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Precipitation of T1 and theta′ Phase in Al‐4Cu‐1Li‐0.25Mn During Age Hardening: Microstructural Investigation and Phase‐Field Simulation
- Experimental and phase field studies of age hardening response of a high purity Al‐4Cu‐1Li‐0.25Mn‐alloy (mass %) during isothermal aging are conducted. In the experiments, two hardening phases are identified: the tetragonal θ′ (Al₂Cu) phase and the hexagonal T1 (Al₂CuLi) phase. Both are plate shaped and of nm size. They are analyzed with respect to the development of their size, number density and volume fraction during aging by applying different analysis techniques in TEM in combination with quantitative microstructural analysis. 3D phase‐field simulations of formation and growth of θ′ phase are performed in which the full interfacial, chemical and elastic energy contributions are taken into account. 2D simulations of T1 phase are also investigated using multi‐component diffusion without elasticity. This is a first step toward a complex phase‐field study of T1 phase in the ternary alloy. The comparison between experimental and simulated data shows similar trends. The stillExperimental and phase field studies of age hardening response of a high purity Al‐4Cu‐1Li‐0.25Mn‐alloy (mass %) during isothermal aging are conducted. In the experiments, two hardening phases are identified: the tetragonal θ′ (Al₂Cu) phase and the hexagonal T1 (Al₂CuLi) phase. Both are plate shaped and of nm size. They are analyzed with respect to the development of their size, number density and volume fraction during aging by applying different analysis techniques in TEM in combination with quantitative microstructural analysis. 3D phase‐field simulations of formation and growth of θ′ phase are performed in which the full interfacial, chemical and elastic energy contributions are taken into account. 2D simulations of T1 phase are also investigated using multi‐component diffusion without elasticity. This is a first step toward a complex phase‐field study of T1 phase in the ternary alloy. The comparison between experimental and simulated data shows similar trends. The still unsaturated volume fraction indicates that the precipitates are in the growth stage and that the coarsening/ripening stage has not yet been reached.…
Autor*innen: | Ines Häusler, C. Schwarze, M. Umer Bilal, D. Valencia Ramirez, W. Hetaba, Reza Darvishi KamachaliORCiD, Birgit SkrotzkiORCiD |
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Dokumenttyp: | Zeitschriftenartikel |
Veröffentlichungsform: | Verlagsliteratur |
Sprache: | Englisch |
Titel des übergeordneten Werkes (Englisch): | Materials |
Jahr der Erstveröffentlichung: | 2017 |
Veröffentlichende Institution: | Bundesanstalt für Materialforschung und -prüfung (BAM) |
Verlag: | MDPI |
Verlagsort: | Basel, Schweiz |
Jahrgang/Band: | 10 |
Ausgabe/Heft: | 2 |
Erste Seite: | Article 117, 1 |
Letzte Seite: | 21 |
DDC-Klassifikation: | Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften |
Freie Schlagwörter: | Age hardening; Al‐Cu‐Li‐alloy; Elasticity; Growth kinetics; Microstructure; Multi‐component diffusion; Number density; Phase‐field modeling; Precipitates; Volume fraction |
DOI: | 10.3390/ma10020117 |
URN: | urn:nbn:de:kobv:b43-390473 |
ISSN: | 1996-1944 |
Verfügbarkeit des Dokuments: | Datei für die Öffentlichkeit verfügbar ("Open Access") |
Lizenz (Deutsch): | Creative Commons - Namensnennung |
Datum der Freischaltung: | 30.01.2017 |
Referierte Publikation: | Ja |
Datum der Eintragung als referierte Publikation: | 07.04.2017 |
Schriftenreihen ohne Nummerierung: | Wissenschaftliche Artikel der BAM |