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Polymer Reference Materials: Round-Robin Tests for the Determination of Molar Masses
- This article reports round-robin tests dealing with static light scattering (LS), size exclusion chromatography (SEC), and viscometry measurements of 10 reference materials of various polymer classes: poly(styrene)s (PS), poly(methyl methacrylate)s (PMMA), poly(ethylene oxide)s (PEO), and poly(lactide)s (PLA). In the certificates, molar masses and intrinsic viscosities as well as their uncertainties are specified. Additional values from nuclear magnetic resonance (NMR), infrared spectroscopy (IR), differential scanning calorimetry (DSC), melt flow index (MFR), and matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS), which were determined exclusively in BAM laboratories are given, as well. These results represent the base for the BAM certification work of creating polymer reference materials according to the BAM Guidelines for the Production and Certification of BAM Reference Materials, a version of the European guidelines (BCR/01/97). TheseThis article reports round-robin tests dealing with static light scattering (LS), size exclusion chromatography (SEC), and viscometry measurements of 10 reference materials of various polymer classes: poly(styrene)s (PS), poly(methyl methacrylate)s (PMMA), poly(ethylene oxide)s (PEO), and poly(lactide)s (PLA). In the certificates, molar masses and intrinsic viscosities as well as their uncertainties are specified. Additional values from nuclear magnetic resonance (NMR), infrared spectroscopy (IR), differential scanning calorimetry (DSC), melt flow index (MFR), and matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS), which were determined exclusively in BAM laboratories are given, as well. These results represent the base for the BAM certification work of creating polymer reference materials according to the BAM Guidelines for the Production and Certification of BAM Reference Materials, a version of the European guidelines (BCR/01/97). These samples are available for third-party user.…
Autor*innen: | Ulrich Just, Steffen WeidnerORCiD, P. Kilz, T. Hofe |
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Dokumenttyp: | Zeitschriftenartikel |
Veröffentlichungsform: | Verlagsliteratur |
Sprache: | Englisch |
Titel des übergeordneten Werkes (Englisch): | International journal of polymer analysis and characterization |
Jahr der Erstveröffentlichung: | 2005 |
Verlag: | Gordon and Breach Publ. |
Verlagsort: | Amsterdam |
Jahrgang/Band: | 10 |
Ausgabe/Heft: | 3-4 |
Erste Seite: | 225 |
Letzte Seite: | 243 |
Freie Schlagwörter: | CRM; Intrinsic viscosity; Light scattering (LS); Molar mass determination; Polymer reference materials; Size exclusion chromatography (SEC) |
DOI: | 10.1080/10236660500418039 |
ISSN: | 1023-666X |
ISSN: | 1563-5341 |
Verfügbarkeit des Dokuments: | Physisches Exemplar in der Bibliothek der BAM vorhanden ("Hardcopy Access") |
Bibliotheksstandort: | Sonderstandort: Publica-Schrank |
Datum der Freischaltung: | 19.02.2016 |
Referierte Publikation: | Ja |
Datum der Eintragung als referierte Publikation: | 12.01.2006 |