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Neutron Bragg edge imaging for in situ mapping of crystallographic phase-transformations and of temperature distributions during GTAW of supermartensitic stainless steel

  • In Neutron-Bragg-Edge Imaging (NBEI) experiments, we studied the phase transition during butt-welding of supermartensitic steel plates. Gas tungsten arc welding (GTAW) was used with a motorized torch allowing for automated weldments. The austenitization in the heat affected zone (HAZ) underneath the welding head could be clearly visualized at λ = 0.39 nm, a wavelength smaller than the Bragg edge wavelengths of both austenite and martensite. Also, the re-transformation into the martensitic phase upon cooling was detected. However, we observed an unexpected additional change in transmission at λ = 0.44 nm that is a wavelength larger than the wavelength of the Bragg edges of both the martensitic and austenitic phases. We attribute this change to the Deybe-Waller-Factor that describes the temperature dependence of coherent scattering at a crystal lattice. The observed two-dimensional attenuation map corresponds well with a temperature distribution modelling by software macros in ANSYS.In Neutron-Bragg-Edge Imaging (NBEI) experiments, we studied the phase transition during butt-welding of supermartensitic steel plates. Gas tungsten arc welding (GTAW) was used with a motorized torch allowing for automated weldments. The austenitization in the heat affected zone (HAZ) underneath the welding head could be clearly visualized at λ = 0.39 nm, a wavelength smaller than the Bragg edge wavelengths of both austenite and martensite. Also, the re-transformation into the martensitic phase upon cooling was detected. However, we observed an unexpected additional change in transmission at λ = 0.44 nm that is a wavelength larger than the wavelength of the Bragg edges of both the martensitic and austenitic phases. We attribute this change to the Deybe-Waller-Factor that describes the temperature dependence of coherent scattering at a crystal lattice. The observed two-dimensional attenuation map corresponds well with a temperature distribution modelling by software macros in ANSYS. Here, the absolute temperature values could be achieved by calibrating the modelled attenuation with help of a thermocouple placed at the steel plate. This allows in return for a direct two-dimensional temperature reading based on the Debye-Waller-relation between neutron attenuation and sample temperature.zeige mehrzeige weniger

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Metadaten
Autor*innen:Axel Griesche, Tobias MenteORCiD, Henning Markötter, M. Al-Falahat, N. Kardjilov
Dokumenttyp:Vortrag
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2023
Organisationseinheit der BAM:9 Komponentensicherheit
9 Komponentensicherheit / 9.4 Integrität von Schweißverbindungen
DDC-Klassifikation:Technik, Medizin, angewandte Wissenschaften / Ingenieurwissenschaften / Ingenieurwissenschaften und zugeordnete Tätigkeiten
Freie Schlagwörter:Debye-Waller-Faktor
Themenfelder/Aktivitätsfelder der BAM:Material
Veranstaltung:ITMNR-9
Veranstaltungsort:Buenos Aires, Argentina
Beginndatum der Veranstaltung:12.10.2022
Enddatum der Veranstaltung:16.10.2022
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:24.10.2023
Referierte Publikation:Nein
Eingeladener Vortrag:Nein
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