TY - CONF A1 - Müller, U. A1 - Miccoli, Lorenzo A1 - Fontana, Patrick T1 - Ein Kalkeinpressmörtel für die Instandsetzung von Lehmbauten N2 - Die Instandsetzung von Lehmbauwerken ist keine einfache Aufgabe. Der Baustoff Lehm hat vergleichsweise schwache mechanische Eigenschaften. Er ist außerdem anfällig gegenüber eindringendem Wasser, wobei er sehr schnell seinen Zusammenhalt verlieren kann, wenn gewisse Feuchtegehalte überschritten werden. Instandsetzungskonzepte für Bauwerke aus solchen Materialien stellen deshalb eine Herausforderung dar. Historische Lehmbauwerke zeigen oft Schäden in Form von starker Rissbildung, die durch statische oder dynamische Lasten hervorgerufen sein kann. Häufig werden solche Risse wegen mangelnder Fachkenntnis und / oder fehlender Techniken nur ungenügend instandgesetzt. Die Rissinstandsetzung mit Einpressmörteln birgt insbesondere für Lehmbaustoffe eine Herausforderung und erfordert spezifische Anforderungen an den Einpressmörtel, wie z. B. niedriger Wassergehalt, gutes Wasserrückhaltevermögen, niedriges Schwindmaß, an das instandzusetzende Material angepasste Festigkeit und E-Modul sowie eine gute Haftung am Lehmuntergrund. Zusätzlich müssen Einpressmörtel eine ausreichende Fließfähigkeit aufweisen, um kleine Risse und Hohlräume ohne Entmischung zu füllen. Deshalb muss das rheologische Verhalten des Einpressmörtels gut untersucht und kontrolliert werden, um die gewünschte Wirkung zu erzielen. Die Rissinstandsetzung bei Lehmbauwerken erfolgt traditionell durch manuelles Stopfen mit einem Mörtel. Natürlich können auf diese Weise nur Risse mit einer großen Breite verfüllt werden. Ein weiterer Nachteil ist, dass Risse, die durch dickere Wände verlaufen, nicht vollständig mit den für das Stopfen verwendeten Werkzeugen erreicht werden können. Kalkgebundene Einpressmörtel für Lehmbaustoffe werden gewöhnlich für die Wiederbefestigung von Putzen und weniger aus statisch-konstruktiven Gründen eingesetzt Aufgrund der Eigenschaften von Lehm, müssen Einpressmörtel auf Basis von hydraulischem Kalk nach EN 459-1 wesentliche Anforderungen an eine Reihe von Eigenschaften erfüllen, die sich auf die Verträglichkeit, die Dauerhaftigkeit und insbesondere die Injektionsfähigkeit beziehen. Das Ziel der vorgestellten Untersuchungen war einen Einpressmörtel zu herzustellen, mit dem die strukturelle Kontinuität in Lehmmauerwerk oder anderen massiven Lehmwänden (Stampf- und Wellerlehm) durch Rissverpressung wiederhergestellt werden kann. Das Material bestand aus Kalkhydrat mit Zusätzen von Puzzolanen und Kalksteinfüller. T2 - Lehm 2016 - 7. Internationale Fachtagung für Lehmbau CY - Weimar, Germany DA - 12.11.2016 KW - Baustoffe KW - Einpressmörtel KW - Kalkhydrat KW - Lehmbau KW - Instandsetzung KW - Historische Bauwerke PY - 2016 SP - 1 EP - 10 PB - Eigenverlag Dachverband Lehm e. V. CY - Weimar AN - OPUS4-38824 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, U. A1 - Miccoli, Lorenzo A1 - Fontana, Patrick T1 - A lime-based grouting material for the repair of earthen structures N2 - The repair of earthen structures is not an easy task. Earth as a construction material has comparatively weak mechanical properties. It is also susceptible towards liquid water, were it can lose cohesion very quickly if certain moisture contents are exceeded. Repair concepts of structures built with such materials are therefore challenging. Historical earthen structures often exhibit damages in form of extensive cracking, which may have been caused by static or dynamic loads. Frequently these cracks are insufficiently or inappropriately repaired because of lack of knowledge and / or technology. In particular, the behaviour of crack repair by grouting poses a challenge in earthen materials and demands specific requirements for the grouting mortar, such as low water content, good water retention, low shrinkage. Grouting materials require additional specifications such as compatible strengths and Young’s modulus as well as good adhesion to the earthen substrates. In