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Sintering and piezoelectric properties of K0.5Na0.5NbO3 glass microspheres

  • Laser-fused K0.5Na0.5NbO3 (KNN) powder of 75% transparent fraction has been sintered by pressureless sintering, spark plasma sintering (SPS), and hot isostatic pressing (HIP). The laser-fused KNN has a fictive temperature of 503 °C and an onset crystallization temperature of around 529 °C. The results have shown that sintering of the laser-fused KNN powder utilizing the viscous flow of the transparent microspheres (amorphous content)–at the kinetic window (26 °C)–is possible. The highest yield relative density is around 83% at a sintering temperature of 525 °C and at a sintering pressure of 280 MPa. Limited density has been reached because of formation of crystalline surface layers around the amorphous areas. The samples hipped at 525 °C have low piezoelectric coefficient d33 of 5 pC/N because of the residual porosity that led to early dielectric breakdown during the polarization. The sintering behavior, the resulting microstructure as well as the measured properties will beLaser-fused K0.5Na0.5NbO3 (KNN) powder of 75% transparent fraction has been sintered by pressureless sintering, spark plasma sintering (SPS), and hot isostatic pressing (HIP). The laser-fused KNN has a fictive temperature of 503 °C and an onset crystallization temperature of around 529 °C. The results have shown that sintering of the laser-fused KNN powder utilizing the viscous flow of the transparent microspheres (amorphous content)–at the kinetic window (26 °C)–is possible. The highest yield relative density is around 83% at a sintering temperature of 525 °C and at a sintering pressure of 280 MPa. Limited density has been reached because of formation of crystalline surface layers around the amorphous areas. The samples hipped at 525 °C have low piezoelectric coefficient d33 of 5 pC/N because of the residual porosity that led to early dielectric breakdown during the polarization. The sintering behavior, the resulting microstructure as well as the measured properties will be discussed.zeige mehrzeige weniger

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Metadaten
Autoren/innen:F. J. Hmood, Jens Günster, J. Heinrich
Dokumenttyp:Zeitschriftenartikel
Veröffentlichungsform:Verlagsliteratur
Sprache:Englisch
Titel des übergeordneten Werkes (Englisch):Journal of the European Ceramic Society
Jahr der Erstveröffentlichung:2015
Organisationseinheit der BAM:5 Werkstofftechnik
5 Werkstofftechnik / 5.4 Keramische Prozesstechnik und Biowerkstoffe
Herausgeber (Institution):European Ceramic Society
Verlag:Elsevier Ltd.
Verlagsort:Oxford
Jahrgang/Band:35
Ausgabe/Heft:15
Erste Seite:4143
Letzte Seite:4151
Freie Schlagwörter:Glass microspheres; KNN
DOI:https://doi.org/10.1016/j.jeurceramsoc.2015.07.035
URL:http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=Alerting&SrcApp=Alerting&DestApp=WOS&DestLinkType=FullRecord;UT=WOS:000361575800009
ISSN:0955-2219
ISSN:1873-619X
Verfügbarkeit des Volltexts:Volltext-PDF im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:20.02.2016
Referierte Publikation:Ja
Datum der Eintragung als referierte Publikation:25.11.2015