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Two tasks in environmental monitoring - calibration and characterization of gas sensors and remote sensing with multicopter platforms - Part 2

  • Emissions of ammonia into the environment are mainly caused by agriculture, but also by combustion processes in waste and by road traffic. Even at low concentrations, this substance is not only an odour nuisance, but also a substance with ecological and climatic relevance. Therefore, BAM tested commercial electrochemical, and metal oxide based sensors, which have limited suitability for measuring in the environmental molar fraction range. Alternatively, own developments for the detection of ammonia in the trace range were implemented, wherein the analyte is measured by changing the fluorescence of a BODIPY dye at 550 nm by means of a portable fluorescence sensor directly from the gas phase. For the calibration of ammonia sensors and measuring instruments, a stationary system based on the mixture of certified test gases from pressure cylinders with calibrated mass flow controllers is available. A test gas generator was developed for on-site calibration and testing of sensors andEmissions of ammonia into the environment are mainly caused by agriculture, but also by combustion processes in waste and by road traffic. Even at low concentrations, this substance is not only an odour nuisance, but also a substance with ecological and climatic relevance. Therefore, BAM tested commercial electrochemical, and metal oxide based sensors, which have limited suitability for measuring in the environmental molar fraction range. Alternatively, own developments for the detection of ammonia in the trace range were implemented, wherein the analyte is measured by changing the fluorescence of a BODIPY dye at 550 nm by means of a portable fluorescence sensor directly from the gas phase. For the calibration of ammonia sensors and measuring instruments, a stationary system based on the mixture of certified test gases from pressure cylinders with calibrated mass flow controllers is available. A test gas generator was developed for on-site calibration and testing of sensors and measuring devices. The generation of ammonia-containing gases in the environmental relevant range of levels below 1000 nmol/mol is carried out by the permeation method according to ISO 6145-10. For the traceability of ammonia, standards are provided and further developed by the National Metrological Institutes and designated institutes. Metrological standards are based on SI units and are a basis for traceability of sensors or gas analysers.zeige mehrzeige weniger

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Metadaten
Autor*innen:Carlo Tiebe, Matthias BartholmaiORCiD
Koautor*innen:Kornelia Gawlitza
Dokumenttyp:Vortrag
Veröffentlichungsform:Präsentation
Sprache:Englisch
Jahr der Erstveröffentlichung:2018
Organisationseinheit der BAM:1 Analytische Chemie; Referenzmaterialien
1 Analytische Chemie; Referenzmaterialien / 1.9 Chemische und optische Sensorik
8 Zerstörungsfreie Prüfung
8 Zerstörungsfreie Prüfung / 8.1 Sensorik, mess- und prüftechnische Verfahren
DDC-Klassifikation:Naturwissenschaften und Mathematik / Chemie / Analytische Chemie
Freie Schlagwörter:Ammonia; Environmental monitoring; Fluorescence sensor; Test gas generation
Themenfelder/Aktivitätsfelder der BAM:Umwelt
Umwelt / Sensorik
Veranstaltung:Aarhus University, Department of Environmental Science, External seminar with Matthias Bartholmai and Carlo Tiebe
Veranstaltungsort:Roskilde, Denmark
Beginndatum der Veranstaltung:29.08.2018
Enddatum der Veranstaltung:29.08.2018
Verfügbarkeit des Dokuments:Datei im Netzwerk der BAM verfügbar ("Closed Access")
Datum der Freischaltung:04.09.2018
Referierte Publikation:Nein
Eingeladener Vortrag:Nein
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