TY - JOUR A1 - Constantinescu, B. A1 - Bugoi, R. A1 - Cojocaru, V. A1 - Radtke, Martin A1 - Calligaro, T. A1 - Salomon, J. A1 - Pichon, L. A1 - Röhrs, S. A1 - Ceccato, D. A1 - Oberländer-Târnoveanu, E. T1 - Micro-SR-XRF and micro-PIXE studies for archaeological gold identification - The case of Carpathian (Transylvanian) gold and of Dacian bracelets N2 - Trace-elements are more significant for provenancing archaeological metallic artifacts than the main components. For gold, the most promising elements are platinum group elements (PGE), Sn, Te, Sb, Hg and Pb. Several small fragments of natural Transylvanian gold – placer and primary – were studied by using micro-PIXE technique at the Legnaro National Laboratory AN2000 microbeam facility, Italy and at the AGLAE accelerator, C2RMF, Paris, France and by using micro synchrotron radiation X-ray fluorescence (micro-SR-XRF) at BESSY synchrotron, Berlin, Germany. The goal of the study was to identify the trace-elements, especially Sn, Sb and Te. A spectacular application to five Dacian gold bracelets authentication is presented (Sn and Sb traces). KW - Micro-PIXE KW - Micro-SR-XRF KW - Gold KW - Dacian bracelets KW - Transylvania PY - 2008 DO - https://doi.org/10.1016/j.nimb.2008.03.054 SN - 0168-583X SN - 1872-9584 VL - 266 IS - 10 SP - 2325 EP - 2328 PB - Elsevier CY - Amsterdam AN - OPUS4-17736 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo T1 - Inline detection of microbial infections on the basis of airborne metabolites using ion mobility spectrometry T2 - Postharvest Unlimited 2008 CY - Berlin, Germany DA - 2008-11-04 PY - 2008 AN - OPUS4-18153 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klein, P. A1 - Theiler, Geraldine A1 - Friedrich, K. T1 - Tribological behavior of short Carbon fiber reinforced PTFE- and PEEK-compounds T2 - 15th International Sealing Conference CY - Stuttgart, Germany DA - 2008-10-07 KW - Polymer composite KW - Tribology KW - Low temperatures PY - 2008 SN - 978-3-00-025884-8 IS - A 22 SP - 292 EP - 301 PB - Leithner Media Production CY - Ebelsbach AN - OPUS4-19518 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Strub, Erik A1 - Plarre, Rüdiger A1 - Radtke, Martin A1 - Reinholz, Uwe A1 - Riesemeier, Heinrich A1 - Schoknecht, Ute A1 - Urban, Klaus A1 - Jüngel, P. T1 - Determination of Cr(VI) in wood specimen: A XANES study at the Cr K edge N2 - The content of chromium in different oxidation states in chromium-treated wood was studied with XANES (X-ray absorption near-edge structure) measurements at the Cr K absorption edge. It could be shown that wood samples treated with Cr(VI) (pine and beech) did still contain a measurable content of Cr(VI) after four weeks conditioning. If such wood samples were heat exposed for 2 h with 135 °C prior conditioning, Cr(VI) was no longer detected by XANES, indicating a complete reduction to chromium (III). KW - X-ray spectroscopy KW - XANES KW - XAS KW - XRF KW - Specifikation KW - Reduction PY - 2008 DO - https://doi.org/10.1016/j.nimb.2008.03.011 SN - 0168-583X SN - 1872-9584 VL - 266 IS - 10 SP - 2405 EP - 2407 PB - Elsevier CY - Amsterdam AN - OPUS4-17555 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Radtke, Martin T1 - SR-XRF analysis of trace amounts of Pt in gold alloys T2 - European Conference on X-ray Spectrometry CY - Dubrovnik, Croatia DA - 2008-06-16 PY - 2008 AN - OPUS4-17845 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Guerra, M. F. A1 - Radtke, Martin A1 - Reiche, I. A1 - Riesemeier, Heinrich A1 - Strub, Erik T1 - Analysis of trace elements in gold alloys by SR-XRF at high energy at the BAMline N2 - Measuring in a non-destructive way the characteristic trace elements of the metal allows following the circulation of gold in the past. The aim of this work is to probe the possibilities of X-ray fluorescence with high energy synchrotron radiation (SR-XRF) at the BAMline at BESSY II to determine the concentration of Pt in ancient gold alloys. A HP-Ge detector was used to measure the Pt K-lines excited with an incident energy of 79.5 keV. Data processing was done by subtraction of a Pt free gold standard spectrum from the spectrum of the sample. Depending on the sample composition, the MDL ranges between 40 and 90 ppm. The first results obtained for a small set of gold alloys of different thickness, size and composition showed that high energy SR-XRF is a significant method for the non-destructive determination of Pt in gold. KW - SR-XRF KW - Gold KW - Provenancing KW - Trace elements PY - 2008 DO - https://doi.org/10.1016/j.nimb.2008.03.008 SN - 0168-583X SN - 1872-9584 VL - 266 IS - 10 SP - 2334 EP - 2338 PB - Elsevier CY - Amsterdam AN - OPUS4-17735 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Cross, Carl Edward A1 - Coniglio, Nicolas ED - Carl E. Cross, ED - John C. Lippold, ED - Böllinghaus, Thomas ED - Herold, H. T1 - Weld solidification cracking: critical conditions for crack initiation and growth N2 - A perspective will be given that outlines important considerations in evaluating and predicting weldability. An examination will be made of the local conditions necessary for solidifications crack initiation and growth in a weld. This will be done in light of two prominent thermo-mechanical approaches involving critical strain and critical strain rate. Critical conditions will be identified based upon values available in the literature. Methods used to measure strain and strain rate will be compared. The interpretation of crack lenght measurements commonly used to quantify weldability will be questioned, based upon our current understanding of the problem. Complications and problem areas needing better definition will be identified and discussed, including strain distribution in the mushy zone, segregation at grain boundaries, effect of impurities, and effect of cooling rate on solidification path. Finally, a suggestion will be made for a new approach to weld development using in-situ strain rate measurements and new composition-strain rate maps that define the boundary between crack an no-crack conditions. T2 - Hot cracking phenomena in welds II CY - Berlin, Germany DA - 2007-03-05 KW - Solidification Cracking KW - Hot Cracking KW - Crack Initiation KW - Crack Growth KW - Critical Strain KW - Critical Strain Rate KW - Weldability Testing KW - Crack Prediction PY - 2008 SN - 978-3-540-78627-6 SP - 39 EP - 58 PB - Springer CY - Berlin AN - OPUS4-18319 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Askar, Enis A1 - Schröder, Volkmar A1 - Acikalin, Hatice Aydan A1 - Steinbach, J. T1 - Die Explosionsgrenzen von Ethylenoxidgemischen bei Sterilisationsprozessen N2 - Für die sicherheitstechnische Beurteilung von Sterilisationsprozessen wurden die Explosionsgrenzen von Gasgemischen aus Ethylenoxid, Inertgas und Luft experimentell bestimmt. Die Messungen sind mit Stickstoff, Kohlenstoffdioxid und Wasserdampf bei 20 und 100 °C sowie bei 0,4 und 1,0 bar durchgeführt worden. Mit Hilfe der Daten wurde ein halbempirisches Modell entwickelt, mit dem die Explosionsfähigkeit von Prozessgasgemischen berechnet werden kann. KW - Ethylenoxid KW - Explosionsgrenze KW - Explosionsschutz KW - Inertisierung KW - Sterilisation PY - 2008 DO - https://doi.org/10.1002/cite.200800010 SN - 0009-286X SN - 1522-2640 VL - 80 IS - 5 SP - 643 EP - 647 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-17484 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Coniglio, Nicolas A1 - Cross, Carl Edward ED - Carl E. Cross, ED - John C. Lippold, ED - Böllinghaus, Thomas ED - Herold, H. T1 - Weld parameter and minor element effects on solidification crack initiation in Aluminium N2 - Earlier work has established that a critical amount of 4043 filler is required to avoid solidification cracking when arc-welding 6060 aluminium, depending upon local strain conditions. For example, when the mushy zone behind the weld pool experiences a tensile strain from combined thermal and shrinkage stresses, the possibility exists for crack initiation. For a greater rate of strain, it has been determined that a greater 4043 dilution (i.e. higher weld metal silicon content) is required to avoid crack initiation. Making use of the Controlled Tensile Weldability (CTW) test and local strain extensometer measurements, a boundary has been established between crack and no-crack conditions for different local strain rates and filler dilutions, holding all other welding parameters constant. Using this established boundary as a line of reference, additional parameters have now been examined and their influence on cracking has been characterized. These parameter influences have included studies of weld travel speed, weld pool contaminants (Fe, O, and H), and grain refiner additions (TiAl3 + Boron). Each parameter has been independently varied and its effect on cracking susceptibility quantified in terms of a critical strain rate required to initiate cracking for a given 4043 filler dilution. T2 - Hot cracking phenomena in welds II CY - Berlin, Germany DA - 2006-03-05 KW - Aluminium Alloys KW - Solidification Cracking KW - Weld Defect KW - Hot Cracking KW - Crack Initiation KW - Critical Strain Rate KW - Parameter Effects KW - Minor Elements PY - 2008 SN - 978-3-540-78627-6 SP - 277 EP - 310 PB - Springer CY - Berlin AN - OPUS4-18323 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Weimann, Karin A1 - Müller, A. ED - Ravindra K. Dhir, ED - Peter C. Hewlett, ED - Laslo J. Csetenyi, ED - Moray D. Newlands, T1 - Effects of wet processed crushed concrete fines as secondary aggregates in building materials T2 - International Conference "Role for Concrete in Global Development" CY - Dundee, Scotland, UK DA - 2008-07-08 KW - Recycling KW - Beton KW - Bauschutt KW - Recycled aggregates KW - Crushed concrete fines KW - Wet treatment KW - Jig KW - Building material properties PY - 2008 SN - 978-1-84806-037-1 IS - EP86 SP - 499 EP - 510 PB - IHS BRE Press AN - OPUS4-18802 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Proß, E. T1 - Thin film coatings for lubricated slip-rolling contacts up to 3.500 MPa of initial Hertzian contact pressure T2 - Plenarvortrag auf dem "16th International Colloquium of Tribology" CY - Esslingen am Neckar, Germany DA - 2008-01-15 PY - 2008 AN - OPUS4-16256 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Simons, C. A1 - Mans, C. T1 - New polymeric reference materials for XRF and LA-ICP-MS - development and characterization T2 - POLYDAYS 2008, Active and Adaptive Polymeric Materials, Freie Universität Berlin CY - Berlin, Germany DA - 2008-10-01 PY - 2008 AN - OPUS4-17832 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo T1 - Entwicklung und Validierung eines Verfahrens zur Bestimmung von verdecktem Schimmelpilzbefall mittels Ionenmobilitätsspektroskopie T2 - 2. IMS Anwendertreffen CY - Leipzig, Germany DA - 2008-05-26 PY - 2008 AN - OPUS4-17504 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Simons, C. T1 - New polymeric reference materials for XRF and LA-ICP-MS - development and characterization T2 - Analytica CY - Munich, Germany DA - 2008-04-01 PY - 2008 AN - OPUS4-17833 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Woydt, Mathias T1 - Überrollbeständige Dünnschichten unter geschmierter Wälzreibung bis 3.500 MPa N2 - Die Wälzbeständigkeit von Kohlenstoffdünnschichten (DLC, Diamond Like Carbon) ist im Lauf den letzten Jahren wesentlich verbessert worden. Gleichwohl sind weitere Leistungssteigerungen nötig besonders bezüglich der Temperaturbeständigkeit und der prozessbedingten Oberflächenrauheit der abgeschiedenen Schichten. Dieser Beitrag stellt ein neuartiges Schicht-Substrat-System vor. Dieses ist mit unlängst entwickelten DLC-Dünnschichten unter geschmierter Wälzbeanspruchung in einem Benchmark verglichen worden. Eine der zirkonium-basierten Dünnschichten erweist sich als wälzbeanspruchbar und -beständig unter hohen anfänglichen Hertzsche Pressungen bis P0max = 3.500 MPa und offenbarte in einem Erstbefüllungsmotoröl bei 120°C auch geringe Misch-/Grenzreibungszahlen. Als Vergleich erreichen die DLC Schichten 10 Millionen Zyklen bei RT bis maximalen Hertzsche Pressungen von P0max = 2.940 MPa. Einige DLC-Schichten erzielen diese hohe Belastbarkeit auch bei 120°C. Die Zr-basierten Dünnschichten erfordern keine darauf angepaßten Schmierstoffformulierungen. Diese nanostrukturierten Dünnschichten beruhen auf einer Architektur und einem Prozess, die sich zusammen für die Großserie eignen. T2 - 49. Jahrestagung der Gesellschaft für Tribologie CY - Göttingen, Germany DA - 2008-09-22 PY - 2008 AN - OPUS4-18195 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Simons, C. T1 - New polymeric reference materials for XRF and LA-ICP-MS - development and characterization T2 - European Conference on X-ray Spectrometry CY - Dubrovnik, Croatia DA - 2008-06-16 PY - 2008 AN - OPUS4-17844 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Thünemann, Andreas T1 - Nanoparticle size analysis - Small-angle X-Ray scattering T2 - 32nd Meeting of the International Standard Organization ISO/TC24/SC4 CY - Stratford-upon-Avon, England DA - 2008-09-05 PY - 2008 AN - OPUS4-17952 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Riesemeier, Heinrich T1 - Materials research at the 7T-Wave Length Shifter, WLS-1 at BESSY: Instrumentation and selected results T2 - Seminar, ANKA CY - Karlsruhe, Germany DA - 2008-03-03 PY - 2008 AN - OPUS4-17898 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rasheva, Z. T1 - Tribologisches Verhalten von PEEK-basierten Verbundwerkstoffen für Vakuumanwendungen T2 - IVW-Kolloquium CY - Kaiserslautern, Germany DA - 2008-09-16 PY - 2008 AN - OPUS4-18193 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eliezer, D. T1 - A new technology for hydrogen storage in Capillary Arrays T2 - 2008 International Hydrogen Conference - Effects of Hydrogen on Materials CY - Jackson, WY, USA DA - 2008-09-07 PY - 2008 N1 - Geburtsname von Kluge, Martin: Beckmann-Kluge, M. - Birth name of Kluge, Martin: Beckmann-Kluge, M. AN - OPUS4-18189 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -