrzeige weniger

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Metadaten
Autor*innen:Sarah Mandy Munsch
Koautor*innen:Christoph Strangfeld, Sabine Kruschwitz
Dokumenttyp:Posterpräsentation
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2018
Organisationseinheit der BAM:8 Zerstörungsfreie Prüfung
8 Zerstörungsfreie Prüfung / 8.2 Zerstörungsfreie Prüfmethoden für das Bauwesen
DDC-Klassifikation:Naturwissenschaften und Mathematik / Chemie / Analytische Chemie
Freie Schlagwörter:Mercury intrusion porosimetry; NMR relaxometry; Pore size; Synthetic and building materials
Themenfelder/Aktivitätsfelder der BAM:Chemie und Prozesstechnik
Veranstaltung:Magnetic Resonance in Porous Media 14
Veranstaltungsort:Gainesville, FL, USA
Beginndatum der Veranstaltung:18.02.2018
Enddatum der Veranstaltung:22.02.2018
URN:urn:nbn:de:kobv:b43-443868
Bemerkung:
Geburtsname von Munsch, Sarah Mandy: Nagel, S. M. -  Birth name of Munsch, Sarah Mandy: Nagel, S. M.
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:05.03.2018
Referierte Publikation:Nein
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