TY - CHAP A1 - Schartel, Bernhard A1 - Kebelmann, Katharina ED - Hu, Y. ED - Wang, X. T1 - Fire testing for the development of flame retardant polymeric materials N2 - Flame retarded polymeric materials are used in various applications in which a certain fire behavior is demanded. Protection goals are defined, such as limited flammability in terms of hindered sustained ignition or limited contribution to a fire, and these protection levels are tested with defined specimens or components in defined fire scenarios, that is to say, different fire tests. Passing a specific fire test by meeting whatever its demands is often the most important development goal, so the parameters of the different fire tests vary widely to emphasize different fire properties. Some fire tests are used to screen or provide a general assessment of flame retardant polymers during development, while other fire tests and tailored experiments are performed to address special phenomena or understand the flame retardancy modes of action. For all fire testing, the devil is in the details – demanding know-how and crucial efforts to manage the quality of investigations and advanced interpretation. This chapter aims to offer a structured overview of all these aspects. KW - Fire testing KW - Flame retardant KW - Fire retardant KW - Flammability KW - Ignition KW - Oxygen index KW - Cone calorimeter KW - UL 94 KW - Developing fire KW - Uncertainty KW - Fire resistance PY - 2020 SN - 978-1-138-29578-7 SP - 35 EP - 55 PB - CRC Press AN - OPUS4-50236 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Meftah, F. A1 - Pesavento, F. A1 - Davie, C. A1 - Dal Pont, S. A1 - Zeiml, M. A1 - Korzen, Manfred A1 - Millard, A. ED - Millard, A. ED - Pimienta, P. T1 - Advanced Modelling N2 - In this chapter, advanced models based on a General thermo-Hydro-Mechanical (THCM) Framework are considered. In These approaches, the concrete is considered as a porous medium, the pores of which are partly filled by gas (a mixture of air and vapour) and water. KW - Concrete KW - High temperature KW - Stress-strain-relation PY - 2019 SN - 978-3-030-11994-2 SN - 978-3-030-11995-9 DO - https://doi.org/10.1007/978-3-030-11995-9 SN - 2213-204X SN - 2213-2031 SP - 27 EP - 65 PB - Springer CY - Cham, Switzerland AN - OPUS4-50174 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Wünsch, Christoph A1 - Simon, Franz-Georg ED - Maletz, Roman ED - Dornack, Christina ED - Ziyang, Lou T1 - The reduction of greenhouse gas emissions through the source-separated collection of household waste in Germany N2 - The production of secondary materials from waste materials requires, in most cases, significantly lower energy amounts than the primary material production of raw materials. Along with lower energy demand, the greenhouse gas emissions produced are also lower. The duty of a modern waste management system should therefore be to collect and sort the waste materials in a way that the highest amounts of single material fractions with the highest qualities can be generated. In this contribution, the greenhouse gas balances of the theoretical treatment of the household waste, if collected as mixed waste in sanitary landfills, in waste incineration plants, or in mechanical-biological treatment plants, are compared to the existing separate waste collection and treatment in Germany in 2014. The results show that the treatment of the mixed collected household waste in sanitary landfills would lead to a significant release of greenhouse gases. The treatment in MBTs with the recovery of valuables and the further disposal of the biologically stabilized fraction on landfills, as well as the treatment of the high calorific fraction (also called refuse derived fuel – RDF) in RDF plants, coal-fired power plants, or cement kilns, would lead to small amounts of avoided greenhouse gas emissions. The thermal treatment in waste incineration plants would lead to moderate amounts of avoided greenhouse gases. Only with the actually practiced separate collection and treatment of household waste were significant amounts of greenhouse gas emissions avoided. In total, this is approximately 5.5 million tons of carbon dioxide equivalents for approximately 45.5 million tons of separate collected and treated household waste in Germany in 2014. KW - Greenhouse gas accounting KW - Greenhouse gas mitigation KW - Household waste KW - Material recycling KW - Separate collection PY - 2018 SN - 978-3-319-69071-1 DO - https://doi.org/10.1007/698_2017_35 VL - 63 SP - 269 EP - 287 PB - Springer International Publishing CY - Berlin ET - 1 AN - OPUS4-44937 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Manzoni, Anna Maria A1 - Glatzel, U. ED - Buschow, K.H.J. ED - Flemings, M.C. ED - Kramer, E.J. ED - Veyssière, P. ED - Cahn, R.W. ED - Ilschner, B. ED - Mahajan, S. T1 - High-Entropy Alloys: Balancing Strength and Ductility at Room Temperature N2 - A new race for high performance structural materials has started since the discovery of high entropy alloys at the beginning of the 21st century. The possible combination of several elements in an, until then, unknown composition space opened the ground for discovering new materials. Solid solution strengthening remains the most prominent mechanisms that is active in this family of materials, but it is supported by all other strengthening mechanism on the path to better and better performing materials. Chemical, thermal and mechanical approaches are combined to optimize these alloys. Optimum performances can be reached by using a high number of different strengthening mechanisms, induced both by composition and processing. The most prominent with composition induced mechanism is precipitation hardening, and on the processing side it is cold working such as cold-rolling, torsion or extrusion. The contribution uses tensile test data at room temperature solely for comparison – high temperature and cryogenic data are omitted because it would lead beyond the scope of this manuscript. KW - High entropy alloys KW - Compositionally complex alloys PY - 2020 DO - https://doi.org/10.1016/B978-0-12-803581-8.11774-6 PB - Elsevier Inc. AN - OPUS4-50575 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Skrotzki, Birgit A1 - Czichos, Horst ED - Hennecke, Manfred ED - Skrotzki, Birgit T1 - Materialprüfung N2 - Die Materialprüfung dient der Analyse der Eigenschaften, der Qualität und der Sicherheit vonMaterialien undWerkstoffen. Die häufigsten Verfahren umfassen die Analyse der chemischen Zusammensetzung und der Mikrostruktur sowie die Ermittlung von Werkstoffkennwerten. Dazu zählt auch die Bestimmung des Materialverhaltens unter verschiedenen Beanspruchungen bis hin zu komplexen Beanspruchungen. Die Verwendung von Referenzmaterialien, Referenzorganismen und Referenzverfahren dient der Zuverlässigkeit und Richtigkeit von Messungen, Prüfungen und Analysen. KW - Materialprüfung KW - Werkstoffprüfung KW - Chemische Analyse KW - Mikrostrukturuntersuchung KW - Gefügeuntersuchung KW - Werkstoffmechanische Prüfung KW - Zerstörungsfreie Prüfung KW - Referenzmaterial KW - Referenzorganismus KW - Referenzverfahren PY - 2019 SN - 978-3-662-57492-8 DO - https://doi.org/10.1007/978-3-662-57492-8_30-1 SP - 1 EP - 27 PB - Springer-Verlag GmbH CY - Berlin, Heidelberg ET - 35 AN - OPUS4-50516 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Wosniok, Aleksander ED - Werneck, M.M. ED - da Silva Barros Allil, R.C T1 - POF Sensors for Structural Health Monitoring N2 - The ever more ambitious strategic goals of meeting the requirements in ensuring technical safety and security of civil structures have resulted in flourishing development of innovative structural health monitoring (SHM) technologies for early damage diagnosis and prognosis. At the same time, implementing SHM systems provides tangible economic benefits derived from lower life-cycle costs associated with reduction in the maintenance, repair and insurance expenses. Due to the large size and harsh environmental conditions common to most civil structures, the broad range of favorable physical-mechanical properties of POFs allow for customized monitoring solutions for a wide variety of applications. In addition to common SHM-related advantages of optical fibers including their electromagnetic immunity, small size, lightweight as well as spark-free and non-conductive characteristics, POFs offer better bending and fracture resistance then their glass-counterparts. Particularly, the improved robustness of POFs, their ease of handling, low Young’s Modulus and high elastic limit of 10% compared to 1% in silica glass [1] are relevant to practical applications. Depending on the composition, dopants, drawing process and geometry [2], strain measurement up to 45% [3] or even above 100% [4,5] has been demonstrated with standard POFs. Therefore, the dominant market expected for POF sensors includes monitoring of high-strain-rate deformations in earthwork structures, crack detection in concrete and masonry structures [6] or overstressing in high-rise steel structures exposed to moisture, corrosion, leakage, fatigue, vibration, fire, overflow, earthquake and intentional damage. For fracture monitoring within concrete structures, the sensory usage of POFs becomes especially favorable since the extremely alkaline environment of concrete mixtures is well known to be corrosive to standard silica glass optical fibers (GOFs) [1,7]. Most of advanced distributed sensing techniques are commonly based on Rayleigh backscatter reflectometry using commercially available multimode (MM) POFs. Such typical MM POFs range from a step-index (SI) poly(methyl methacrylate) (PMMA) POF having a core diameter of 1 mm to a low-loss graded-index (GI) perfluorinated (PF) POF based on poly(perfluorobutenyl-vinylether) also known as CYTOP [8] with a 50 µm core diameter. The relatively low optical attenuation value of 30 dB/km at 1.3 µm [9,10] makes PFGI POFs also interesting for distributed Brillouin sensing [11-14]. Compared to GOFs, PFGI POFs offer better potential for temperature measurement and have comparably low theoretical attenuation limit [15]. Therefore, POF-based distributed Brillouin sensing is expected to play an important role in the future of SHM, especially at high-strain ranges. The significance of the Brillouin measurment technique can be also enhanced by further development of the single-mode (SM) POFs which are still subject of research and are used for coherent detection techniques [6]. Furthermore, SM PMMA POFs have been characterized in a Mach-Zehnder interferometer setup for strain values up to 15.8% [16,17]. The current development of SM perfluorinated and microstructured POFs (mPOFs) represents an immense promise for quasi-distributed dynamic measurement at high strain levels based on fiber Bragg grating (FBG) technology. While SM mPOFs with optical losses of about 1 dB/m can be fabricated [6], the SM PF POFs presented by Zhou et al. feature low attenuation of even less than 0.2 dB/m in the wavelength range of 1.41 µm to 1.55 µm [18]. At the same time, the SM PF POFs