In situ tomographic imaging with hard x rays at Bamline (BESSY II)
- The BAMline at the synchrotron X-ray source BESSY II (Berlin, Germany) is supporting researchers especially in materials science [1]. As a non-destructive characterization method, synchrotron X-ray imaging, especially tomography (SXCT) with hard X-Rays, plays an important role in structural 3D characterization. The imaging capabilities allow for in-situ and operando experiments. In this presentation the equipment, data handling pipeline as well as various examples from material science are presented. In series-connected lithium-ion cells are susceptible to an electrical safety hazard called over-discharge. Here the behavior of copper dissolution and deposition during over-discharge is presented, which leads to irreversible loss of capacity and internal short circuits. The concentration of dissolved and deposited copper is quantified. Also, a non-uniform distribution pattern of copper deposition on the cathode is shown. The second example deals with an Al alloy 7017 customized for aThe BAMline at the synchrotron X-ray source BESSY II (Berlin, Germany) is supporting researchers especially in materials science [1]. As a non-destructive characterization method, synchrotron X-ray imaging, especially tomography (SXCT) with hard X-Rays, plays an important role in structural 3D characterization. The imaging capabilities allow for in-situ and operando experiments. In this presentation the equipment, data handling pipeline as well as various examples from material science are presented. In series-connected lithium-ion cells are susceptible to an electrical safety hazard called over-discharge. Here the behavior of copper dissolution and deposition during over-discharge is presented, which leads to irreversible loss of capacity and internal short circuits. The concentration of dissolved and deposited copper is quantified. Also, a non-uniform distribution pattern of copper deposition on the cathode is shown. The second example deals with an Al alloy 7017 customized for a 3d-printing process by means of laser-based powder bed fusion (PBF-LB) technique. These advanced alloys have a significantly higher modulus of elasticity than conventional Al alloys, making them attractive for applications requiring high stiffness. SXCT during In-situ tensile tests confirmed that fracture initiation strongly depends on defects created during printing. However, the cracks are deflected from decohesion around inclusions/precipitates embedded in the Al matrix, increasing ductility. Low temperature cofired ceramic (LTCC) multilayer housings offer 3D-circuits for a wide range of applications in telecommunications, microsystems and sensor technology. Such housings are produced by combining structured and metallized ceramic layers using tape-casting and multilayer technology. The characterization of the integrity, deformation, defects, and positioning of the internal metal features was carried out using in-situ SXCT at up to 950°C. A high-precision nail penetration tool was developed to characterize the mechanically induced thermal runaway (TR) of lithium-ion battery (LIB) cells in a dynamic temperature range down to -190 °C. To investigate safety-specific low-temperature transport conditions, the damaged cells were tomographically imaged during thawing.…
Autor*innen: | Henning Markötter |
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Koautor*innen: | Michael Sintschuk, Shahabeddin Dayani, Tatiana Mishurova, B. Mehta, Mustapha Eddah, Björn MiellerORCiD, Nils Böttcher, Jonas Krug von Nidda |
Dokumenttyp: | Vortrag |
Veröffentlichungsform: | Präsentation |
Sprache: | Englisch |
Jahr der Erstveröffentlichung: | 2024 |
Organisationseinheit der BAM: | 3 Gefahrgutumschließungen; Energiespeicher |
3 Gefahrgutumschließungen; Energiespeicher / 3.1 Sicherheit von Gefahrgutverpackungen und Batterien | |
5 Werkstofftechnik | |
5 Werkstofftechnik / 5.4 Multimateriale Fertigungsprozesse | |
8 Zerstörungsfreie Prüfung | |
8 Zerstörungsfreie Prüfung / 8.5 Röntgenbildgebung | |
DDC-Klassifikation: | Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Angewandte Physik |
Freie Schlagwörter: | Li-ion battery; Synchrotron radiation; X-ray tomography |
Themenfelder/Aktivitätsfelder der BAM: | Energie |
Energie / Elektrische Energiespeicher und -umwandlung | |
Veranstaltung: | ICTMS - International Conference on Materials and Structures 2024 |
Veranstaltungsort: | Cape Town, South Africa |
Beginndatum der Veranstaltung: | 01.07.2024 |
Enddatum der Veranstaltung: | 05.07.2024 |
Verfügbarkeit des Dokuments: | Datei im Netzwerk der BAM verfügbar ("Closed Access") |
Datum der Freischaltung: | 18.07.2024 |
Referierte Publikation: | Nein |
Eingeladener Vortrag: | Ja |