addition, grouts have to be sufficiently flowable to fill small cracks and voids without segregation or bleeding. Therefore, the rheological behaviour has to be well understood and controlled to gain the desired effects. The repair of cracks in earthen buildings is traditionally done by stuffing manually mortar into the gap. Naturally, this method is only usable for cracks with large widths. Another disadvantage is that cracks going through thicker walls cannot be completely reached by the tools used for stuffing the mortar into the crack. Lime based grouts for earthen materials were usually used for re-attachment of plasters but less for structural reasons. Due to the nature of earthen materials grouts based on formulated or hydraulic lime (according to the definition in EN 459-1) have to meet considerable demands on a variety of properties, which are related to compatibility, durability and in particular to the ability of being injected. The goal of this study was to create a grout, which can be used to re-establish structural continuity in cracked earthen masonry or other massive earth walls (rammed earth and cob) with the focus on grouting cracks. The grout material was based on hydrated lime (calcium hydroxide) with additions of pozzolana and lime stone filler. T2 - Lehm 2016 - 7th International Conference on Building with Earth CY - Weimar, Germany DA - 12.11.2016 KW - Building Materials KW - Grout mortar KW - Hydraulic lime KW - Earth construction KW - Repair KW - Historical buildings PY - 2016 SP - 1 EP - 8 PB - Eigenverlag Dachverband Lehm e. V. CY - Weimar AN - OPUS4-38825 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Steckenmesser, D. A1 - Vogel, Christian A1 - Steffens, D. T1 - P-Verfügbarkeit von Recyclingprodukten N2 - Die Pflanzenversuche der vorliegenden Arbeit zeigen sehr gut, dass das Pyrolyse Produkt der Firma Pyreg zwar in der kurzfristigen P-Verfügbarkeit nur mäßig abschnitt, dafür aber eine gute P-Nachlieferung aufweist. Dies kann maßgeblich auf die im Produkt vorliegenden P-Verbindungen zurückgeführt werden.Es zeigt sich weiterhin, dass durch eine Na2CO3-Gabe die kurzfristige Verfügbarkeit von eisengefällten Klärschlämmen verbessert werden kann, es aber keinen Einfluss auf die langfristige P-Nachlieferung hat. Das BAM-Verfahren mit Na2SO4 liefert ein Produkt, welches sowohl eine gute kurzfristige P-Verfügbarkeit, als auch eine gute langfristige P-Nachlieferung hat. Dies kann auf die dabei entstehende P-Form, CaNaPO4, zurückgeführt werden. Ferner zeigen die Experimente, dass auch schwerlösliche Phosphate mit N2-fixierendem Rotklee mobilisiert werden können. T2 - 128. VDLUFA-Kongress CY - Rostock, Germany DA - 13.09.2016 KW - Phosphor KW - Recycling KW - Düngemittel PY - 2016 SN - 978-3-941273-23-8 SP - 57 EP - 73 PB - VDLUFA-Verlag CY - Darmstadt AN - OPUS4-38906 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Paul, Andrea A1 - Heilmann, M. T. A1 - Schmid, Thomas A1 - Maiwald, Michael T1 - Multivariate classification of Raman spectra from synthetic polymers – an approach for the improved detection of microplastics N2 - The increasing pollution of terrestrial and aquatic ecosystems with plastic debris, which leads to the accumulation of microscopic plastic particles of still unknown fate, is an upcoming problem of our time. In order to monitor the degree of contamination and to understand the underlying processes of degradation and internalization of plastic debris, analytical methods are urgently needed, which help to identify and quantify microplastics. Currently, expensive collected and purified materials enriched on filters are investigated by (micro) infrared spectroscopy (FTIR). Few studies using micro-Raman spectroscopy have been published as well. In contrast to FTIR, Raman spectroscopy can handle wet samples, but it suffers from interference of fluorescent materials. Both micro-FTIR- and micro-Raman, always include time consuming scanning and mapping procedures followed by the manual inspection and