have the potential for improved thermal stability compared to their PMMA counterparts [19]. This whole chapter provides a comprehensive overview on current POF-based sensing principles and SHM technologies, highlighting their diverse applications in civil engineering structures. In the application-related context, close attention is paid to the development of smart sensor-based geotextiles and geogrids. Such geosynthetics-integrated distributed POF sensors have proven to be a promising solution for two- or even tree-dimensional monitoring of critical high mechanical deformations in both geotechnical and masonry structures. Moreover, geosynthetics in the form of nonwoven geotextiles as well as polymer-based geogrids used as carrier materials for POF sensors enable optimized load transfer from the monitored structure to the measuring fiber without losing their original functionality. In other words, smart geosynthetics provide a cost-efficient dual solution for, on the one hand, well-established increase of structure stability and decrease of erosion effects, on the other hand, early-warning and detection capabilities in the prevention and elimination of potential hazards and lasting damages. KW - Plastic Optical Fiber Sensor KW - OTDR KW - Brillouin Sensing KW - Interferometric Sensor KW - FBG KW - Long Period Grating KW - Smart Geosynthetics PY - 2020 SN - 978-1-13829-853-8 SP - 267 EP - 283 PB - CRC Press Taylor & Francis Group CY - Boca Raton, FL, USA AN - OPUS4-50561 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Maiwald, Michael ED - Meyer, Simon T1 - Voll integrierte und vernetzte Systeme und Prozesse - Perspektive: Smarte Sensorik, Aktorik und Kommunikation N2 - Unternehmen der chemischen Industrie müssen neuen Pfade beschreiten, um in einem veränderten Umfeld erfolgreich bestehen zu können. Dazu gehört insbesondere, das Potenzial digitaler Technologien zu nutzen. Die volle Integration und intelligente Vernetzung von Systemen und Prozessen kommt allerdings nur zögerlich voran. Dieser Beitrag ist ein Loblied auf die Feldebene. Er möchte dazu ermutigen, die Digitalisierung der Prozessindustrie auf Basis smarter Sensorik, Aktorik und Kommunikation ganzheitlicher zu denken und informiert über aktuelle technische Perspektiven, wie das Ein-Netzwerk-Paradigma, Ad-hoc-Vernetzungen, Edge-Computing, FPGAs, virtuelle Maschinen oder Blockchain. Diese geben smarter Sensorik, Aktorik und Kommunikation eine völlig neue Perspektive. KW - Smarte Sensoren KW - Smarte Aktoren KW - Digitalisierung KW - Prozessindustrie KW - Prozess-Sensoren 4.0 PY - 2019 SN - 978-3-8356-7436-3 SP - 28 EP - 40 PB - Vulkan-Verlag GmbH CY - Essen AN - OPUS4-50035 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Lisec, Jan A1 - Jaeger, C. ED - Antonio, C. T1 - Statistical and Multivariate Analysis of MS-Based Plant Metabolomics Data N2 - Raw data from metabolomics experiments are initially subjected to peak identification and signal deconvolution to generate raw data matrices m × n, where m are samples and n are metabolites. We describe here simple statistical procedures on such multivariate data matrices, all provided as functions in the programming environment R, useful to normalize data, detect biomarkers, and perform sample classification. KW - Mass-Spectrometry KW - Multivariate Statistics PY - 2018 SN - 978-1-4939-7819-9 SN - 978-1-4939-7818-2 DO - https://doi.org/10.1007/978-1-4939-7819-9_20 SN - 1064-3745 SN - 1940-6029 VL - 1778 SP - Chapter 20, 285 EP - 296 PB - Springer-Verlag AN - OPUS4-45492 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Hofmann-Böllinghaus, Anja ED - Vogdt, F. U. T1 - Brandschutz N2 - Grundlagen des vorbeugenden baulichen Brandschutzes KW - Brandprüfungen KW - Bauvorschriften PY - 2022 SN - 978-3-8348-2189-8 SP - 199 EP - 220 PB - Springer ET - 1 AN - OPUS4-54317 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schartel, Bernhard ED - Morgan, A.B. T1 - Multicomponent Flame Retardants N2 - The important take home message of this chapter: When multicomponent flame retardant systems are applied to polymeric materials, it becomes possible to address multiple fire properties, increase efficiency, and minimize flame retardant use to maximize polymer property balance. Flame retardants are combined or used together with adjuvants or synergists; fibers and fillers make a crucial contribution to their fire properties. Multicomponent systems are discussed in their capacity as an overall powerful strategy for achieving and optimizing non-halogenated flame-retardant polymeric materials. KW - Flame retardants KW - Synergy KW - Adjuvants KW - Fillers KW - Fibres PY - 2022 SN - 978-1-119-75056-7 SP - 413 EP - 474 PB - Scrivener Publishing LLC CY - Bevery ET - 2nd Edition AN - OPUS4-54426 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Colini, Claudia A1 - Shevchuk, I. A1 - Huskin, K. A. A1 - Rabin, Ira A1 - Hahn, Oliver ED - Quenzer, J. B. T1 - A New Standard Protocol for Identification of Writing Media N2 - Our standard protocol for the characterisation of writing materials within advanced manuscript studies has been successfully used to investigate manuscripts written with a pure ink on a homogeneous writing surface. However, this protocol is inadequate for analysing documents penned in mixed inks. We present here the advantages and limitations of the improved version of the protocol, which now includes imaging further into the infrared region (1100−1700 nm). KW - Archaeometry KW - Manuscripts KW - Non-destructive testing PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-543454 SN - 978-3-11-074545-0 DO - https://doi.org/10.1515/9783110753301-009 VL - 25 SP - 161 EP - 182 PB - Walter de Gruyter GmbH CY - Berlin/Boston AN - OPUS4-54345 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Hahn, Oliver A1 - Golle, U. A1 - Wintermann, Carsten A1 - Laurenza, D. ED - Quenzer, J. B. T1 - Scientific Analysis of Leonardo’s Manuscript with Anatomic Drawings and Notes N2 - In this paper, we discuss the importance of scientifically investigating cultural artefacts in a non-invasive way. Taking as test case Leonardo da Vinci’s Manuscript with anatomic drawings and notes, which is stored in Weimar, we clarify fundamental steps in the chronology of this folio. By means of microscopy, infrared reflectography, UV photography, and X-ray fluorescence analysis, we were able to identify various types of sketching material and several varieties of iron gall ink. For his sketches, Leonardo used two different sketching tools, a lead pencil and a graphite pencil, as well as several types of ink for developing these sketches into drawings. With regard to ink, it is important to observe that there is no difference between the ink Leonardo used for drawing and the ink he used for writing text. Based on the materials analysed, we suggest a chronology for the creation of this unique folio. KW - Archaeometry KW - Non-invasive analysis KW - Drawings KW - Leonardo da Vinci PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-543460 SN - 978-3-11-074545-0 DO - https://doi.org/10.1515/9783110753301-011 VL - 25 SP - 213 EP - 228 PB - Walter de Gruyter GmbH CY - Berlin/Boston AN - OPUS4-54346 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Dietz, Georg A1 - Golle, U. A1 - Hahn, Oliver A1 - Ketelsen, T. A1 - Melzer, C. A1 - Wintermann, Carsten ED - Semff, M. T1 - Der fabelhafte Möglichmacher N2 - Der Beitrag würdigt die Verdienste Wolfgang Hollers bei der Etablierung fächerübergreifender Kooperationen zwischen Natur- und Geisteswissenschaften innerhalb der Zeichnungsforschung. KW - Archäometrie PY - 2022 SN - 978-3-947641-20-8 SP - 370 EP - 371 PB - Sieveking Verlag CY - München AN - OPUS4-54355 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Küttenbaum, Stefan A1 - Braml, T. A1 - Taffe, A. A1 - Maack, Stefan ED - Pellegrino, C. ED - Faleschini, F. ED - Zanini, M.A. ED - Matos, J.C. ED - Casas, J.R. ED - Strauss, A. T1 - From Uncertainty in Measurement to Certainty in Bridge Reassessment N2 - "The reassessment of bridges continues to take great importance both nationally and internationally. A major challenge is to find computation models reflecting the actual properties of the considered structures sufficiently accurate. Besides regular inspections, the conduction of advanced measurements is suitable to generate reliable information about a structure to be assessed. Prior to incorporating measurement results in reassessment, the relevance, the trueness, and the precision of the measured information needs to be stated. On the one hand, the use of information whose quality has not been assessed can lead to errors with serious consequences. On the other, the measurement of irrelevant information is inefficient. Although the use of measured data in assessment is currently mostly unregulated, their appreciation in reliability analyses is beneficial since the built environment can be assessed more realistically. Utilizing NDT in reassessment has the potential to extend remaining lifetimes of a structure, save resources, and improve infrastructural availabilities. The power of judgment regarding the decision on the reliability of an existing structure can be increased. In this contribution, an approach is outlined to process non-destructively gathered measurement data in a comparableway in order to include themeasured information in probabilistic reliability assessments of existing structures. An essential part is the calculation of measurement uncertainties. The effect of incorporating evaluated NDT-results is demonstrated by means of a prestressed concrete bridge and GPR measurements conducted on this bridge as a case-study. The bridge is assessed regarding SLS Decompression using the NDT-results." KW - Reliability KW - Assessment KW - Existing structures KW - NDT KW - Concrete PY - 2022 DO - https://doi.org/10.1007/978-3-030-91877-4_58 VL - 200 SP - 509 EP - 517 PB - Springer CY - Cham AN - OPUS4-54019 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schönhals, Andreas A1 - Böhning, Martin A1 - Szymoniak, Paulina ED - Schönhals, Andreas ED - Szymoniak, Paulina T1 - (Nano)Composite Materials—An Introduction N2 - The chapter gives a brief introduction to (nano)compositecomposite materials having the focus on polymer-based nanocomposites. The different dimensionalities of nanoparticles are introduced, along with their distribution in the matrix. Different application fields of polymer-based nanocomposites, like flame retardancy, filled rubbers, nanofilled thermosets and thermoplastics, separation membranes and nanodielectrics, are considered in greater detail. KW - Polymer-based nanocomposites KW - Nanoparticle KW - Distribution of nanoparticles KW - Filled rubbers KW - Filled thermosets and plastics KW - Separation membranes KW - Nanodielectrics PY - 2022 DO - https://doi.org/10.1007/978-3-030-89723-9_1 SP - 1 EP - 31 PB - Springer CY - Cham, Switzerland AN - OPUS4-54565 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Szymoniak, Paulina A1 - Schönhals, Andreas ED - Schönhals, Andreas ED - Szymoniak, Paulina T1 - Epoxy-Based Nanocomposites—What Can Be Learned from Dielectric and Calorimetric Investigations? N2 - Epoxy-based nanocomposites are promisingmaterials for industrial applications (i.e., aerospace, marine, and automotive industries) due to their extraordinary mechanical and thermal properties. Regardless of the broad field of applications, there is still a considerable need to identify their structure–property relationships. Here, a detailed dielectric and calorimetric (DSC and fast scanning calorimetry) study on different epoxy-based nanocomposites was performed. Bisphenol A diglycidyl ether (DGEBA) cured with diethylenetriamine (DETA) was employed as the polymeric matrix, which was reinforced with three diverse nanofillers that exhibit different interaction strengths with the epoxy matrix (halloysite nanotubes, surface modified halloysite nanotubes, and taurine-modified layered double hydroxide). The structure, molecular mobility, and vitrification behavior are discussed in detail, focusing on the intrinsic structural and dynamic heterogeneity, as well as interfacial properties. KW - Nanocomposites KW - Epoxi nanocomposites KW - Dynamics KW - Interphase KW - Ridis amorphous fraction KW - Dielectric spectroscopy KW - Flash DSC KW - Temparatur modulated Flash DSC KW - Temperature modulated DSC PY - 2022 DO - https://doi.org/10.1007/978-3-030-89723-9_11 SP - 335 EP - 367 PB - Springer CY - Cham, Switzerland AN - OPUS4-54566 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Eissel, A. A1 - Engelking, Lorenz A1 - Treutler, K. A1 - Schroepfer, Dirk A1 - Wesling, V. A1 - Kannengießer, Thomas ED - da Silva, L. F. M. ED - Martins, P. A. F. ED - Reisgen, U. T1 - Nickel-Iron-Alloy Modification to Enhance Additively Welded Microstructure for Subsequent Milling N2 - The aerospace industry uses nickel–iron alloys, e.g., FeNi36, to create moulding tools for composite materials, since these alloys have a low coefficient of thermal expansion. Nickel–iron alloys are hard-to-cut materials. The moulding tools are large in size and involve complex structures, making them cost-intensive and difficult to manufacture. Thus, the focus is set on additive manufacturing, which can additionally enable the repair of components in order to eliminate local defects. However, the process usually results in a heterogeneous microstructure and anisotropic mechanical properties. As there is a high demand for a precise and exact fit of the precision moulds and the surface quality, the welded components must be subsequently machined. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. Consequently, a modification of the microstructure morphology is achieved through specific alloy modifications in order to stabilise and improve the subsequent machining process. Therefore, titanium and zirconium are chosen as modification elements with a maximum 1% weight percent and are added to nickel–iron alloy powder. The elements are alloyed, and build-up welded by plasma-transferred-arcwelding. The resulting microstructure morphology of the welded wall structure and the machining properties are then determined. It can be shown that titanium has a significant effect on the structural morphology of the welded layers, as well as on the machining. KW - Alloy modification KW - Alloy 36 KW - Plasma-transferred arc welding KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 SN - 978-3-030-95463-5 DO - https://doi.org/10.1007/978-3-030-95463-5_6 SP - 85 EP - 99 PB - Springer CY - Cham AN - OPUS4-55484 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Epple, Niklas A1 - Fontoura Barroso, Daniel A1 - Niederleithinger, Ernst A1 - Hindersmann, I. A1 - Sodeikat, C. A1 - Groschup, R. ED - Rizzo, P. ED - Milazzo, A. T1 - From the Lab to the Structure: Monitoring of a German Road Bridge Using Embedded Ultrasonic Transducers and Coda Waves N2 - The ‘Gänstorbrücke’ bridge between the cities of Ulm and Neu-Ulm is one of the best-monitored bridges all over Germany. In addition to an already active bride monitoring system, we have equipped the bridge with 30 ultrasonic transducers to explore the monitoring possibilities at an in-service large-scale reinforced concrete structure with continuous active ultrasonic measurements. The monitoring system is based on the detection of small changes in the entire signal, especially the multiply scattered parts of the recording, the so-called coda. Applying Coda Wave Interferometry (CWI), subtle changes in the signal can be detected and related to changing velocities in the area between source and receiver. A comparison of the results from coda wave interferometry with the strain measurements of the permanent monitoring system shows a correlation between strain measurements and CWI results. We discuss the challenges of changing environmental conditions, pose for interpretation of the results, and highlight the advantages of embedded versus externally attached ultrasonic transducers in permanent bridge monitoring, especially when coda wave interferometry is applied. KW - Bridge monitoring KW - Ultrasound KW - Embedded sensors KW - Coda wave interferometry PY - 2022 SN - 978-3-031-07258-1 DO - https://doi.org/10.1007/978-3-031-07258-1_83 VL - 254 SP - 824 EP - 832 PB - Springer Cham CY - Cham AN - OPUS4-55385 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Kessler, R. W. A1 - Kessler, W. A1 - Maiwald, Michael ED - Meyers, R. A. T1 - Inline and Online Process Analytical Technology with a Focus on Optical Spectroscopy N2 - Process analytical technology (PAT) is a cross-sectional technology and thus essential for future smart production. While in the past decades, the focus of process optimization strategies was on increasing efficiency, in the future, the focus will be on the sustainability of a production and its products. In addition, products will be increasingly personalized in order to match the property profile exactly to the intended use. PAT is able to provide context-sensitive information at the molecular level for process control. Spectroscopic sensors can determine inline and simultaneously both the chemical composition and its sub-microscopic morphology. The article will focus on the optical spectroscopy and therefore starts with a brief introduction on the basic concepts of molecular spectroscopy. In addition, the particularities of measuring liquids, surfaces, or particulate systems in PAT applications are described. This should enable the reader to select the appropriate method for the specific problem. Many examples from everyday industrial practice illustrate the applications. The areas covered are the manufacturing industry, process and pharmaceutical industry, food industry, as well as biotechnology and medical technology. Future will show that PAT is especially important for applications in the field of medicine (point of care) circular economy (recycling, water–wastewater, etc.). It is important to emphasize that sustainability in industrial production can only be successful with an inter- and transdisciplinary close exchange between the different disciplines. KW - Process Analytical Technology KW - Optical Spectroscopy KW - Encyclopedia of Analytical Chemistry KW - Sensors KW - Process Industry PY - 2022 SN - 978-0-47002-731-8 DO - https://doi.org/10.1002/9780470027318.a9791 SP - 1 EP - 31 PB - JohnWiley & Sons, Ltd. AN - OPUS4-56688 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Gornushkin, Igor B. ED - Galbács, G. T1 - Calibration-Free Quantitative Analysis N2 - Calibration-free methods in laser-induced breakdown spectroscopy, CF LIBS, serve as an alternative to calibration-based LIBS techniques. Their major advantage is the ability for fast chemical analysis in situations where matrix-matched standards are not readily available (as, e.g., in the analysis of biological materials and remote analysis) or amount of samples are limited. Their main applications are in the industry, geology, biology, archeology, and even space exploration. This chapter overviews the principle of operation and performance of CF LIBS techniques. KW - Laser induced plasma KW - Calibration-free LIBS PY - 2022 SN - 978-3-031-14501-8 DO - https://doi.org/10.1007/978-3-031-14502-5 SP - 67 EP - 100 PB - Springer Nature Switzerland AG AN - OPUS4-56651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Vogel, Christian A1 - Roesch, Philipp A1 - Wittwer, Philipp A1 - Simon, Franz-Georg ED - Holm, O. ED - Thomé-Kozmiensky, E. ED - Quicker, P. ED - Kopp-Assenmacher, S. T1 - Per- und polyfluorierte Alkylsubstanzen (PFAS) im Klärschlamm N2 - Per- and polyfluoroalkyl substances (PFAS) are a group of more than 4700 anionic and cationic anthrophonic substances which have been used extensively in a variety of products and industries due to their inert chemical stability and resistance to degradation by heat or acids. As a result of continuous use, mainly in aviation firefighting foams, thousands of industrial and military installations have been found to contain contaminated soil and groundwater resources. However, because of the continuous use of fluorinated consumer products, also effluents and sewage sludge from wastewater treatment plants (WWTPs) have been shown to be an important source of PFAS contamination into the aquatic environment. Resulting from recent stricter regulations and restrictions in the last years on the use of long chain (≥C8) PFAS, there is a significant shift in the chemical industry towards production of short (C4-C7) and ultrashort (C1-C3) chain alternatives. With the amendment of the Sewage Sludge Ordinance in 2017 the German legislation banned sewage sludge application on agricultural land, and by 2029/2032 sewage sludge will be completely prohibited from agricultural application. While environmental exposure of organic pollutants like PFAS, pesticides and pharmaceuticals are no longer desirable, phosphorus (P) from sewage sludge must still be used to produce high-quality P-fertilizers for a circular economy. Currently, plant-available P-fertilizers from sewage sludge/wastewater can be produced using a variety of treatment approaches including precipitation, leaching, and thermal treatment. However, the fate of legacy and emerging PFAS compounds during P leaching, precipitation and treatment from sewage sludge and wastewater is for the most parts still unknown. KW - Combustion Ion Chromatography KW - Per- and Polyfluoroalkyl substances (PFAS) KW - Klärschlamm KW - Düngemittel PY - 2022 SN - 978-3-944310-65-7 SP - 270 EP - 279 PB - Thomé-Kozmiensky Verlag GmbH CY - Neuruppin AN - OPUS4-56290 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Zarinwall, A. A1 - Waniek, Tassilo A1 - Finke, B. A1 - Sadaat, R. A1 - Sturm, Heinz A1 - Garnweitner, G. ED - Sinapius, M. ED - Ziegmann, G. T1 - Particle Surface Modification N2 - Whilst a decisive role of the particle-matrix interphase on the mechanical properties of nanoparticle-filled polymers has been demonstrated in the last years, the arbitrary design of this interphase remains a very challenging goal. In principle, this could be realized via an appropriate