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Measurement of detection efficiency and response functions for an Si(Li) x-ray spectrometer in the range 0.1-5 keV

  • Efficiency and response functions were determined for a modern commercial energy-dispersive x-ray spectrometer in the photon energy range 0.1-5 keV using dispersed and undispersed synchrotron radiation. The spectrometer was equipped with an Si(Li) detector crystal, a thin-film window and a digital pulse processor. Monochromatized synchrotron radiation from the PTB VUV radiometry beamline at the electron storage ring BESSY was used for the absolute determination of the detection efficiency with a typical relative uncertainty of 1-2% in the photon energy range 0.1-1.5 keV by direct comparison with calibrated photodiodes. At higher photon energies, the efficiency was found by comparison of the measured and calculated undispersed synchrotron radiation spectrum. The absolute intensity of the synchrotron radiation was known with a relative uncertainty of less than 1%. In the overlapping region, the results from the two independent experiments are in full agreement. The energy dependence ofEfficiency and response functions were determined for a modern commercial energy-dispersive x-ray spectrometer in the photon energy range 0.1-5 keV using dispersed and undispersed synchrotron radiation. The spectrometer was equipped with an Si(Li) detector crystal, a thin-film window and a digital pulse processor. Monochromatized synchrotron radiation from the PTB VUV radiometry beamline at the electron storage ring BESSY was used for the absolute determination of the detection efficiency with a typical relative uncertainty of 1-2% in the photon energy range 0.1-1.5 keV by direct comparison with calibrated photodiodes. At higher photon energies, the efficiency was found by comparison of the measured and calculated undispersed synchrotron radiation spectrum. The absolute intensity of the synchrotron radiation was known with a relative uncertainty of less than 1%. In the overlapping region, the results from the two independent experiments are in full agreement. The energy dependence of the measured efficiency can be explained only with a detector model assuming that there is no dead layer. A simple model for the effect of incomplete charge collection (ICC) was applied to describe the measured response functions. Consequences of the ICC such as broadening and shift of low-energy peaks and redistribution of counts around 1.84 keV are explained with the model, in accordance with the experimental results.zeige mehrzeige weniger

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Metadaten
Autor*innen:Mathias ProcopORCiD, F. Scholze
Dokumenttyp:Zeitschriftenartikel
Veröffentlichungsform:Verlagsliteratur
Sprache:Englisch
Titel des übergeordneten Werkes (Englisch):X-ray spectrometry
Jahr der Erstveröffentlichung:2001
Verlag:Wiley
Verlagsort:Chichester
Jahrgang/Band:30
Ausgabe/Heft:2
Erste Seite:69
Letzte Seite:76
DOI:10.1002/xrs.472
ISSN:0049-8246
Verfügbarkeit des Dokuments:Physisches Exemplar in der Bibliothek der BAM vorhanden ("Hardcopy Access")
Bibliotheksstandort:ZX 1
Datum der Freischaltung:19.02.2016
Referierte Publikation:Ja
Datum der Eintragung als referierte Publikation:07.06.2001
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