measurement of selected particles. T2 - 11. Kolloquium Arbeitskreis Prozessanalytik CY - Wien, Austria DA - 30.11.2015 KW - Prozessanalytik KW - Microplastics KW - Mikroplastik KW - Raman-Spektroskopie KW - Polymers KW - Multivariate classification PY - 2015 SP - 80 EP - 81 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-38847 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jörres, R. A1 - Ehret, M. A1 - Karrasch, S. A1 - Herbig, B A1 - Schierl, R. A1 - Seeger, Stefan A1 - Langner, J. A1 - Nowak, D. T1 - Respiratorische Effekte von Drucker- und Kopierer-Emissionen – eine kontrollierte Expositionsstudie N2 - Die möglichen gesundheitlichen Auswirkungen von Laserdruckeremissionen sind immer wieder Gegenstand von Aufmerksamkeit. Wir untersuchten die Effekte 75-minütigerExpositionen gegenüber Low-Emittern (LE, Untergrund 2000 – 4000 UFP/cm3) und High-Emittern (HE, 100.000 UFP/cm3). T2 - 56. Kongress der Deutschen Gesellschaft für Pneumologie und Beatmungsmedizin e.V. CY - Berlin, Germany DA - 18.03.2015 KW - Expositionsstudie in-vivo KW - Bürogeräte KW - Emissionen KW - Partikel PY - 2015 DO - https://doi.org/10.1055/s-0035-1544873 VL - 69-V516 SP - V516 PB - Thieme CY - Stuttgart AN - OPUS4-38752 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ferraioli, M. A1 - Abruzzese, D. A1 - Miccoli, Lorenzo A1 - Mandara, A. ED - Galea, P. ED - Borg, R. P. ED - Farrugia, D. ED - Agius, M. R. ED - D'Amico, S. ED - Torpiano, A. ED - Bonello, M. T1 - Dynamic identification and seismic safety of two masonry towers N2 - The recent experience of Italian seismic events provided wide observational information about typical behaviour, damage patterns and intrinsic vulnerability of monumental buildings. Evidence indicates that historical constructions are by far the most vulnerable from the seismic point of view. As a consequence, they demand for the definition of urgent strategies for the protection of cultural heritage from seismic hazard. The main goal of an in-depth knowledge of the structure should help to avoid inadequate, unsuitable or dangerous rehabilitation operations, as well as to select non-invasive and reversible techniques for the best exploitation of material and technology features. The definition of reliable models and methods for seismic risk assessment of historical constructions is today a very important topic. Typical problems of masonry structures concern aspects like inherent structural lacks, material degradation, geotechnical problems, buckling behaviour of slender elements and dynamic loading vulnerability. Modelling the mechanical behaviour of masonry may play an important role, due to both inherent material complexity and great scatter in mechanical properties. Effective procedures for the identification of the structural parameters from static and dynamic testing are thus required. In particular, dynamic measurements may be very useful for the identification of mechanical properties and soil restraints and, consequently, for the calibration of advanced numerical finite element models. The paper addresses two case studies of structural monitoring and seismic assessment of medieval masonry towers in Italy: the bell tower of Aversa and the bell tower of Capua. These monuments, placed in the Campania region, were monitored by means of full-scale environmental vibration testing. Measured responses are then used for modal identification with a typical finite element model updating technique based on vibration test results. Parameters optimization is carried out on the basis of a criterion which minimises a weighted error on modal properties. A satisfactory improvement in the determination of modal parameters is thus obtained, resulting in a close agreement between the modal properties observed in dynamic tests and those calculated from numerical model. Seismic assessment is finally performed based on nonlinear static analysis of the tower under multimodal distributions of lateral loads. Results from nonlinear analysis indicate the potential