surfacemodification of the nanofiller prior to its incorporation in the polymer. For most systems, such as for boehmite nanofillers, however, the interaction of organic modifiers with the particle surface has not been studied in detail, and only single studies are known rather than systematic investiga- tions on the effects of different chemical functions anchored on the particle surface. In this chapter, we present an extensive study on the binding of APTES, a common silane surface modifier, with boehmite, and show that thermogravimetric analysis (TGA) coupled with mass spectrometry (MS) is a convenient and highly suitable method to elucidate the ligand binding in detail. Furthermore, a two-step coupling strategy is presented, demonstrating that based on APTES anchored to the parti- cle surface, the condensation of various carboxylic acids can be utilized to enable highly diverse chemical properties of the nanofillers, which leads to very different particle-matrix interactions in the nanocomposites. KW - APTES KW - Boehmite KW - Nanoparticle KW - TGA-MS PY - 2021 SN - 978-3-030-68522-5 SN - 978-3-030-68523-2 DO - https://doi.org/10.1007/978-3-030-68523-2 SN - 2194-8240 SN - 2194-8259 SP - 119 EP - 142 PB - Springer Nature Switzerland AG CY - Cham AN - OPUS4-53727 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Bonse, Jörn A1 - Kirner, Sabrina V. A1 - Krüger, Jörg ED - Sugioka, K. T1 - Laser-Induced Periodic Surface Structures (LIPSS) N2 - Laser-induced periodic surface structures (LIPSS) are a universal phenomenon and can be generated on almost any material by irradiation with linearly polarized radiation. This chapter reviews the current state in the field of LIPSS, which are formed in a “self-ordered” way and are often accompanying materials processing applications. LIPSS can be produced in a single-stage process and enable surface nanostructuring and, in turn, adaption of optical, mechanical, and chemical surface properties. Typically, they feature a structural size ranging from several micrometers down to less than 100 nm and show a clear correlation with the polarization direction of the light used for their generation. Various types of LIPSS are classified, relevant control parameters are identified, and their material-specific formation mechanisms are analyzed for different types of inorganic solids, i.e., metals, semiconductors, and dielectrics. Finally, technological applications featuring surface functionalization in the fields of optics, fluidics, medicine, and tribology are discussed. KW - Laser-induced periodic surface structures (LIPSS) KW - Femtosecond laser KW - Laser ablation KW - Microstructures KW - Nanostrcutures PY - 2021 SN - 978-3-030-63646-3 (Print) SN - 978-3-030-63647-0 (Online) DO - https://doi.org/10.1007/978-3-030-63647-0_17 SP - 879 EP - 936 PB - Springer-Nature Switzerland AG CY - Cham ET - 1 AN - OPUS4-53728 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Jauregui-Correa, J. C. A1 - Otremba, Frank A1 - Romero-Navarrete, José A. A1 - Hurtado-Hurtado, G. ED - Pucheta, M. ED - Cardona, A. ED - Preidikman, S. ED - Hecker, R. T1 - Determination of the Effect of Sloshing on the Railcar-Track Dynamic Behavior N2 - This paper presents the study of the impact caused by a liquid Cargo on a railway infrastructure. The dynamic behavior of a tank car corresponds to a multibody dynamic system with several degrees of freedom. This study’s data were obtained from a scale experimental fixture consisting of a track and a railcar with a tank. The track was instrumented with strain gauges and the railcar with accelerometers. The data showed non-periodic and periodic terms; therefore, the results were analyzed with the Empirical Mode Decomposition method (EMD). It was found that the EMD identified the signal components that were related to the sloshing. These components represent the mode shapes of the original signal. The location of the sloshing in the track was found applying spectrograms to the accelerometer data. This paper’s experimental outputs suggest that the sloshing effect is detectable at the track and in the vehicle dynamics. KW - Sloshing effect KW - Empirical Mode Decomposition KW - Wheel/track interaction KW - Multibody dynamics PY - 2021 SN - 978-3-030-88750-6 DO - https://doi.org/10.1007/978-3-030-88751-3_14 SP - 131 EP - 140 PB - Springer Nature Switzerland AG AN - OPUS4-53561 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Bertovic, Marija A1 - Virkkunen, I. ED - Meyendorf, N. ED - Ida, N. ED - Singh, R. ED - Vrana, J. T1 - NDE 4.0: New Paradigm for the NDE Inspection Personnel N2 - Nondestructive evaluation (NDE) is entering an era of the fourth industrial revolution and will undergo a major transformation. NDE is a vital part of industry and a successful move to NDE 4.0, it will require not just developing and embracing new technologies, but also developing and adopting new ways of working and becoming an integral part of the overall Industry 4.0. This will pose new challenges for the inspection personnel. To ensure the expected benefits from NDE 4.0, inspectors need stay in charge of the changing inspections. The promised autonomy and interconnectedness of NDE 4.0 will supersede the majority of traditional inspector tasks and will in turn require a different set of skills and raise different demands and challenges for the inspection personnel, thus conflicting the current “procedure-following”-“level I-III” paradigm. The new industry 4.0 technologies can be integrated into the current framework, but exploiting their full potential requires changes in the role of the inspectors. The inspectors will be relieved from the tedious and error-prone aspects of the current system. At the same time, they will need to take responsibility for increasingly complex automated systems and work in closer collaboration with other experts. We propose that the traditional inspector roles will be transformed into that of the system developer, caretaker, and problem solver, each requiring a specific set of skills and assuming different responsibilities. For full NDE 4.0, NDE must abandon its traditional role as a self-contained entity with well-defined boundaries and take its role in the wider system that is the industry 4.0. KW - Non-Destructive Evaluation KW - NDE 4.0 KW - Industry 4.0 KW - Inspection Personnel KW - Human-Centered Approach KW - Human-Machine Interaction KW - Human Factors KW - Acceptance PY - 2021 SN - 978-3-030-48200-8 DO - https://doi.org/10.1007/978-3-030-48200-8_9-1 SP - 1 EP - 31 PB - Springer, Cham AN - OPUS4-53551 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Niederleithinger, Ernst A1 - Wang, Xin A1 - Epple, Niklas A1 - Schumacher, T. A1 - Ahmend, S. A1 - Klikowicz, P. ED - Yokota, H. ED - Frangopol, D. W. T1 - Ultrasonic coda wave monitoring of concrete structures: First experiences with large-scale experiments and real structures N2 - Ultrasonic monitoring, making use of the sensitivity of the coda of repeated transmission meas-urements to changes in stress, temperature, moisture, as well as localized or distributed damage, has gotten at-tention in structural health monitoring (SHM) research recently. Analysis methods such as coda wave inter-ferometry (CWI), including its nonlinear extension, have been shown to be able to measure ultrasonic wave velocity changes with a 1∙10-5 resolution, while indicators such as cross-correlation or cross-coherence have been used to distinguish between reversible and irreversible changes. Several small- and large-scale laboratory experiments have demonstrated that stress changes in structures can be captured or damage detected in a very early stage. The use of this technique for pre-warning before failure are currently under investigation, as well as detailed research on the physical causes and the connection between ultrasonic wave properties and materi-al/structural behavior. Recently, several of large-scale laboratory and real structures have been instrumented with embedded ultrasonic transducers to gather experience and evidence on how to use this technology in re-al-world applications. Preliminary results from installations on a new bridge, an existing bridge, a tunnel, a la-boratory earthquake test as well as a historic stadium in Germany, Poland, and the United States, respectively, are presented. Environmental influences (mainly temperature) and validation by load tests are discussed. KW - Coda wave interferometry KW - Structural health monitoring KW - Ultrasound KW - Concrete KW - Bridges PY - 2021 SN - 978-0-367-23278-8 DO - https://doi.org/10.1201/9780429279119-345 SP - 2525 EP - 2531 PB - Taylor & Francis CY - London, UK AN - OPUS4-54168 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Silveira, D. A1 - Oliveira, C. A1 - Varum, H. A1 - Ioannou, I. A1 - Miccoli, Lorenzo A1 - Tarque, N. A1 - Parisi, F. A1 - Fenu, L. A1 - Solis, M. A1 - Rodriguez-Mariscal, J. D. ED - Varum, H. ED - Parisi, F. ED - Tarque, N. ED - Silveira, D. T1 - Mechanical Characterization of Adobe Bricks N2 - The mechanical characterization of adobe bricks is an important first step in the study of the behaviour of adobe masonry. For this reason, in the last decades, different authors have conducted research on the mechanical behaviour of adobes from various regions of the world. Despite the importance of mechanical characterization, there are still only a few standards and normative documents with clear indications for the mechanical testing of earthen materials and, in general, These indications are not thorough and vary among different countries. Consequently, authors tend to adopt different types of test specimens and procedures in their experimental work, thus obtaining results that are not directly comparable. The fact that the materials and procedures traditionally used are also not standardized,varying greatly from region to region, also contributes to the difficulty of comparing results from different studies. This chapter presents a review of the indications provided by codes, standards and other technical recommendations for the mechanical testing of adobe bricks, as well as a detailed review of procedures adopted, and results obtained by different authors regarding the mechanical characterization of traditional adobe bricks. This chapter focuses, in particular, on the behaviour of adobe bricks when subjected to simple compression. It provides an overview of the existing knowledge and identifies needs for future research and development. KW - Adobe KW - Adobe masonry KW - Mechanical behaviour KW - Test procedures KW - Standards PY - 2021 SN - 978-3-030-74736-7 DO - https://doi.org/10.1007/978-3-030-74737-4 SN - 2194-9832 VL - 20 SP - 35 EP - 54 PB - Springer Nature Switzerland AG AN - OPUS4-54170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Oliveira, C. A1 - Silveira, D. A1 - Varum, H. A1 - Parisi, F. A1 - Miccoli, Lorenzo A1 - Solis, M. A1 - Rodriguez-Mariscal, J. D. A1 - Tarque, N. ED - Varum, H. ED - Parisi, F. ED - Tarque, N. ED - Silveira, D. T1 - Mechanical Characterization of Adobe Masonry N2 - The characterization of the mechanical properties and behaviour of adobe masonry is fundamental for the understanding of the structural behaviour of adobe constructions. Thus, in the last decades, experimental studies focused on this topic have been carried out by different authors. Many of the existing experimental works, however, were carried out aiming to support broader studies focused on the seismic behaviour of adobe constructions and are not very detailed. Moreover, authors tend to adopt different procedures in their experimental work, since there are few indications in existing standards for testing adobe masonry. The wide variety in materials used, both for the adobes and mortars, further complicates this work, making it difficult to compare results obtained in different studies. This chapter provides an overview of the indications given by standards and other technical recommendations for the mechanical testing of adobe masonry. It presents a review of existing research on the mechanical behaviour of adobe masonry, addressing studies that focus on: (i) compression behaviour, (ii) shear behaviour, (iii) joint shear behaviour. It provides a global analysis of the existing knowledge, suggesting improvements for normative documents and identifying future Research needs. KW - Adobe masonry KW - Mechanical behaviour KW - Experimental tests KW - Standards PY - 2021 SN - 978-3-030-74736-7 DO - https://doi.org/10.1007/978-3-030-74737-4_4 SN - 2194-9832 VL - 20 SP - 55 EP - 92 PB - Springer Nature Switzerland AG AN - OPUS4-54171 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Gehlen, C. A1 - Kränkel, T. A1 - Meng, Birgit A1 - Osterminski, K. A1 - Meyer, F. A1 - Schröder, P. ED - Zilch, K. T1 - Baustoffe im Betonbau N2 - In dem Kap. „Baustoffe im Betonbau“ werden zunächst die Baustoffe vorgestellt, die für die Herstellung von Stahlbeton- und Spannbetonbauwerken erforderlich sind (im Wesentlichen Beton, Betonstahl und Spannstahl). Herstellungsbedingte, typische Eigenschaftsprofile der Baustoffe werden aufgezeigt und ein Bezug zu entsprechenden Anwendungsgebieten hergestellt. KW - Betontechnik KW - Bindemittel KW - Betonstahl KW - Spannstahl KW - Herstellungsprozesse KW - Eigenschaften KW - Anwendungsbeispiele PY - 2019 SN - 978-3-658-21749-5 DO - https://doi.org/10.1007/978-3-658-21749-5_15-1 SP - 1 EP - 63 PB - Springer Fachmedien Wiesbaden GmbH AN - OPUS4-54173 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Niederleithinger, Ernst ED - Meyendorf, N. ED - Ida, N. ED - Singh, R. ED - Vrana, J. T1 - NDE 4.0 in Civil Engineering N2 - Civil engineering industry is one of the most important industry sectors in the worldwide economy. It contributes significantly to the gross economic product and general employment. Even more important, it provides many of the basic needs of the society (e.g., housing, infrastructure, and protection from natural hazards). The concept of “Industry 4.0” or “Smart Production” has not yet made significant progress in the civil engineering industry. The designing, building, and operating processes are still widely dominated by the exchange of printed documents and drawings. Most objects (buildings and other constructions) are unique, and a large part of the production still requires a large amount of manual labor. As-built documentation and quality assurance are often neglected. Civil engineering is among the industry sectors with the lowest level of digitalization and the lowest gain in productivity. However, this is going to change. In the past decade, several drivers have challenged the ways clients, contractors, and authorities currently operate. These drivers include but are not limited to an increasing demand for serialization and automatization or the mandatory introduction of “Building Information Modeling” (BIM) in public procurement as well as the upcoming use of digital twins. NDE plays an increasing role in quality assurance, condition assessment, and monitoring of structures. However, with very few exceptions, applications are mostly nonstandardized and performed only at selected sites. To change this, the NDT-CE community including manufacturers, service providers, clients, and the scientific community must work consistently on open data formats, interfaces to BIM, standardization, and validated ways for a quantitative use of the results in the assessment of constructions. KW - NDE 4.0 KW - Civil engineering KW - BIM KW - IFC PY - 2021 SN - 978-3-030-48200-8 DO - https://doi.org/10.1007/978-3-030-48200-8 SP - 1 EP - 14 PB - Springer Nature CY - Cham, Switzerland AN - OPUS4-54161 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Böllinghaus, Thomas A1 - Rhode, Michael A1 - Falkenreck, T. ED - Bender, B. ED - Göhlich, D. T1 - Korrosion und Korrosionsschutz N2 - Das Kapitel beginnt mit einer kurzen Einführung über die Korrosion (Wechselwirkung zwischen einem Metall, einer korrosiven Umgebung und der der jeweiligen Konstruktion). Im zweiten Abschnitt werden die wichtigsten Formen der wässrigen elektrochemischen Korrosion (Flächenkorrosion, galvanische, selektive und interkristalline Korrosion sowie Loch- und Spaltkorrosion) betrachtet. Darüber hinaus wird die elektrochemische Korrosion unter mechanischer Belastung betrachtet (Spannungsrisskorrosion, wasserstoffunterstützte Rissbildung, Korrosionsermüdung), sowie Sonderformen der Korrosion (Erosion, Fretting und mikrobiologisch induzierte Korrosion). Der dritte Abschnitt befasst sich mit der chemischen und Hochtemperaturkorrosion (Oxidation, Aufkohlung, Hochtemperatur-Wasserstoffangriff, Aufschwefelung, Nitrierung, Halogenierung). Zusätzlich enthält das Kapitel Maßnahmen zur Vermeidung der Korrosion. KW - Korrosion KW - Korrosionsschutz KW - Spannungsrisskorrosion KW - Wasserstoff KW - Loch- u. Spaltkorrosion PY - 2021 SN - 978-3-662-59710-1 DO - https://doi.org/10.1007/978-3-662-59711-8_34 VL - 1 SP - 691 EP - 725 PB - Springer-Verlag GmbH, ein Teil von Springer Nature CY - Berlin ET - 26 AN - OPUS4-52156 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Droste, Bernhard A1 - Wolff, Dietmar A1 - Bevilacqua, A. A1 - Reiche, I. A1 - Harvey, J. A1 - Hirose, M. A1 - Kumano, Y. A1 - McConnell, P. A1 - Saegusa, T. A1 - Einziger, R. ED - González-Espartero, A. T1 - Methodology for a Safety Case of a Dual Purpose Cask for Storage and Transport of Spent Fuel N2 - Spent nuclear fuel which is generated in the operation of nuclear reactors needs to be safely managed following its removal from the reactor core. On-site power reactor storage pools were designed on the assumption that after a short period of time spent nuclear fuel would be removed for reprocessing and disposal or further storage elsewhere. The amount of highly radioactive spent fuel that needs to be stored over longer periods of time is growing and additional storage capacity is required. One of the widely used options for additional storage capacity is the use of casks for dry storage of spent fuel. Among various existing dry storage concepts, several Member States are utilizing a concept of dual purpose casks (DPCs). This publication provides practical advice on the structure and contents of a DPC integrated safety case with reference to existing IAEA requirements relevant to the licensing and use of transport and storage casks for spent fuel. KW - Dual Purpose Cask KW - Spent Fuel KW - Storage KW - Transport PY - 2020 UR - https://www.iaea.org/publications/10966/methodology-for-a-safety-case-of-a-dual-purpose-cask-for-storage-and-transport-of-spent-fuel SN - 978-92-0-131620-2 SN - 1011–4289 SP - 1 EP - 109 PB - IAEA Publishing Section CY - Vienna, Austria AN - OPUS4-51962 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Küttenbaum, Stefan A1 - Feistkorn, S. A1 - Braml, T. A1 - Taffe, A. A1 - Maack, Stefan ED - Rizzo, P. ED - Milazzo, A. T1 - Methods to Quantify the Utility of NDT in Bridge Reassessment N2 - The purpose of this contribution is to introduce and to apply the developed approach of incorporating non-destructively gathered measurement results (instead of deterministic information and assumptions) into a reassessment model of a typical prestressed concrete road bridge and to outline the advantages. An essential part is the quality evaluation of the non-destructively measured information, that deals primarily with two questions. Could the object or parameter to be obtained reliably detected and if, how accurate are the inspection results achieved? Therefore, the importance of the combination of a probability of detection (POD)-approach and measurement uncertainty calculations is emphasized. With regard to the introduced case-study it is shown, for which structure parameters an assumption deviating from the actual (and measurable) situation has a particularly strong (and possibly arithmetically unfavorable) influence on the structural reliability. Measurements on such parameters are particularly beneficial for a reliable and robust reassessment. In conclusion, the individual reassessment results without consideration and with consideration of evaluated non-destructive inspection results are compared. KW - Non-destructive testing (NDT) KW - Structural safety KW - Concrete bridges KW - Measurement uncertainty KW - Probability of detection (POD) PY - 2021 SN - 978-3-030-64593-9 DO - https://doi.org/10.1007/978-3-030-64594-6_40 SN - 2366-2557 VL - 127 SP - 403 EP - 413 PB - Springer Nature Switzerland CY - Cham, Switzerland AN - OPUS4-52009 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Epple, Niklas A1 - Fontoura Barroso, Daniel A1 - Niederleithinger, Ernst ED - Rizzo, P. ED - Milazzo, A. T1 - Towards Monitoring of Concrete Structures with Embedded Ultrasound Sensors and Coda Waves – First Results of DFG for CoDA N2 - Due to the importance of reinforced concrete structures for modern society, damage assessment during the entire life-cycle of such structures has become a special interest in non-destructive testing. Using embedded ultrasound sensors in combination with other measurement methods, numerical modeling and self-made data collectors, tailored specifically for monitoring tasks, the German research group DFG FOR CoDA aims to investigate and develop novel methods for damage detection and rapid model updating in reinforced concrete structures. In the first stage of the project, besides the development of custom-built, low-cost data collectors, ultrasonic transducers are embedded in a large, reinforced concrete specimen on a BAM test site near Berlin. In this experiment, the influence of changing environmental conditions (mainly temperature) on the ultrasound signal is investigated using coda-wave interferometry. The results show a correlation between changes in temperature and ultrasonic velocity. Such changes must be taken into consideration in a long-term monitoring setup to distinguish between reversible and permanent changes. By correcting the data using a linear relation between concrete temperature and velocity change to remove the seasonal trends and by low-pass filtering the data to remove daily variations can remove most of the temperature influence on the ultrasound measurements. KW - Ultrasound KW - Coda Wave Interferometry (CWI) KW - Embedded sensors KW - Structural health monitoring PY - 2021 SN - 978-3-030-64593-9 SN - 978-3-030-64594-6 DO - https://doi.org/10.1007/978-3-030-64594-6_27 VL - 127 SP - 266 EP - 275 PB - Springer Nature CY - Cham, Switzerland AN - OPUS4-52012 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Otremba, Frank A1 - Hildebrand, R. A1 - Romero Navarrete, J. A. A1 - Sklorz, Christian ED - Otremba, Frank T1 - A simplified analytical approach on the dynamic pressures in cylindrical vertical tanks N2 - A simplified methodology is proposed to estimate the dynamic pressures developed within partially filled cylindrical vertical tanks when subjected to earthquake-related horizontal accelerations. The total pressure at the bottom of the tank is calculated as the superposition of vertical and horizontal pressures. While the magnitude of the vertical pressure depends on the free surface height of the liquid, the horizontal pressure depends on the magnitude of the horizontal acceleration and on the diameter of the tank. The liquid free surface oscillation angle is simulated based upon the principles of the simple pendulum analogy for sloshing. The length of the pendulum, however, is set on the basis of a methodology to calculate the free sloshing frequency of partially filled containers. Such a methodology is experimentally verified in this work. The outputs of the model for full scale situations, suggest that the lateral perturbation - sloshing phenomenon (earthquake effect) can generate an increase in the total pressure of 56% above the no lateral perturbation situation, further suggesting that such an overpressure should be taken into account when designing tanks that could be potentially subjected to earthquake-related perturbations. KW - Vertical cylindrical tanks KW - Pendulum analogy KW - Experimental approach KW - Sloshing, transition matrix approach KW - Hazmat PY - 2021 SN - 978-981-15-8273-8 SP - 1 EP - 15 PB - Springer AN - OPUS4-51982 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Adam, Christian ED - Holm, O. ED - Thome-Kozmiensky, E. ED - Quicker, P. ED - Kopp-Assenmacher, S. T1 - Verwertung von Klärschlamm N2 - Die natürlichen Nährstoffkreisläufe werden durch anthropogene Einflüsse, wie das Einbringen von Schadstoffen in nährstoffreiche Stoffströme, und die ungünstige lokale Verteilung der Nährstoffe (z.B. im Zuge der Intensivtierhaltung), erheblich gestört. Es sind lokale Unter- und Überversorgungen mit Nährstoffen zu beobachten. Gelangen die Nährstoffe in Gewässer, kommt es zum bekannten Phänomen der Eutrophierung. Hierbei ist der Nährstoff Phosphat meist der limitierende Faktor und es bestehen große Bestrebungen den anthropogenen Eintrag in Fließgewässer, Seen und Binnenmeere zu unterbinden. Der Schutz der Ostsee vor Nährstoffeinträgen ist beispielsweise ein sehr wichtiges Thema geworden und wird u.a. von der Baltic Sea Action Group verfolgt. Weitere Auswirkungen des bestehenden Systems sind Entzüge aus dem Nährstoffkreislauf, wie etwa bei der Deponierung phosphor- aber gleichzeitig auch schadstoffhaltiger Klärschlammaschen oder bei der Mitverbrennung von Klärschlamm in Müllverbrennungsanlagen, Kraftwerken oder Zementwerken. Hier wird das Phosphat ebenfalls als Bestandteil von Aschen deponiert oder in Form von Baustoffen einer sinnvollen stofflichen Nutzung entzogen. Gegen diese Art des Verlusts von Phosphat aus dem Nährstoffkreislauf hat der Gesetzgeber mit der Novellierung der Klärschlammverordnung reagiert, die am 3. Oktober 2017 in Kraft getreten ist und u.a. Regelungen zur Rückgewinnung von Phosphat aus Klärschlamm und Klärschlammasche enthält. Klärschlämme aus kommunalen Abwasserbehandlungsanlagen ab einer genehmigtenAusbaugröße von über 100.000 bzw. über 50.000 Einwohnerwerten (EW) dürfen nach einer Übergangsfrist ab dem 1. Januar 2029 bzw. 2032 nicht mehr in der Landwirtschaft oder im Landschaftsbau verwertet werden. Die Betreiber dieser Anlagen sind zur Rückgewinnung des im Schlamm enthaltenen Phosphors verpflichtet, wenn der Klärschlamm einen Phosphorgehalt von 20 g/kg Trockenrückstand (TR) oder mehr aufweist. Für Klärschlämme mit P-Gehalten > 40 g/kg TR reicht alternativ die Absenkung der P-Konzentration um 50 % aus. Die Rückgewinnung kann aus dem Schlamm oder aus der Verbrennungsasche des thermisch vorbehandelten Klärschlamms erfolgen. Aus der Asche müssen mindestens 80 % des Phosphoranteils zurückgewonnen werden. Anstelle einer Phosphorrückgewinnung aus Klärschlämmen aus kleineren und mittelgroßen Abwasserbehandlungsanlagen (bis 50.000 EW) können diese Schlämme auch weiterhin zu Düngezwecken auf Böden ausgebracht werden, sofern die Anforderungen und insbesondere die Grenzwerte der Klärschlammverordnung und des Düngerechts eingehalten werden. In der Abwasserreinigung wird der Makronährstoff Phosphor je nach Typ und Größe der Abwasserreinigungsanlage durch verschiedene Verfahren der Phosphatelimination weitgehend in die feste Phase, den Klärschlamm, überführt. Dies geschieht durch die Zugabe von Fällmitteln auf der Basis von Eisen- oder Aluminiumsalzen, oder durch das Verfahren der vermehrten biologischen Phosphorelimination (Bio-P). Das Phosphat liegt nun abhängig vom eingesetzten Verfahren als Bestandteil der gewachsenen Biomasse, als gefälltes Salz, adsorbiert an Eisen(oxi)hydroxiden oder im Falle der Bio-P Klärschlämme auch intrazellulär in Form von Polyphosphaten vor. Weitergehende Informationen hierzu sind im Beitrag von Kratz et al. Pflanzenverfügbarkeit und agronomische Effizienz von klärschlamm-basierten Phosphor (P) – Recyclingdüngern in diesem Buch zu finden. Die Bindungsformen unterscheiden sich demnach nach Art der eingesetzten Technologie der Phosphatelimination erheblich und haben einen entscheidenden Einfluss auf die verschiedenen Möglichkeiten der P-Extraktion und Rückgewinnung. KW - Abwasser KW - Phosphor KW - Klärschlamm KW - Klärschlammasche KW - Recycling PY - 2018 SN - 978-3-94431-043-5 SP - 165 EP - 186 PB - Thome-Kozmiensky Verlag GmbH CY - Neuruppin AN - OPUS4-46549 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Kratz, S. A1 - Adam, Christian A1 - Vogel, Christian ED - Holm, O. ED - Thome-Kozmienski, E. ED - Quicker, P. ED - Kopp-Assenmacher, S. T1 - Pflanzenverfügbarkeit und agronomische Effizienz von klärschlammbasierten Phosphor (P)-Recyclingdüngern N2 - Die agronomische Effizienz von Düngemitteln wird üblicherweise im Vegetationsversuch geprüft. Vegetationsversuche erlauben die Betrachtung unterschiedlicher Kulturpflanzen und deren Strategien der Nährstoffmobilisierung und -Aneignung ebenso wie die Berücksichtigung verschiedener Substrattypen und deren Eigenschaften hinsichtlich Nährstofffixierung und -freisetzung. Solche Versuche, selbst wenn sie nicht im Feld, sondern nur im Gefäß durchgeführt werden, sind jedoch sowohl zeit- als auch kostenintensiv. In erster Näherung wird die Pflanzenverfügbarkeit insbesondere von Phosphor (P)-Düngemitteln daher herkömmlicherweise mit Hilfe standardisierter chemischer Extraktionsmethoden abgeschätzt, deren Durchführung in der deutschen ebenso wie in der europäischen Düngemittelverordnung normiert ist. Diese Methoden werden auch im Rahmen der staatlichen Düngemittelverkehrskontrolle genutzt, um die Einhaltung düngemittelrechtlicher Vorgaben zu überprüfen. Wie jüngere Arbeiten gezeigt haben, ist jedoch die Übertragung herkömmlicher Standardextraktionsmethoden auf neue Dünger aus Recyclingmaterialien wie Klärschlamm mit einigen Schwierigkeiten verbunden. Korrelationen zwischen P-Aufnahme im Vegetationsversuch und chemischer Löslichkeit im Standardextrakt sind oft nur mäßig bis schwach oder überhaupt nicht signifikant. Die vorliegende Literaturübersicht gibt einen Überblick zum aktuellen Stand des Wissens über die chemische Löslichkeit von klärschlammbasierten P-Recyclingdüngern, deren Effizienz im Vegetationsversuch und statistische Relationen zwischen beiden Parametern. Anschließend werden alternative Methoden zur Abschätzung der P-Verfügbarkeit von Recyclingdüngern vorgestellt, die derzeit Gegenstand der wissenschaftlichen Diskussion sind. KW - P-Recyclingdünger KW - Phosphat KW - DGT-Methode KW - Agronomische Effizienz PY - 2018 SN - 978-3-944310-43-5 SP - 391 EP - 408 PB - Thome-Kozmiensky Verlag GmbH CY - Neuruppin AN - OPUS4-46551 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Lübben, S. A1 - Enzner, V. A1 - Holm, Olaf ED - Thiel, S. ED - Thome-Kozmiensky, E. ED - Friedrich, B. ED - Pretz, T. ED - Quicker, P. ED - Senk, D. G. ED - Wotruba, H. T1 - Aufbereitung von Teilströmen der Abfallverbrennungsasche zu hochwertigen Zuschlagstoffen und deren Einsatz als Recyclingprodukte in der Baustoffindustrie T1 - Treatment of Separated Mass Fractions of Waste Incineration Bottom Ashes for the Use as Secondary Construction Material N2 - In the framework of the project OPTIMIN a fractionation of BA in different grain size distributions with an integrated washing step has been carried out. Due to further treatment and measurements of the resulting three fractions 0–0.2 mm, 0.2–2 mm and 2–25 mm, the possible application in asphalt, concrete or cement has been investigated. One option could be the use of fresh BA which has been treated prior to the ageing processes. The preliminary results show the shifting of pollutants to the fine fraction but also components responsible for the ageing processes. Parts of the fine fraction hold the limit values for the cement plant of the project partner. On the other hand, the Contents of copper and zinc exceed the standard values for the process. The coarser fractions are free from mineral coatings and are not agglomerated in the case of the use of fresh BA. A following industrial separation step of glass has been successful. From the physical point of view an application in asphalt or concrete for the coarser fractions seems to be feasible. However, in leaching experiments a high release of different metals, especially copper, could be detected. This is probably due to the poorly conceived washing process but needs to be further investigated. N2 - Im Rahmen des Projekts OPTIMIN wurde eine Fraktionierung von Rostasche in verschiedene Korngrößenverteilungen mit integriertem Waschschritt durchgeführt. Aufgrund der weiteren Behandlung und Analyse der resultierenden drei Fraktionen 0–0,2 mm, 0,2–2 mm und 2–25 mm wurde die mögliche Verwertung in Asphalt, Beton oder Zement untersucht. Eine Option könnte die Verwendung von frischer Rostasche sein, die vor dem Einsetzen von Alterungsprozessen behandelt wird. Die vorläufigen Ergebnisse zeigen die Verlagerung von Schadstoffen in die Feinfraktion, aber auch von Anteilen, die für die Alterungsprozesse verantwortlich sind. Teile der Feinfraktion halten die Grenzwerte für das Zementwerk des Projektpartners ein. Andererseits übersteigen die Gehalte an Kupfer und Zink die Vorgabewerte für den Prozess. Die gröberen Fraktionen sind frei von mineralischen Anhaftungen und agglomerieren bei der Verwendung von frischer Rostasche nicht. Die nachfolgende Abtrennung von Glas war erfolgreich. Aus bauphysikalischer Sicht erscheint eine Anwendung in Asphalt oder Beton für die gröberen Fraktionen möglich. In Auslaugtests konnte jedoch eine hohe Freisetzung verschiedener Metalle, insbesondere Kupfer, nachgewiesen werden. Dies ist wahrscheinlich auf den schlecht konzipierten Waschprozess zurückzuführen, muss jedoch weiter untersucht werden. KW - Ersatzbaustoffe KW - Rostasche PY - 2018 SN - 978-3-944310-41-1 VL - 5 SP - 152 EP - 172 PB - TK Verlag CY - Neuruppin ET - 1 AN - OPUS4-46618 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Herzel, Hannes A1 - Kugler, Stefan Anton A1 - Schaaf, T. A1 - Adam, Christian ED - Holm, O. ED - Thome-Kozmiensky, E. ED - Quicker, P. ED - Kopp-Assenmacher, S. T1 - Herstellung neuer Düngemittelausgangsstoffe durch thermochemische Behandlung von Klärschlammaschen N2 - Klärschlammasche kann viel Phosphor enthalten (bis zu 12%). Aus diesem Grund ist diese Asche ein gutes Ausgangsmaterial für Phosphordünger. Aufgrund der geringen Pflanzenverfügbarkeit des Phosphors in der Asche ist eine Aufbereitung notwendig. In diesem Buchbeitrag wird das thermochemische Verfahren AshDec vorgestellt, welches von dem Fachbereich 4.4 mit der Firma Outotec entwickelt worden ist. Es werden die Hintergründe diskutiert, die Phasenreaktionen bei diesem Prozess besprochen, Pflanzenversuche ausgewertet, verschiedene Extraktionen diskutiert und ein Konzept für eine mögliche Pilotanlage dargestellt. KW - Phosphor KW - Extraktionen KW - Alkalien KW - Thermochemisch PY - 2018 SN - 978-3-94431-043-5 SP - 495 EP - 512 PB - Thome-Kozmiensky Verlag GmbH CY - Neuruppin AN - OPUS4-46603 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Daum, Werner A1 - Czichos, Horst ED - Grote, Karl-Heinrich ED - Bender, Beate ED - Göhlich, Dietmar T1 - Messtechnik und Sensorik N2 - Für den allgemeinen Maschinenbau wichtige Messtechnik und Sensorik werden grundlegend und anwendungsbezogen beschrieben. KW - Messtechnik KW - Sensorik KW - Maschinenbau PY - 2018 SN - 978-3-662-54804-2 DO - https://doi.org/10.1007/978-3-662-54805-9 SP - W 2 EP - W 44 PB - Springer Vieweg CY - Berlin ET - 25 AN - OPUS4-47132 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Oesch, Tyler A1 - Stelzner, Ludwig A1 - Weise, Frank ED - Herrmann, H. ED - Schnell, J. T1 - Non-destructive evaluation of the contribution of polymer-fibre orientation and distribution characteristics to concrete performance during fire N2 - Although concrete itself is not a combustible material, concrete mixtures with high density, such has high-performance concretes (HPCs), are susceptible to significant damage during fires due to explosive spalling. Past research has shown that the inclusion of polymer fibres in high density concrete can significantly mitigate this fire damage. The exact mechanisms causing this increased spalling resistance are not yet fully under-stood, but it is thought that the fibres facilitate moisture transport during fire exposure, which in turn contributes to relief of internal stresses in the spalling-susceptible region. In this study, X-ray Computed Tomography (CT) was applied to observe the interaction between polymer fibres and cracking during thermal exposure. For this purpose, two concrete samples containing different polymer fibre types were subjected to incremental application of a defined thermal exposure. CT images were acquired before and after each thermal exposure and powerful image processing tools were used to segment the various material components. This enabled a detailed analysis of crack formation and propagation as well as the visualization and quantification of polymer fibre characteristics within the concrete. The results demonstrated that the orientation of both fibres and cracks in polymer-fibre reinforced concrete tend to be anisotropic. The results also indicated that crack geometry characteristics may be correlated with fibre orientation, with cracks tending to run parallel to fibre beds. Clear quantitative relationships were also observed between heating and increasing cracking levels, expressed in terms of both crack surface area and crack volume. KW - X-ray Computed Tomography (CT) KW - Polypropylene Fibres KW - Fire Performance KW - Fibre-Reinforced Concrete (FRC) KW - Fibre Orientation Analysis PY - 2019 SN - 978-3-030-00868-0 DO - https://doi.org/10.1007/978-3-030-00868-0 SP - 51 EP - 73 PB - Springer Nature Switzerland AG AN - OPUS4-47206 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Knabe, Nicole A1 - Gorbushina, Anna ED - Gurtler, V. ED - Trevors, J. T. T1 - Territories of rock-inhabiting fungi: Survival on and alteration of solid air-exposed surfaces N2 - Subaerial biofilms that are omnipresent at the interface between all solid substrates and the atmosphere are composed of a unique and widespread group of ascomycetes called rock-inhabiting fungi or microcolonial fungi (MCF), typically in communities with other microorganisms. While subaerial biofilms in toto have important roles in mineral weathering and biodeterioration of materials, methodological approaches to subaerial biofilm communities are diverse and frequently focussed on MCF. Here, we review the historical development of the research methods applied in the field and consider perspectives to increase our understanding of the biofilm-induced changes of solid substrate surfaces. KW - Biologically induced mineral weathering KW - Geobiology KW - Microcolonial fungi KW - Subaerial biofilm KW - Symbiosis PY - 2018 UR - https://linkinghub.elsevier.com/retrieve/pii/S0580951718300047 SN - 9780128146040 DO - https://doi.org/10.1016/bs.mim.2018.06.001 VL - 45 SP - Chapter 6, 145 EP - 169 PB - Elsevier AN - OPUS4-47181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schmidt, Wolfram A1 - Leinitz, Sarah A1 - Mota, Berta A1 - Crasselt, Claudia ED - Liu, Jiaping ED - Wang, Ziming ED - Holland, Terence ED - Huang, Jing ED - Plank, Johann T1 - Influence of the aqueous phase of cement paste on the rheology in the presence of PCE N2 - The paper presents rheometric results and hydration curves for cementitious systems based on cement mixed with different aqueous phases at solid volume fraction of  = 0.45. The varied aqueous phases were deionized water, limewater, the filter residue of a cement paste mixed at w/c = 2.0, and the filtrate of cement paste at solid volume fraction of 0.45. Each cementitious system provided different amounts and sizes of particles formed in the aqueous phase. The pastes were observed with and without polycarboxylate ether based superplasticizer. It was observed that the presence of particles causes higher PCE saturation dosages to achieve a minimum value, but the minimum value is only affected in the case of large particles. In all cases with and without PCE, the presence of small particles causes increased plastic viscosity. In addition, with decreased number and size of hydrates in the aqueous phase the hydration was retarded, which was specifically pronounced in the presence of PCE KW - Aqueous phase of cement paste KW - Polycarboxylate ether KW - Rheology KW - Yield stress KW - Plastic viscosity KW - Heat of hydration KW - Syngenite KW - Solid volume fraction PY - 2018 SN - 978-1-64195-029-9 SP - SP-329-34, 428 EP - 443 PB - American Concrete Institute CY - Farmington Hill, Michigan AN - OPUS4-47107 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Wolff, Dietmar A1 - Völzke, Holger A1 - Bevilacqua, A. A1 - Alejano, C. A1 - Conde, J.M. A1 - Einziger, R.E. A1 - Fukuda, S.-I. A1 - González Espartero, A. A1 - Gouzy-Portaix, S. A1 - Haddad Andalaf, R.E. A1 - Hambley, D. A1 - Issard, H. A1 - Kessler, J. A1 - Kurpaska, L. A1 - Legat, A. A1 - Qureshi, A.H. A1 - Ruiz, J. A1 - Shirai, K. A1 - Šmaižys, A. A1 - Verrastro, C.A. ED - González Espartero, A. T1 - Demonstrating performance of spent fuel and related storage system components during very long term storage - Final report of a coordinated research project N2 - This publication summarizes the work carried out during an IAEA coordinated research project (CRP) on safe and reliabe management of spent nuclear fuel. This work contributes to the overall goal of demonstrating the performance of spent nuclear fuel and related storage systems components over long durations, and facilitates the transfer of this knowledge to Member States. The technical areas addressed by the CRP participants were related to potential degradation mechanisms in metal casks and concrete overpacks, such as stress corrosion cracking; long term integrity and performance of the fuel cladding; thermo-mechanical behaviour of the metal seals; and long term gamma and neutron shielding capability. The participants also considered past and ongoing demonstration programmes. For each technical topic addressed the main conclusions have been drawn, including information on the development of specific monitoring and inspection techniques as well as future opportunities for closing relevant data gaps. A major achievement is also the establishment of a worldwide network of experts working on current research projects to demonstrate the long term performance of spent fuel in dry storage systems. KW - Spent fuel KW - Storage system components KW - Very long term storage PY - 2019 UR - https://www.iaea.org/publications/13553/demonstrating-performance-of-spent-fuel-and-related-storage-system-components-during-very-long-term-storage SN - 978–92–0–103319–2 SN - 1011–4289 VL - 1878 SP - 1 EP - 198 PB - IAEA Publishing Section CY - Vienna, Austria AN - OPUS4-48519 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Auersch, Lutz ED - Krylov, Victor T1 - Fast trains and isolating tracks on inhomogeneous soils N2 - Methods have been presented for detailed studies of railway vibration and for the fast prediction of train-induced ground vibration. The ground vibration is generated by static or dynamic loads. The main purpose of this contribution was to show the influence of inhomogeneous soils on the different vibration components. Layered soils, namely a soft layer on a stiffer half-space, yield a quite specific transmission behavior. The low-frequency and sometimes also high-frequency cut-off of the transfer function of the soil is demonstrated in theory and by experiments at many sites of which the soil model is approximated from dispersion and transfer function measurements. The layer frequency divides the frequency range in a low-frequency range, where the stiff half-space rules the low amplitudes, and a high amplitude high-frequency range which is mainly determined by the softer top layer. A thick soft layer yields a very low layer frequency, so that the higher soft soil amplitudes have a wider range down to low frequencies. A thin layer yields a high layer frequency, so that the high frequencies above this layer frequency are dominant. The higher the contrast between the stiff half-space and the soft layer is, the stronger the increase between the half-space and layer amplitudes, the more characteristic are the spectra of the soil transfer function. The range of measured soils has been from vS1 down to 125 m/s, vS2 up to 1000 m/s and the layer frequencies are within 10 Hz < f0 < 75 Hz. Moreover, during this measuring campaign in Switzerland, all 11 sites showed clearly the layer-on-half-space behaviour. The transfer functions of inhomogeneous soils have been used to predict the ground vibration due to dynamic axle loads which is usually thought to be the most important component. The passage of static loads, in the contrary, results in very small vibration amplitudes for low train speeds, which can only be found at near distances and at low frequencies. They attenuate very rapidly with distance and lose very rapidly the higher frequency content. The passage of static axle loads can be included in the prediction of railway vibration just for completeness. Special attention should be given to the case if the train runs with the Rayleigh-wave speed of the soil (Rayleigh train). The Rayleigh-train effect is strongest for a homogeneous half-space: At the near-field of the track the amplitudes are raised strongly compared to normal trains, and in addition, little attenuation with distance is observed. In case of a layered soil, the low-frequency cut-off reduces the frequency range and the amplitudes of the homogeneous quasi-static ground vibrations. Therefore, the Rayleigh-train effects are clearly reduced by a layered soil and they disappear if the layer frequency (for example for a thin layer) is higher than the frequency band of the axle impulse. The Rayleigh-train effect could completely disappear in a randomly inhomogeneous soil, but this has not been analysed so far. The axle impulses from static loads can have an additional, quite different effect. They can be scattered by a randomly inhomogeneous soil so that a part (the scattered part) of the axle impulse can reach further distances from the track. This can establish a certain mid-frequency component of the ground vibration which becomes dominant in the far-field, and this important component exists for all train speeds. Experimental results from BAM and international measurements show the importance of the corresponding frequency range. The mitigation of train induced ground vibration by elastic and stiff track elements has been analysed threefold. The vehicle-track interaction yields the reduction at high frequencies above the vehicle-track resonance. This is the standard effect. The filtering of trackbed errors by the bending stiffness of the track yields a certain mid-frequency effect. An even stronger mid-frequency effect is predicted for the mitigation of the scattered axle impulses by the bending stiffness and elastic elements of the track. KW - Ground vibration KW - Inhomogeneous soils KW - Train excitation KW - Prediction KW - Mitigation KW - Layered soils KW - Soft track elements KW - Track beam KW - Scattered axle impulses KW - Wavenumber method KW - Multi-beam method PY - 2019 SN - 978-0-7277-6379-2 DO - https://doi.org/10.1680/gvfhsr.63792.027 SP - Chapter 2, 27 EP - 75 PB - ICE Publishing CY - London ET - 1 AN - OPUS4-48432 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Simon, Franz-Georg A1 - Holm, Olaf A1 - Kalbe, Ute ED - Thiel, S. ED - Thome-Kozmiensky, E. ED - Pretz, T. ED - Senk, D. G. ED - Wotruba, H. T1 - Antimon in Rostaschen aus der Müllverbrennung – Auslaugverhalten und Rückschlüsse für die Aufbereitung N2 - Antimon (Sb) wird industriell vorwiegend als Flammschutzmittel in Kunststoffen verwendet. Am Ende des Lebenszyklus landet etwa die Hälfte des produzierten Sb, vorwiegend über entsprechend dotierte Kunststoffe, in Haus- und vor allem Industrieabfällen und in der Folge auch in relevanten Mengen in Rostaschen aus der Verbrennung dieser Abfälle. Zwar werden in den Produkten Sb-Verbindungen in der Oxidationsstufe 3 eingesetzt, in den Aschen liegt Sb jedoch wegen der leichten Oxidierbarkeit überwiegend in der Oxidationsstufe 5 als Oxyanion vor (Sb(OH)6- oder Sb2O74-). Die Freisetzung beim Kontakt mit Wasser ist zunächst gering, weil die Antimonate schwerlösliche Verbindungen mit Ca2+ bilden. Durch die Carbonatisierung der Aschen während der vorgeschalteten Lagerung sinkt der pH-Wert im Eluat. Die Konzentration von Ca im Eluat nimmt mit fortschreitender Elutionsdauer ab, wodurch sich das Lösungsgleichgewicht verschiebt und Antimonate gelöst werden können. Dieses Verhalten wird durch einen Langzeitversuch mit Lysimetern bestätigt. Experimentelle Daten aus unterschiedlichen Elutionstests wurden mit dem Solver-Modul in MS Excel gefittet. Daraus ergibt sich Ca(Sb(OH)6)2xCa0.78(OH)1.56 als mögliche Verbindung für in Rostaschen enthaltenes Ca-Antimonat. Laut Entwurf der MantelVO ist für Sb in Rostaschen eine Regulierung vorgesehen. Die darin vorgesehenen Grenzwerte könnten ein Problem für Rostaschen darstellen und gefährden die Verwertung der mineralischen Fraktion. In den meisten Bundesländern geschieht der Vollzug derzeit nach dem LAGA Merkblatt M20. Die darin festgelegten Parameter zur Bewertung berücksichtigen im Prinzip nur eine Richtung, bei der sich die Materialeigenschaften im Zuge der Alterung von Rostaschen verbessern. Dieser Zusammenhang ist bei Sb nicht gegeben, was bei der Beurteilung des Gefahrenpotentials aber Berücksichtigung finden sollte. Das entgegengesetzte Verhalten von Sb stellt Aufbereiter und Verwerter möglicherweise vor Probleme. Die Einführung einer Ersatzbaustoffverordnung im Rahmen der MantelVO soll bundeseinheitliche Rechtssicherheit bei der Verwertung von mineralischen Recyclingmaterialien schaffen. Damit würde dann auch eine Grundlage für Investitionen in verbesserte Aufbereitungsverfahren geschaffen werden. Da im Hinblick auf Sb aus dargestellten Zusammenhängen jedoch eher das Gegenteil zu befürchten ist, besteht Forschungsbedarf, um dieses Problem zu lösen. KW - Antimon KW - Rostasche KW - Nassaufbereitung PY - 2019 SN - 978-3-944310-47-3 VL - 6 SP - 148 EP - 164 PB - TK-Verlag CY - Nietwerder ET - 1 AN - OPUS4-47989 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Syc, M. A1 - Simon, Franz-Georg A1 - Biganzoli, L. A1 - Grosso, M. A1 - Hyks, J. ED - Holm, O. ED - Thome-Kozmiensky, E. T1 - Resource recovery from incineration bottom ash: Basics, concepts, principles N2 - Waste-to-energy (WtE) is one of the leading technologies for municipal solid waste (MSW) treatment in Europe. According to Eurostat data, in 2015, 27 % of MSW was utilized in WtE plants, which represents more than 80 million tons per year. Therefore, the European annual production of incineration bottom ash (IBA) is about 20 million tons, as it is about 25 wt% of input MSW. In the European List of Waste, IBA is listed as mirror entry (i.e. waste materials which should be classified as either non-hazardous or hazardous, depending on its hazardous properties and/or content of hazardous substances) under codes 19 01 11 and 19 01 12. Recent trends indicate that WtE allows, apart from utilization of the energy content of waste, also the recovery of various valuable components. Hence, WtE can be included in the key technologies that can put the circular economy concept into practice. Secondary raw materials in the case of WtE are solid residues, especially IBA, as it is a secondary source, particularly of ferrous metals (Fe) and non-ferrous metals (NF) and glass. Moreover, the residual mineral fraction can be used for various applications in the construction industry, i.e. as aggregates substitute for bound or unbound applications, in cement manufacturing or, as indicated by recent research, also in more sophisticated applications, e.g. for ceramics production. Recovery of these metals can also cause huge greenhouse gas savings. Alone in Europe, metal recovery from IBA reduces greenhouse gas emissions by approximately 3.2 million tonnes of CO2 equivalent. KW - Bottom ash KW - Recovery PY - 2018 SN - 978-3-944310-44-2 VL - 1 SP - 1 EP - 10 PB - Thomé-Kozmiensky Verlag GmbH CY - Neuruppin ET - 1 AN - OPUS4-46146 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Golle, U. A1 - Hahn, Oliver A1 - Wintermann, C. ED - Knebel, K. ED - Ortlieb, C. ED - Püschel, G. T1 - Kunsttechnologische und materialwissenschaftliche Zugänge in der Restaurierung zu Parerga in Goethes naturwissenschaftlichen Sammlungen N2 - In Goethes naturwissenschaftlichen Sammlungen, die als Arbeits- und Studiensammlungen, zum Teil aber auch als Lehrsammlung für den Sohn August angelegt sind, haben sich sowohl die eigentlichen Sammlungsobjekte als auch deren vermeintlich ursprünglichen Kontexte durch Beschriftungen, Etiketten und in Teilen noch existierende Präsentationsmedien erhalten. Es stellt sich jedoch die grundsätzliche Frage nach deren Ursprünglichkeit. Präsentieren sich die Objekte noch so wie zur Goethezeit oder erfuhren die historischen Dichotomien im Laufe der Zeit Veränderungen, sodass die zeitgenössischen Präsentationsformen und die damit verbundenen didaktischen Funktionen heute nicht mehr lesbar sind? KW - Parerga KW - Paratext KW - ZfP KW - Archäometrie PY - 2018 SN - 978-3-95498-415-2 VL - 1 SP - 235 EP - 282 PB - Sandstein Verlag CY - Dresden AN - OPUS4-47043 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Romero-Navarrete, José A. A1 - Otremba, Frank ED - Romero-Navarrete, José A. ED - Otremba, Frank T1 - A computational scheme for assessing driving N2 - The systematization of the analysis, based on the Software proposed in this paper, could contribute to integrally improve the sustainability of the Transportation. KW - Computational scheme KW - Assessing KW - Driving PY - 2019 SN - 978-3-030-22870-5 SN - 978-3-030-22871-2 DO - https://doi.org/10.1007/978-3-030-22871-2 SN - 2194-5357 VL - 1 SP - 44 EP - 58 PB - Springer CY - Switzerland AN - OPUS4-48585 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Otremba, Frank A1 - Romero, Jose A. ED - Sio-Iong Ao, T1 - Modeling of vehicle-cargo interaction under different environments N2 - The safety of any transport system depends on a multitude of conditions, parameters and circumstances. In this regard, the interaction of the carried Cargo with the carrying vehicle represents a factor influencing the overall safety of any transport. The effects of cargo on the vehicle have to do with the vibration or shifting of the cargo, affecting the lateral stability of the vehicles and the braking performance. Such interaction has been associated to road crashes and maritime vehicles capsizing. Simulation of cargo-vehicle interaction thus represents an interesting Topic when a reduction in transport accidents is pursued. In this paper, the fundamentals principles for simulating the interaction of the liquid cargo and the carrying vehicle, is presented. In the case of a road transportation, the proposed simplified Simulation methodologies, show good agreement with a full-scale test. KW - Transition matrix approach KW - Braking performance KW - Experimental approach KW - Newton approach Ship stability KW - Sloshing PY - 2018 SN - 978-981-13-2191-7 SP - 47 EP - 57 PB - Springer Nature CY - Singapore AN - OPUS4-46773 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -