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Oxidative ageing of elastomers: experiment and modelling

  • During an extensive test programme at the Bundesanstalt für Materialforschung und prüfung, material property changes of EPDM O-rings were investigated at different ageing times and an ageing temperature of 125 °C. To exclude possible diffusion limited oxidation (DLO) effects that can distort the data, IRHD micro hardness measurements were performed over the cross-section of compressed O-rings. Continuous stress relaxation measurements were conducted on samples free of DLO effects. The additional effect of physical processes to irreversible chemical ones during a long-term thermal exposure is quantified by the analysis of compression set measurements under various test conditions. By combining the different experimental methods, characteristic times relative to the degradation processes were determined. On the basis of experimental data, a microphysically motivated model that takes into account reversible and irreversible processes was developed. The parameter identification strategyDuring an extensive test programme at the Bundesanstalt für Materialforschung und prüfung, material property changes of EPDM O-rings were investigated at different ageing times and an ageing temperature of 125 °C. To exclude possible diffusion limited oxidation (DLO) effects that can distort the data, IRHD micro hardness measurements were performed over the cross-section of compressed O-rings. Continuous stress relaxation measurements were conducted on samples free of DLO effects. The additional effect of physical processes to irreversible chemical ones during a long-term thermal exposure is quantified by the analysis of compression set measurements under various test conditions. By combining the different experimental methods, characteristic times relative to the degradation processes were determined. On the basis of experimental data, a microphysically motivated model that takes into account reversible and irreversible processes was developed. The parameter identification strategy of the material model is based on our experimental investigations on homogeneously aged elastomer O-rings. The simulated results are in good agreement with the experiments.zeige mehrzeige weniger

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Metadaten
Autor*innen:Maha Zaghdoudi
Koautor*innen:Anja Kömmling, Matthias Jaunich, Dietmar Wolff
Dokumenttyp:Vortrag
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2021
Organisationseinheit der BAM:3 Gefahrgutumschließungen; Energiespeicher
3 Gefahrgutumschließungen; Energiespeicher / 3.4 Sicherheit von Lagerbehältern
DDC-Klassifikation:Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Ingenieurwissenschaften und zugeordnete Tätigkeiten
Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Angewandte Physik
Freie Schlagwörter:Compression set; Compression stress relaxation; IRHD micro hardness; Modelling
Themenfelder/Aktivitätsfelder der BAM:Energie
Energie / Kerntechnische Entsorgung
Material
Material / Degradation von Werkstoffen
Veranstaltung:ACEX-14th International Conference on Advanced Computational Engineering and Experimenting
Veranstaltungsort:Malta
Beginndatum der Veranstaltung:04.07.2021
Enddatum der Veranstaltung:08.07.2021
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:19.07.2021
Referierte Publikation:Nein
Eingeladener Vortrag:Nein
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