collapse mechanisms and evidence dangerous structural weakness which may play a role in the seismic vulnerability of the towers. T2 - Georisk in the Mediterrean and their mitigation CY - Valletta, Malta DA - 20.07.2015 KW - masonry towers KW - ambient vibration tests KW - dynamic characterisation KW - seismic assessment PY - 2016 SN - 978-88-98161-20-1 SP - 250 EP - 251 PB - Mistral Service AN - OPUS4-37204 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holm, Olaf A1 - Simon, Franz-Georg T1 - Recovery of copper from small grain sizes of municipal solid waste incineration bottom ash by means of density separation N2 - Small grain sizes of municipal solid waste incineration (MSWI) bottom ash (BA) contain elemental and chemically bonded metals in appreciable amounts, especially copper. As different copper species have in general a higher density compared to the prevalent minerals, processes for density separation seemed to be favorable for the recovery of copper. Investigations with a centrifugal classifier were therefore carried out with BA from MWSI which have been used for a few years as the covering material for a landfill. The results show an appreciable enrichment of the precious copper. The concentrates contained up to 60 mg/kg copper in the dry weight (DW) (in general about 30 – 40 mg/kg DW) with enrichment factors of around 20 and a copper recovery of up to 50 % (in general around 20 %). A test series in order to evaluate the potential benefit for sequential processing illustrate the low efficiency for a further processing of the tailings. T2 - SUM 2014 - 2nd Symposium on Urban Mining CY - Bergamo, Italy DA - 19.052014 KW - Municipal solid waste incineration (MSWI) KW - Density separation KW - Bottom ash (BA) KW - Copper PY - 2014 SN - 9788862650311 SP - 1 EP - 7 PB - CISA Publisher CY - Padova, Italy AN - OPUS4-37308 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Le, Quynh Hoa A1 - Bäßler, Ralph A1 - Yevtushenko, Oleksandra A1 - Kratzig, Andreas A1 - Bettge, Dirk T1 - Synergistic effects of impurities in the condensate on the corrosion of CO2 transport pipeline N2 - For the reliability of transport pipelines the corrosion resistance of the materials used needs to be determined in conditions, which are possible during the transport process. In some situations condensation of components out of the CO2 stream can occur. To study the effect of condensate on transport pipeline steel, a “worst-case scenario” gas mixture, containing 2.5 % H2O, 1.8 % O2, 1000 ppmv NO2, and 220 ppmv SO2, was proposed, fed (1.5 L/min) into a glass reactor containing coupon-shaped specimens for 120 600 h at 278 K (to simulate the underground pipeline transport), and resulted in the condensate containing 0.114 M H2SO4 and 0.0184 M HNO3 (pH 2.13). Basing on this “original” condensate, exposure tests and electrochemical characterization together with pH and conductivity in CO2 saturated condition at the same temperature were carried out. The role of each gas impurity and the combination of them, when the condensate is formed, was studied by investigating the role of individual and varying combination of acidic components in the condensate on the corrosion behaviors of the commercial pipeline-steel (L360NB). It can be concluded that although the condensation of NOx in form of HNO3 causes faster corrosion rate, it is the condensation of SOx or the combination of SOx and NOx that may cause much more severe problems in form of localized and pitting corrosions. Different to the corrosion products formed in CO2 atmosphere without impurities (mainly iron carbonate) the corrosion products resulted from these acidic condensation have no protectability, indicating the need of controlling gas quality during the transportation within the pipeline network. T2 - EUROCORR 2017 - PRAG CY - Prague, Czech Republic DA - 03.09.2017 KW - CCUS KW - CO2 corrosion KW - Carbon steels KW - Condensate PY - 2017 SP - Paper 75636,.1 EP - 4 AN - OPUS4-41874 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Miccoli, Lorenzo A1 - Müller, U. A1 - Fontana, Patrick ED - Mazzolani, F. M. ED - Lamas, A. ED - Calado, L. ED - Proenca, J. M. ED - Faggiano, B. T1 - Strengthening of rammed earth structural elements. Mechanical behaviour under shear and cyclic loading N2 - An experimental investigation was carried out to study the in-plane shear behaviour of rammed earth structural elements strengthened with polyester fabric strips. The original idea for the retrofitting with polyester fabric strips was to introduce a vertical element for walls in order to take up horizontal loads resulting in a shear response of the building element. It has to be considered that vertical slits into the walls for fixing the strips are points of weakness and have to be mitigated by the adhesive. In this case a base coat mortar was employed. Strengthened elements were tested to exploit the strength potential of earthen materials and to solve its lack of tensile strength, significantly improving not only strength but also ductility. As part of the study results of a testing campaign of unstrengthened structural elements were considered. Strengthened elements were tested in diagonal compression/shear and cyclic shear-compression. A unique reinforcement orientation was used. The results of these tests are presented in this paper and include the load-displacement behaviours, crack patterns, failure modes. The results showed that the reinforcement was the most effective under cyclic shear-compression tests, with increase in load and displacement capacity observed. Under diagonal compression the reinforcement did not likely contribute significantly to the shear resistance, due to a lack of embedment length of the strips. T2 - 3rd International Conference on Protection of Historical Constructions (PROHITECH 2017) CY - Lisbon, Portugal DA - 12.07.2017 KW - Rammed earth KW - Diagonal compression tests KW - Shear-compression tests KW - Strengthening KW - Polyester fabric strips PY - 2017 SN - 978-989-8481-58-0 SP - 157 EP - 158 PB - IST-Press AN - OPUS4-41263 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ferraioli, M. A1 - Miccoli, Lorenzo A1 - Abruzzese, D. ED - Mazzolani, F. M. ED - Lamas, A. ED - Calado, L. ED - Proenca, J. M. ED - Faggiano, B. T1 - Seismic risk assessment of the Santa Maria a Vico bell tower. Ambient vibration measurements and numerical model tuning N2 - The paper investigates the dynamic characterisation along with the numerical model tuning and the seismic risk assessment of a monumental masonry tower in Italy namely the Santa Maria a Vico bell tower. Full-scale ambient vibration tests were performed under the impact of environmental loads. The technique of modal extraction in the frequency domain was applied. In-situ investigation survey was used in calibrating the refined 3D finite element model. The FEM tuning was carried out by varying the mechanical parameters and accounting for the restraint offered by the neighbouring buildings and the role of soil–structure interaction. The paper shows that the modal identification is a reliable technique that can be used in-situ for assessing the dynamic behaviour of monumental buildings. The tuned FEM model of the tower was usefully employed to determine the theoretical fundamental frequencies, which accurately fit the experiment data. Finally, the seismic performance of the bell tower was assessed using a non-linear static procedure based on the multi-modal pushover analysis and the capacity spectrum method. The results confirm that seismic events of moderate intensity can produce heavy damage to the masonry tower presented in this study. T2 - 3rd International Conference on Protection of Historical Constructions (PROHITECH 2017) CY - Lisbon, Portugal DA - 12.07.2017 KW - Masonry tower KW - Ambient vibration tests KW - Dynamic characterisation KW - Seismic assessment PY - 2017 SN - 978-989-8481-58-0 SP - 159 EP - 160 PB - IST-Press AN - OPUS4-41279 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -